EXPERIMENT A: CIS-TRANS CONVERSION OF BUTENEDIOIC ACID PRE-LAB ASSIGNMENT 1. Maleic acid is the cis version and fumaric acis is the trans version of butenedioic acid. 2. 3. See attached paper. 4. Maleic anhydride is the compound that crystalizes in part A in the experiment. 5. HCl acts as a catalyst to break one of the carbonyl group in the maleic acid which rotates the structure to form a trans structure of the butonal acid which is the fumaric acid. And it does so by donating
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Darsh Patel Dr. Anthony Chem 101-L 20 March 2013 Indirect gravimetric determination of hydrate compound in a mixture Objective To determine the percent BaCL2*2H2O in sample of hydrated mixture. Materials: Aprons‚ goggles Gravimetric balance(electronic weighing scale) Crucible without cover Bunsen burner Lighter flint Iron Support stand Wire mat‚ glove Clay triangle Procedure: Step 1. Support a clean porcelain crucible and its cover on a clay triangle (see Figure 1). Heat them in
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Analysis of an Unknown Mixture Performed: 2/13/14 Submitted: 3/3/14 Abstract: The purpose of this experiment was to separate and identify the two unknown compounds. The sample used was 105 and it contain 2-propanol and 2-heptanone. IR spectrums were taken of the contents of the second and sixth test tubes and showed the presence of an OH functional group and a small amount of ketone in test tube two and a large presence of ketone in test tube six. The average boiling points of the test tubes
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Impurity Lab Report Aim: To find out the difference of the boiling point and melting point when adding impurity (salt) to water. Diagram: Method: 1.Set up the apparatus as shown in the diagram 2. Get a known amount of ice in the beaker (half full)‚ and a known amount of salt in another beaker 3. Measure the temperature (melting point) of the ice without adding any impurity (salt). 4. Measure the temperature (melting point) of the ice after adding the salt into the beaker. 5. Heat up
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of a Mixture Purpose: To become familiar with the methods of separating substances from one another using decantation‚ extraction‚ and sublimation techniques. Apparatis and Chemicals: balance‚ Bunsen burner‚ rubber hose‚ tongs‚ 2 evaporating dishes‚ 2 watch glasses‚ 100-mL graduated cylinder‚ clay triangles‚ 2 ring stands‚ 2 iron rings‚ 2 glass stirring rods‚ unknown mixture of NaCl‚ NH4Cl‚ SiO2. Discussion: Mixtures are composed of two or more substances mixed together. Mixtures can
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Hypothesis: The higher the concentration of hydrochloric acid‚ the faster the reaction will take place because there will be more hydrochloric acid particles to collide with the marble chip particles therefore resulting in a quicker reaction. The lower the concentration‚ the weaker the reaction will be as there will be fewer particles so less chance of a collision and a lower rate of reaction. Equipment: Conical flask – to hold the hydrochloric acid and marble chips Boiling tube – to hold and indicate
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ACYL COMPOUNDS: SOAPS AND DETERGENTS Experiment # 8 I. Objectives To observe the general properties of carboxylic acids. To compare the acidity of carboxylic acids and phenols. To verify experimentally the interconversion among acyl compounds. To become familiar with the physical and chemical properties of fats and oils and to understand the chemical basis of these properties. To learn how to prepare soap. To compare the properties of soap and synthetic detergents. II. Data and
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Experiment No. 1: MELTING POINT AND BOILING POINTS OF ORGANIC COMPOUNDS ABSTRACT The properties of organic compounds depend on their chemical structures. Intermolecular forces of attraction affect physical properties such as melting and boiling point. Through the Thomas Hoover apparatus‚ the melting point of 8 test compounds was determined. Salicylic acid exhibited the highest melting point while naphthalene‚ the lowest. The stronger the intermolecular forces of attraction‚ the higher the melting
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Hyejin Cho 12 June 2013 Separation of a Mixture Abstract: In this experiment‚ the three processes of extraction‚ sublimation and recrystallization will be used to separate a mixture of salicylic acid and naphthalene. The first part of extraction will be to separate the salicylic acid from the naphthalene using diethyl ether and aqueous sodium bicarbonate. The naphthalene will reside in the ether and be the top layer‚ while the salicylic acid resides in the sodium bicarbonate bottom layer
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EXPERIMENT 1: REACTIONS OF ENOLATE IONS WITH CARBONYL GROUPS Aims In this experiment we used two techniques for the reactions of enolate ions with carbonyl groups. One technique used was Doebner reaction and the other technique used was Claisen-Schmidt reaction. Therefore the aim of this experiment is to synthesize trans p-methoxycinnamic acid and to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde. The products would be recrystallized using ethanol
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