covers the learning of simple laboratory techniques such as reflux‚ distillation‚ extraction‚ crystallization and melting point determination‚ preparations of organic compound and separation of mixtures. The Techniques Students are REQUIRED to read and understand the various techniques that will be covered in the laboratory sessions from the textbook. | Techniques | Page | 1 | Laboratory Safety | 6 | 2 | Laboratory Glassware | 31 | 3 | Measurement of Volume and Weight | 39 | 4 | Heating
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Experiment #1: Separation of Acid‚ Base‚ and Neutral Compounds from a Solid Mixture by Liquid-Liquid Extraction Introduction Liquid-liquid extraction is a technique used to separate chemical substances in order to purify or identify the various components of a mixture. Flavors‚ spices‚ perfumes‚ and medicines are just some of the everyday things that are extracted from plants and other natural sources [1]. The basic principle used to carry out this separation is the mixing of two liquids that are
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Separating Acids and Neutral Compounds by Solvent Extraction Introduction The purpose of this experiment was to use solvent extraction techniques in order to separate a mixture consisting of a carboxylic acid (p-toulic acid)‚ a phenol (p-tert-butylphenol)‚ and a neutral compound (acetanilide). Extraction is the process of selectively dissolving one or more of the compounds of a mixture into an appropriate solvent‚ the solution that contains these dissolved compounds is called an extract (Manion
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The compound is the substance that can be two or more elements that can be changed. Water is a compound. It contains both Hydrogen and oxygen that can stand alone by itself. The mixture is when two different substances that are blended together. The air is a mixture of these elements carbon dioxide‚ nitrogen‚ and other stuff. Most mixtures are known to be naturally. The main difference between the compound and the mixture is how they are combined. In the pure substance‚ the only way to know if
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Other nitrogen containing compounds Catecholamine: Dopamine‚ norepinephrine (noradrenaline) and epinephrine (adrenaline) are biologically active amines and are collectively called as Catecholamine. * Dopamine and norepinephrine functions as neurotransmitters. Outside the nervous system‚ norepinephrine and its methylated derivative‚ epinephrine regulates carbohydrate and lipid metabolism. They are released from storage vehicles in the adrenal medulla in response to stress (fright‚ exercise‚ cold
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Experiment Separation of Organic Compounds by Acid-Base Extraction Techniques 5 A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require extraction at some stage of product purification. In this experiment you will use extraction techniques to separate a mixture of an organic acid‚ a base‚ and a neutral compound. Organic acids and bases can be separated from each other and from neutral compounds
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report Isolating the Components of a Three Component Mixture The purpose of this experiment was to separate the component of three mixtures sand‚ sodium chloride and calcium carbonate then calculate the percentage by mass of each component recovered from the mixture. The other purpose of this experiment was to show us the students the concepts associated with physical and chemical properties of substances. Me and my lab partner‚ obtained a mixture of a un known proportion from the instructor
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Experiment Acids‚ Bases‚ and Neutrals Problem Are common house-hold products pH balanced and neutral? Information Gathered pH measures how acidic or alkaline a solution is. The pH scale ranges from 0-14. Solutions that range from 0-6 are considered to be acidic. Solutions that are on the acidic end of the scale are low in pH‚ high in hydrogen ion‚ and low in hydroxyl ions. An acid has a sour taste‚ hence‚ will react to metal and will be corrosive; therefore‚ they are considered as an electrolyte
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TECH0701: Measuring the Melting Points of Compounds and Mixtures Introduction This exercise dealt with the melting points of pure mandelic acid and benzoic acid. The eutectic temperature and composition of mandelic and benzoic acid mixtures were determined. And finally‚ an unknown was identified by its mixtures and melting point. The melting point of a compound is used by organic chemists not only to identify the compound‚ but also to establish its purity. To determine the melting point two
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EXPERIMENTAL PROCEDURE: 1. 2.07 g of the mixture of naphthalene and benzoic acid was weighed accurately on a balance. The mixture was then dissolved in 40 ml dichloromethane and the solution was poured into a separatory funnel. 2. 20 ml of aqueous sodium bicarbonate solution was added to the dichloromethane. A stopper was placed on the separatory funnel and was shaken and pressure was frequently released. The 2 liquids separated into clear layers and the lower layer (dichloromethane layer) was
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