Experiment 2: Separation of a Mixture of Solids Purpose: This experiment allowed me to learn different separation techniques for various substances based on their specific chemical properties. Procedure: I began this experiment by using a magnet to pick up and collect the iron filings out of the mixture. Then the sand was separated by placing the mixture into a beaker and boiling it in distilled water in order to dissolve the salt and benzoic acid‚ once boiling the liquid was poured out leaving
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Mixtures and Solutions can often become confusing because solutions are mixtures‚ but not all mixtures are solutions. A mixture can either be homogeneous or heterogeneous. A homogeneous mixture is where the mixture’s components are distributed uniformly within the mixture. A heterogeneous mixture is where the components are not uniform. Mixtures can either be miscible or immiscible‚ the difference being whether or not the mixture forms a homogeneous mixture or not. In a solution a solute is soluble
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Experiment #5: Esterification of Methyl Benzoate from Benzoic Acid October 28‚ 2010 Abstract: This experiment was conducted to synthesize methyl benzoate from benzoic acid and methanol by using the Fischer esterification method. Methanol (12.5ml) and Benzoic acid (4.9 grams) are heated together in the presence of concentrated sulfuric acid (1.5ml) until equilibrium is achieved. A reflux apparatus is set up for 1 hour to carry out the reaction at the boiling point of the solvent (Methanol
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TABLE OF CONTENTS What is a Mixture? What are the types of Mixtures? Define:-solutions -suspensions -colloids (Draw and compare.) Methods of separation 1. Filtration 2. Distillation (simple and fractional) 3. Paper chromatography 4. Solvent extraction 5. Separating funnel 6. Evaporation 7. Crystallization 8. Sublimation Draw and explain each. What is a mixture??? A mixture is a combination of two or more substances that are not chemically
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Abstract By separating chemicals out of a mixture and purifying them through sublimation and recrystiliation‚ changes in the substances physical properties can be shown. A salicylic acid-naphthalene mixture was mixed together with diethyl ether and saturated sodium bicarbonate. Two layers separated and were extracted after acidifying with HCl. This precipitated the crude salicylic acid. The left over mixture was combined with water and the two layers separated where crude naphthalene was recovered
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Experiment 1: Solubility of Organic Compounds (Answers to Questions) Q1. State what types of inetmolecular forces are present in solutions formed due to intermolecular attractions between the solute and the solvent. A1. For Water-Soluble Compounds: Acetone – Water: Hydrogen bonding and van der Waals forces Acetone – Diethyl Ether: Dipole – (induced) dipole and van der Waals forces Sucrose – Water: Hydrogen bonding and van der Waals forces Ethyl alcohol – Water: Hydrogen bonding
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of Organic Compounds Sunshine Marie Introduction Each year‚ many thousands of new or unknown organic compounds are prepared or extracted from natural sources such as plants‚ fungi and animals. In order to identify an unknown organic compound or the components of a mixture of organic compounds‚ it is necessary firstly to separate and purify the compounds. At any given temperature‚ a certain number of molecules of a substance in the liquid state have sufficient energy to escape from the surface
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LS Separation of Mixtures and Solids Purpose: To become familiar with the separation of mixtures of solids Hypothesis: I will be able to separate the materials using a variety of different methods. First‚ separate the iron fillings using a magnet. Second‚ I will put the rest of the solution into water and separate the insoluble sand from the soluble salt and benzoic acid. Third‚ I will filter out the benzoic acid when crystalized. Lastly‚ I will evaporate the water away leaving crystallized
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Introduction This lab’s purpose was to determine whether Salicylic Acid made from methyl salicylate is the same as Salicylic Acid made from benzene. This information can be found by comparing the difference in melting points of the two samples of Salicylic Acid. Here are the physical properties of Salicylic Acid and the mechanism of reactions that occurred in this lab. How Salicylic Acid is derived: Procedure/Results First‚ .26mL of 2.0mmol methyl Salicylate was measured and put
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Abstract The objective of this experiment was to observe multi-step purification of benzoic acid after performing the extraction from a mixture containing benzoic acid‚ cellulose‚ and methyl orange. Recrystallization was done to remove impurities from the sample. The amount of BA recovered during recrystallization is much less than the extracted amount of BA. The difference between the pure and impure samples was observed by comparison of melting points. It was found that impure samples will have
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