CONDENSATION Synthesis of Cinnamaldehyde I. Introduction Cinnamaldehyde‚ cinnamic aldehyde or 3-phenyl-2-propenal is the major constituent of cinnamon oil‚ extracted from several species of Cinnamomum (C. verum‚ C. burmanii‚ C. cassia)‚ under the family Lauraceae‚ a group of evergreen trees. Cinnamon bark (particularly C. verum) yields 0.4-0.8% oil‚ which contains 60-80% cinnamaldehyde‚ 4-5% sesquiterpenoids (α-humulene‚ β-caryophyllene‚ limonene and others)‚ eugenol‚ cinnamyl acetate‚ eugenol acetate
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Engineering University of Santo Tomas España‚ Manila Abstract Sodium carbonate (Na2CO3)‚ commonly known by trade name soda ash‚ is a white‚ anhydrous‚ powdered or granular material that is an essential raw material used in the manufacturing of glass‚ detergents‚ chemicals‚ and other industrial products. In this experiment‚ the percent alkalinity of the unknown soda ash sample was determined by titrating it with standard HCl solution. After three trials‚ the researchers obtained an average percent
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eLearning 2009 Publication No. 91860 Rate of Reaction of Sodium Thiosulfate and Hydrochloric Acid Rate Laws Introduction The purpose of this demonstration is to investigate the effect of sodium thiosulfate concentration on the rate of reaction of sodium thiosulfate with hydrochloric acid. The reaction‚ which produces solid sulfur‚ will be followed by measuring the time needed for the reaction mixture to become opaque. The results will be analyzed graphically to determine the order of
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In the experiment‚ we tested a sodium chloride solution. Along with the tested solution‚ control groups (water and sodium phosphate) were used to be help understand whether or not NaCl was a buffer. Water was the negative control group and sodium phosphate was the positive control group. If NaCl was a buffer than the pH would be stabled as the sodium phosphate buffer. If NaCl was not a buffer than the pH would fluctuate like the negative control‚ water. During the first trial and prior to the drops
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Lab 4. Volumetric Determination of Impure Sodium Carbonate (Na2CO3) Introduction: To determine the total amount of carbonate in unrefined sodium carbonate‚ soda ash‚ a titration is done using a standardized solution of HCl. Aqueous HCl is a strong acid and therefore almost completely disassociates into H+ and CL-. Therefore‚ when HCl is used in a titration‚ the H+ is the titrant. Carbonate in aqueous solution is able to accept a proton‚ i.e. it acts as a base. When carbonate accepts the H+ a bicarbonate
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Making Sodium Chloride Equipment: Method: 1. Firstly‚ safety measures were taken by putting on laboratory coats‚ wearing safety goggles and tying long hair back. This was to protect clothing‚ eyes and to avoid burning as the experiment included dealing with open flames. 2. The equipment needed (as shown and labelled in picture A) was collected. 3. Using a measuring cylinder for each‚ to be exact with measurements‚ we measured out 10cm³ of HCl and 10cm³
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Synthesis of Acetanilide By: Rick Whitely April 9‚ 2013 Organic Chemistry Lab 1; Professor J. Hutchison Recrystallization is a common method of purifying organic substances through the differences in solubility at different temperature. In this experiment‚ acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heated water bath. The solution was cooled slowly in an ice bath as crystals form out. As the compound crystallizes
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Sodium Zeolite Softening Introduction Cation Exchanger Bead + + + + + - -+ -+ + + + + -+ + + - -+ -+ + - + + -+ Ion exchange is the process in which materials exchange one ion for another‚ hold it temporarily‚ and release it to a regenerating solution. These materials are widely used to treat raw water supplies that contain dissolved salts. Today‚ the most commonly used material is an ion exchange resin. Resins are plastic beads to which a favorable
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12-STANDARDIZATION OF SODIUM HYDROXIDE Standard solutions for titrations are especially pure mixtures with exactly known concentrations. Primary standards are very pure solids. They have the advantage that they can be weighed (the analytical balance is normally the most accurate instrument in the laboratory) and they are stable under laboratory conditions. In this experiment‚ the primary standard is oxalic acid dihydrate‚ H2C2O4 ( 2H2O. It will be used to standardize a solution of sodium hydroxide
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Purpose of this experiment is to synthesis Banana oil by mixture of the isopentyl alcohol and acetic acid . Banana oil smells like fruit mostly it smells like banana. This reasons that this compound uses in different perfume products as well as the gums for the flavor. The reaction that takes place in this experiment is a esterification. In this experiment‚ the carboxyl group of the acetic acid joins with the hydroxyl group of the isopently alcohol‚ catalyzed by the presence of sulfuric acid
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