CONDENSATION Synthesis of Cinnamaldehyde I. Introduction Cinnamaldehyde‚ cinnamic aldehyde or 3-phenyl-2-propenal is the major constituent of cinnamon oil‚ extracted from several species of Cinnamomum (C. verum‚ C. burmanii‚ C. cassia)‚ under the family Lauraceae‚ a group of evergreen trees. Cinnamon bark (particularly C. verum) yields 0.4-0.8% oil‚ which contains 60-80% cinnamaldehyde‚ 4-5% sesquiterpenoids (α-humulene‚ β-caryophyllene‚ limonene and others)‚ eugenol‚ cinnamyl acetate‚ eugenol acetate
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being that Silica gel in TLC 2 was polar and the solvent ethyl acetate-hexane is non-polar it moved relatively with the solvent. The stationary phase in TLC 3‚ alumina is non polar and the solvent ethyl acetate is polar so from the ideal that polar does not attract non-polar benzophenone stick stronger to alumina non-polar rather than moving up with polar solvent ethyl acetate as it did in tlc2. 6. Ethyl acetate is polar and Ethyl acetate- hexane is nonpolar‚ use of polarity differences. Because the
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RUNNING HEAD: Synthesis of Banana Oil Abstract A reflux apparatus was assembled with a water-cooled condenser and a drying tube. Isopentyl alcohol‚ glacial acid sulfuric acid is added to a 25 milliliter round bottom flask and attached to the reflux apparatus. The mixture was boiled‚ the extracted first using water followed by aqueous sodium bicarbonate. The mixture was dried using anhydrous granular sodium sulfate. After dried‚ the sample was placed in a distillation apparatus and heated. This
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attached. substance Hazards‚ risks and safety practices MW (g/mol) Amt. Used Mol. mp (K) bp (K) density(g/cm^3) acetone R11‚ R36‚ R67‚ S9‚ S25‚ S26 58.08 0.24 g 0.004 178.2 329.4 0.79 benzaldehyde R22‚ S24 106.13 0.82 g 0.008 247 451.1 1.0415 ehtyl acetate R11‚ R36‚ R66‚ R67‚ S16‚ S26‚ S33 88.11 2 ml per gram n/a 189.55 350.25 0.897 NaOH R35‚S22‚ S26‚ S38‚ S45‚ S62‚ s24/25 39.997 0.4 g 0.01 591 1663 2.1 Ethanol R11‚ S2‚ S7‚ S16 46.07 2 ml n/a 158.8 351.6 0.789 Dibenzalacetone n/a 234 g/mol n/a n/a
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Gay/Lesbian Families Adoption is an extremely sensitive subject‚(insert dash) especially for individuals who are Gay or Lesbian. There is much controversy on the topic. There are a variety of ways to which it isn’t possible for a couple to adopt. Infertility is becoming a greater problem in our time. In Gerald P. Mallon’s article‚ “Assessing Lesbian and Gay Prospective Foster and Adoptive Families: A Focus on the Home Study Process‚” in 2007. He introduces a few different ways gay men and lesbian
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Quitay Morris Jake N. Professor Rafie Paz ENGL 1013 July 29 2013 Why are Teenagers so Lazy Today? The youth is the hope of the nation. That is the sentence that defines what the teenagers’ worth to the country is. We are supposed to change what the country is now. But the question is . . . Can we? From what I observed is happening now‚ instead of being the country’s biggest hope‚ we seem to be one of its burdens. There’s pre-marital sex‚ prostitution‚ juvenile delinquencies‚ and the list
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added to this tube. If a purple color showed‚ it would indicate there was protein in the test tube. In the third separation of this experiment‚ the hood in the lab was used. The curds were placed in a 100 mL beaker and extracted using 30 mL of ethyl acetate. The curds were crushed with a stirring rod. This extraction was then gravity filtered through a funnel fitted with the filter paper. A rubber policeman was used to scrape the beaker to get as much casein as possible. This casein was then put aside
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2.2 Application of Cu2O nanopowder 2.2.1 Photocatalyst 2.2.2 Solar energy conversion 2.3 Powder formation 2.4 Gas phase 2.4.1 Inert Gas Condensation (IGC) or Gas Phase Condensation 2.4.2 Chemical Vapor Deposition 2.4.3 Laser ablation 2.4.4 Flame synthesis 2.5 Liquid phase 2.5.1 Solvent evaporation method 6 6 7 7 8 9 9 11 11 11 12 12 13 Page ii iii vii viii xii xiii 1 2 3 4 5 pdfMachine iii Is a pdf writer that produces quality PDF files with ease! Produce quality PDF files in seconds and preserve
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Purpose The purpose of this experiment is to determine the rate constants‚ k1‚ for the methyl acetate hydrolysis reaction at 25 °C and 35 °C‚ as well as the overall activation energy of the reaction. Methods Methyl acetate was placed in an HCl solution‚ in which it reacts with water to form acetic acid over time. At each time interval‚ an aliquot of the mixture was removed for titration against NaOH to determine the concentration of the acetic acid produced. From the amount of acetic acid produced
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Protein synthesis is one of the most fundamental biological processes. To start off‚ a protein is made in a ribosome. There are many cellular mechanisms involved with protein synthesis. Before the process of protein synthesis can be described‚ a person must know what proteins are made out of. There are four basic levels of protein organization. The first is primary structure‚ followed by secondary structure‚ then tertiary structure‚ and the last level is quaternary structure. Once someone understands
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