Purpose: To synthesize 1‚2‚3‚4-tetraphenylnaphthalene through a two-step synthesis. The aldol condensation reaction between benzil and dibenzyl ketone forms 2‚3‚4‚5-tetraphenylcyclopentadienone‚ which then reacts with a benzene formed by anthranilic acid and isoamyl nitrate in order to yield 1‚2‚3‚4-tetraphenylnaphthalene. Reaction Equation A: Synthesis of 2‚3‚4‚5-tetraphenylcyclopentadienone: A solution of 4 capsules potassium hydroxide (0.5g) and 5mL anhydrous ethanol was prepared
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Prelab 5B Macrocyclic Synthesis OBJECTIVE: The objective this week is to produce Tetraphenylporphyrin and its metal complex. This will be carried out by condensation of 4 equivalents of Benzaldehyde and pyyrole in the presence of propanoic acid. The product will undergo UV/Visible Spectrum tests to determine its lambda max. The lambda max will show us the relationship between a conjugated system and the visible spectrum. PROCEDURE: Step 1: preparation of meso-tetraphenylporphyrin (TPP)
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Synthesis of Acetanilide By: Rick Whitely April 9‚ 2013 Organic Chemistry Lab 1; Professor J. Hutchison Recrystallization is a common method of purifying organic substances through the differences in solubility at different temperature. In this experiment‚ acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heated water bath. The solution was cooled slowly in an ice bath as crystals form out. As the compound crystallizes
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Terrence Smith Advanced College Writing Dr. Ruby Parker Argument Synthesis April 21‚ 2011 Argument Synthesis In Mr. Siemiesz’s chapter he explained about the National Security Consequences of U.S Oil Dependence and how it could be fixed and changed for the best interest of the country; Mr. Siemiesz outlined specific points or steps the country could take to make those changes he outlined in the chapter. “Those major energy suppliers from Russia to Iraq to Venezuela have been increasingly
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A Synthesis of Safrole and o-Safrole W.H. Perkin & V.M. Trikojus J. Chem. Soc. 1663 (1927) HTML by Rhodium No direct synthesis of safrole has been recorded‚ the most recent attempt being that of Baker and Robinson (JCS‚ 1925‚ 127‚ 1424)‚ who distilled the product of the action of silver oxide and water upon gamma-piperonylpropyltrimethylammonium iodide‚ but obtained isosafrole‚ the double bond moving into the position of greater stability. Kawai (Sci. Papers Inst. Phys. Chem. Res.‚ 1925‚ 3‚ 263)
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DNA and the Gene: Synthesis and Repair 1) Watson and Crick elucidated the structure of DNA in 1953. Their research built on and helped explain the findings of other scientists‚ including ________. A) X-ray diffraction studies by Rosalind Franklin and Maurice Wilkins. B) Chargaff’s rules: C = G and T = A. C) Scientists who recognized that a nucleotide consisted of a sugar‚ a phosphate‚ and a nitrogen-containing base. D) All of the above were important considerations in the elucidation of
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You must pull your support from two of these texts: Beard‚ White‚ Sanders‚ Slouka‚ Burroughs‚ Hurd‚ Morano. Identifying and selecting relevant supporting details is analysis‚ and integrating those details into your essay to support your thesis is synthesis. Your essay—with your original thesis and the details you’ve chosen from the two essays—is a new‚ unique whole. The integration of your thesis‚ your supporting details‚ and your use of language to explain how it all coheres represent the workings
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Producing Isoamyl Acetate from Isoamyl Alcohol and Acetic Anhydride through Esterification Racquel Erica D.G. Isada‚ Jannah B. Juan*‚ Moses Isaiah L. Koh and Hedder A. Lim Department of Biology‚ College of Science University of Santo Tomas‚ España Street‚ Manila 1051 Date Submitted: August 13‚ 2014 Abstract: In this experiment‚ the synthesis of Isoamyl acetate from Isoamyl alcohol and Acetic anhydride was prepared with the process of Esterification. By using the reflux technique‚ extraction
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Synthesis and Analysis of the Coordination Compound Pentaaminechlorideocobalt (III) Chloride Heaven Lin and Forest Lin W.M. Keck Science Department‚ Claremont McKenna‚ Pitzer‚ and Scripps Colleges 925 N. Mills Avenue‚ Claremont‚ California 91711 Abstract Through using the spectrometer and titrations‚ the amount of the coordination compound‚ pentaaminechloridocobalt (III) chloride‚ was determined through a synthesis through an oxidation reduction of cobalt (II) chloride hexahydrate (CoCl2·6H2O)
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Peter Mehnert Rhet 105 Ms. Paterson 11/14/12 Extended Synthesis: Cigarette Smoking Tobacco has played an important role in America from the beginning. It was grown as a cash crop by the Jamestown settlers in 1612‚ but over the years the popular opinion has changed about tobacco. Tobacco is used to make cigarettes‚ which have been extremely popular‚ now known to be extremely dangerous. Even the warnings on the cigarette box have changed to a statement much more alarming. In the 1960s‚ the warning
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