PREPARATION OF ASPIRIN AND DETERMINATION OF THE MELTING POINT Ferrer‚ Lara Melissa V. Faculty of Engineering University of Santo Tomas Manila‚ Philippines ABSTRACT This experiment involved three steps: synthesis of aspirin‚ isolation and purification‚ and the estimation of purity of the final product. The synthesis involved the reaction of salicylic acid and acetic anhydride in the presence of a catalyst‚ phosphoric acid‚ H3PO4. When the aspirin was prepared‚ it was isolated and filtered. The percentage
Premium Aspirin Acetic acid Acetic anhydride
| | | |Chem201L | | Determination of an Unknown Compound using Mixed Melting Point Method Winnie Adrian Ibanez‚ Jerome Allan Japitana‚ and Dante Jimenez III Group no. 7‚ 2Chem a Department of Chemistry‚ College of Science‚ University of Santo Tomas‚ España‚ Manila‚ 1015‚ Philippines |ARTICLE
Premium Chemical compound Chemistry Melting point
Lab #1: Melting Points of Organic Compounds Report Form May 15‚ 2014 1. A “Melting Point Range” refers to the range of temperature at which a solid melts into its liquid state. 2. Pure compounds have narrow or ‘sharp’ melting point ranges‚ 1°C or less if the compound is very pure. A less pure compound exhibits a broader melting point range‚ between 3°C to 10°C as well as a depressed or lower range. 3. Crushing the sample allows for greater surface area-to-volume ratio of the powder‚ this
Premium Temperature Thermodynamics Heat
Preparation and melting point of Aspirin Aspirin is a painkilling drug and is produced worldwide to reduce and stop pain. Aspirin is made up of ehtanoylation of 2-hydroxbenzenecarboxylic acid in a presence of phosphoric acid. AIM: The aim of the experiment is to prepare and produce aspirin as pure as possible. I will do this threw preparing the aspirin and purifying the product threw recrystallization. I will then obtain a melting point of my product to get an estimate of its purity. By the end
Premium Thin layer chromatography Purity Liquid
EXPERIMENT A PREPARATION OF ASPIRIN Abstract This report gives a detailed account of the experimental preparation of aspirin in a laboratory environment as well as some basic industrial background on the product. It also contains information about safety precautions put in place to ensure the safety of the team who carried out the experiment. All results obtained have been included as well as a detailed analysis of what they represent alongside any improvements to the method used. Introduction
Premium Acetic acid Aspirin Acetic anhydride
Reshmi Nair Title: Determination of Aspirin through back titration. Aim: To determine the concentration of Aspirin in a tablet using NaOH and Hcl. Research Question: What is the concentration of Aspirin in a normal tablet? Background: Aspirin is the general name for acetylsalicylic acid (ASA); it is also the trademark of the drug produced by Bayer in Germany. In eighty countries‚ aspirin is a registered trademark‚ but in other places the term aspirin refers to ASA by itself or as an ingredient
Premium Paracetamol Ibuprofen Sodium hydroxide
Preparation and Recrystallisation of Aspirin Contents Page Synopsis iii 1 Introduction 1 1.1 Objective 1 1.2 Background 1 2 Theory 1 3 Procedure 2 3.1 Materials 2 3.2 Preparation 2 3.3 Recrystallisation 3 3.4 Determination of Melting Point 3 4 Results and Calculation 4 4.1 Mass 4 4.2 Percent yield 4 4.3 Melting Point 4 4.4 Appearance 4 5 Discussion 5
Premium Acetic anhydride Acetic acid Aspirin
Preparation and Recrystallization of Aspirin Preparation and Recrystallization of Aspirin Date of the experiment: 9 May 2013 Date of submission: 23 May 2012 Date of the experiment: 9 May 2013 Date of submission: 23 May 2012 Synopsis 1. General Objective: To familiarize with the preparation of some simple organic compound and purify the compound by recrystallization. Specific Objective: The experiment is carried out to: 1.1 Conduct the synthesis of aspirin
Free Aspirin Acetic acid Acetic anhydride
written up what you did in measuring the melting point in 3rd person past tense. | Determining the melting point of aspirin • Firstly we turned on the melting point equipment; we referred to data tables for the actual value for the melting point of the aspirin. • Then we arranged the equipment to a point below the expected melting point we then noted that the rate of heating will influence the reading of the melting point. • Afterward we dipped the sealed capillary
Premium Titration Liquid Sodium hydroxide
Melting Point Determination Identity and Purity of Solid Organic Compounds Objectives • To introduce the technique of melting point determination. • To use the concept of melting points for identification and characterization of organic compounds. • Properly fill and use a capillary melting point tube. • Determine accurate melting point ranges for a wide variety of organic substances. Introduction The melting point of a solid can easily and accurately be determined
Premium Temperature Melting point