Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5% and
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Spectra Analysis Organic Chemistry Lab‚ CHEM 369 The University of Tennessee‚ Knoxville Dr. Smith Spectra 1: tert-butyl cyanoacetate Molecular formula: 141/13 = 10 R 11 => C10H10+11 => C10H21 C10H21NO2 – C3H10 = C7H11NO2 DBE: 2(#C - #H/2 - #X/2 + #N + 2)/2 =2(7 – 11/2 – 0/2 + 1 + 2)/2 = 3=> 1 double bond and 1 triple bond Mass spectrum table: m/z fragment |40
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objective of the experiment was to prepare Benzilic acid by multistep synthesis starting with benzaldehyde. In this setup however‚ product of the first step‚ Benzoin‚ is provided thereby omitting the first step involving the conversion of benzaldehyde. For this experiment‚ the microscale techniques of reflux‚ crystallization‚ and melting-point determination were used. Utilizing these techniques a product yield of 93% for benzil and 57% for Benzilic acid was obtained‚ as well as a melting point range
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Preparation and purification of acetylsalicylic acid Results and Data treatment (A) Preparation of aspirin i) Details about the reactants Reaction of the acetylation of salicylic acid is following From the balanced reaction above‚ it can be seen that the stoichiometry between salicylic acid and acetic anhydride is 1: 1. In this experiment‚ 21.7mmol of salicylic acid was used to react 6.0mL of acetic anhydride and salicylic acid was limiting reagent. The expected amount of salicylic
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Preparation and properties of boric acid Result The mass of borax‚ g | 10.0734 | The mass of watch glass‚ g | 36.2842 | The mass of watch glass with product‚ g | 39.9803 | The mass of product‚ borix acid‚ g | 3.6961 | Test | Result | Boric acid is dissolved in water and methyl red indicator is added. | Pink solution is observed | Mannitol is dissolved in water and methyl red indicator is added. | Pink solution is observed | Both solution is added together | The colour of solution
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Preparation of Acetylsalicylic Acid Abstract Acetylsalicylic acid was prepared using salicylic acid and acetic anhydride. As a result‚ a white‚ powdery substance was formed (0.1931g‚ percent yield 91.30%) and was defined by melting point (124.5 – 134.5°C) and observation of color change with ferric chloride. Introduction Acetylsalicylic acid (aspirin) is one of the most popular analgesic drugs on the market today. It also acts as an antipyretic and anti-inflammatory drug. Salicylic acid itself
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Experiment 6 Preparation and reactions of boric acid Objectives: To prepare boric acid from sodium tetraborate (borax) To carry out tests on the prepared sample of boric acid To study the physical and chemical properties of boric acid Introduction: Boron is an element in the p-block of the periodic table. It has the electron configuration of 1s22s22p1 and is in group 3 or goup 13 (IUPAC classification). In nature‚ it consists of two isotopes 10B (19.6%) and 11B (80.4%). Boron is bonded
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OECD DEVELOPMENT CENTRE Working Paper No. 129 (Formerly Technical Paper No. 129) ECONOMIC REFORM IN EGYPT IN A CHANGING GLOBAL ECONOMY by Joseph Licari Research programme on: Strengthening Links between Developing Countries: Regional Co-operation and Integration December 1997 OCDE/GD(97)226 TABLE OF CONTENTS ACKNOWLEDGEMENTS ........................................................................ 6 RÉSUMÉ .....................................................................................
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by everyday pollution from houses‚ factories‚ cars‚ and etc. This is the concept of acid rain‚ which according to EPA.gov is a broad term referring to a mixture of wet and dry deposition from the atmosphere containing higher than normal amounts of nitric and sulfuric acids. Acid rain isn’t just rain‚ its forms like hail or snow‚ which is wet deposition‚ and smoke or dust‚ which is dry deposition. The effects of acid rain are quite terrifying bringing all types of problems to the Earth‚ for example
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Acid Base Titration bre’ana March 1‚ 2013 Purpose: The purpose of this experiment is to determine the concentration of a solution of NaOH by titration with a standard solution of HCl. It was also the purpose to determine the concentration of a sample of white vinegar by titration with a standard solution of NaOH. Introduction: Using the method of titration is how the experiment gets to the conclusion of the concentration of a solution. When doing this experiment‚ measurement is very important
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