Stapleton June 18‚ 2012 Experiment 32: Identification of a Conjugated Diene from Eucalyptus oil Introduction In this experiment‚ the purpose was to prepare the Diels-Alder adduct of the unknown conjugated diene in Eucalyptus oil and determine the approximate percentage of diene in Eucalyptus oil. To discover the product of this reaction‚ isolate the adduct‚ and classify the diene from the melting point of its adduct. The unknown was one of four conjugated dienes. Maleic
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Identification of a Conjugated Diene from Eucalyptus Oil Introduction: When two carbon-carbon double bonds are positioned next to one another‚ a conjugated diene is formed. Conjugated dienes undergo a cycloaddition reaction with certain double bonds to afford cyclohexenes and related compounds. The reaction is named Diels-Alder. The Diels-Alder reaction is between 1‚3-butadiene and ethylene to produce cyclohexene + dienedienophile. The mechanism of the Diels-Alder reaction is classified as a
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Identification of a Conjugated Diene from Eucalyptus Oil Purpose: The purpose of this experiment was to prepare the Diels-Alder adduct of the unknown Conjugated diene in eucalyptus oil‚ to separate the adduct‚ and identify the unknown diene from the melting point of it¡¯s adduct. Introduction: This experiment was performed using techniques of heating under reflux‚ vacuum filtration‚ recrystallization‚ and melting point measurements. These techniques were used to separate the Diels-Alder
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Title: Identification of Conjugated diene from Eucalyptus Oil Abstract: The purpose of this experiment is to separate and identify a conjugated diene from eucalyptus oil by making its Diels-Alder adduct with maleic anhydride. The unknown is one of four conjugated dienes with its names and the melting points. The melting point of the adduct was 112°C revealed the identity of the diene in eucalyptus oil which was α-phellandrene. Introduction: Some natural hydrocarbons are conjugated dienes or trienes
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Cyclic dienes added to alkene dienophiles also lead to two new form of stereoisomeric products‚ the endo and exo products (Kilway‚ “Lecture”). In cases where dienes and dienophiles align above one another‚ the endo product is formed (Hunt). The endo product will have two axial substituent groups (Kilway‚ “Lecture”). This formation typically forms the major product because it takes less kinetic energy to be formed due to secondary orbital interactions with the substituents in transition states (Hunt)
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Conjugated linoleic acid‚ is a form of linoleic acid‚ an omega-6 fatty acid important to human health (Wang and Jones‚ 2004). The CLA is formed by the bacteria in rumen of certain ruminants but not for humans. It is obtained by humans from dietary sources such as beef‚ lamb and dairy products including milk and cheese (Wang and Jones‚ 2004). CLA is an antioxidant‚ anti-carcinogenic‚ anti-diabetogenic‚ anti-atherosclerotic‚ anti-catabolite as well as an immune system enhancer (Belury‚ 2002). Health
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Extraction of Jathropa curcas Seed Fats and Oil and Identification and Characterization of Unknown Oil Jose G. Intano‚ Jr. and Niescee Eiscene Talaman University of the Philippines Visayas Miagao‚ Iloilo xdvm_apollo469@yahoo.com‚ messyisnessy@gmail.com Abstract The experiment had the objectives of extracting fats and oil from plant sample using 3:2 hexane-isopropanol solvent through Soxhlet method and of identifying and characterizing unknown oil sample using different chemical analyses
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with the chemical composition of essential oil from the fruits of Solanum erianthum‚ a species extensively used in traditional medicine. The essential oil from fruits was extracted by hydrodistillation and the chemical composition of the essential oil was analyzed by gas chromatography-mass spectrometry (GC-MS). The yield of essential oil based on the dry weight of the plant was 0.05 % (v/w). Twenty two compounds accounting for 99.2 % of the total oil were identified. The main compounds were 9
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STEM AND LEAF CHARACTERIZATION OF Eucalyptus deglupta Austria‚ C.‚ Batenga‚ B.‚ Daysa‚ R.‚ Dela Rosa‚ J.‚ Rebong‚ C.1 1 Department of Biology‚ College of Science‚ University of Philippines Baguio Baguio City‚Philippines INTRODUCTION bole that reaches up to 240cm (Figure 1a). It has a multi colored bark that varies from green‚ yellow‚ bluish‚ purplish‚ pink and orange. It has a green under bark and right before exfoliation occurs‚ the bark changes to brownish maroon (Figure 1b). The colors
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Chem 253 - Organic Chemistry I Lab 10: Isolation of Identification of the major constituent of clove oil 3/15/2012 Purpose: The purpose of this lab was to isolate the cove oil from ground cloves and determine the identity of the major constituent that is known to have the molecular formula C10H12O2 through IR spectrometry. Theory: Many people search for alternative ways to treat illnesses other than the conventional use of drugs and surgery. These alternative ways include aromatherapy‚
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