considered by melting point and IR spectroscopy. Final purified triphenylmethanol weighed 8.02 grams and melted at 158.5-162 degrees Celsius. Introduction: Grignard reagents are the most useful way to form primary‚ secondary or tertiary alcohols from a carbonyl group. The Grignard reaction involves the nucleophilic addition of an organomagenesium complex to a carbonyl carbon followed by acid work-up. This reaction involves a single electron transfer between the carbonyl group and the grignard reagent
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Traditional way of synthesizing sensitive rhodamine starts with rhodamine B‚ amino compound‚ and some alkali additive in the presence of weak base. However‚ for RH-PY‚ the stearic hindrance of pyrene slows the reactivity‚ and the reaction does not go to completion. Therefore‚ the reaction procedure was modified as follows. First‚ HATU and DIPEA were used to activate the carboxyl group of rhodamine B‚ then the activated rhodamine B was reacted with 1-aminopyrene. By introducing this method‚ the reaction
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Synthesis of Chloroform -------------------------------------------------------------------------------- With Calcium Hypochlorite and Acetone When chlorine is passed into boiling alcohol‚ both chlorination of the methyl group and oxidation of the primary alcohol group to an aldehyde occur‚ giving trichloro-acetaldehyde or chloral: When chloral is treated with caustic alkali‚ fission of the C-C linkage occurs‚ giving chloroform and a formate. Acetaldehyde and also many ketones‚ such as acetone
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SYNTHESIS OF SILVER NANOPARTICLES AND ITS CYTOTOXIC EFFECT AGAINST THP-1 CANCER CELL LINE 1 * Department of Biotechnology‚ Modern College‚ Shivajinagar‚ University of Pune‚ Pune‚ India. Mrs Rebecca Thombre email rebecca.thombre@gmail.com Telephone 9822224957 020 400966725 ABSTRACT: Nanotechnology is a field of science which involves the synthesis and applications of nanoparticles. Silver nanoparticles (AgNp) have applications in various fields due to their unique
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Synthesis Paper Focus Question: What role do the Harry Potter books play in children’s education? In my freshman year in high school‚ Mr. Mehta‚ the Head of the English department‚ made some changes to our school’s English curriculum. One of these changes included introducing the fifth book of the Harry Potter series‚ Harry Potter and the Order of Phoenix‚ to our reading list. Mr. Mehta’s simple action attracted more attention than ever before! While students lauded his decision‚ most parents
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this lab was to synthesize triphenylmethanol from benzophenone and bromobenzene by the formation of a Grignard compound with the reagents bromobenzene and magnesium metal. The bromobenzene was first transformed into the Grignard compound and was then reacted with the benzophenone to make the final product. The mixture was then mixed with sulfuric acid and the organic layer was extracted via a separatory funnel. The mixture was then recrystallized from methanol and was allowed to dry and the percent
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Abstract This experiment is about the synthesis of 3-nitrobenzaldehyde through nitration. The nitration of benzaldehyde is an example of an electrophilic aromatic substitution reaction‚ in which a proton of an aromatic ring is replaced by a nitro group. Many aromatic substitution reactions are known to occur when an aromatic substrate is allowed to react with a suitable electrophilic reagent‚ and many other groups besides nitro may be introduced into the ring. Although the reaction produced a low
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women are able to take care of children through assistance. Most families in the world take assistance from other to take care of their children. For example‚ the government of US helps families who live there‚ and it gives them clothes‚ food‚ money‚ and scholarships to complete their education. In addition‚ there are many groups of people which help people such as charities. They take money from other people as donation to help people who need to take of children. People always give money to educational
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Megan Garber Professor Keltner Composition 1 3 November 2013 The Ways Media Portrays Women Throughout today’s society‚ media contributes to almost everyone’s daily life. From informative news channels to comical television shows‚ media proves to be effective in advertisement‚ releasing messages and informing the audience. Although media proves to be wildly effective in advertising‚ releasing messages and informing the audience‚ periodically destructive and misleading messages are provided
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without pay. Once we are a cathecist‚ we’re a cathecist forever. Every Christian is a cathecist. “Are you a Christian?” therefor you are a cathecist. We are FREE from Failure of Christians duties‚ Refusal to care for others‚ Earthly comforts or Exclusive relationships and Egoistic tendencies or Excuses. We should not be STUCK from Self-centeredness‚ Temptation‚ Unwillingness to work or Unfit‚ Cultural stubborness or Complacemency and
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