& Drew‚ A.(2007). Fisher esterification: Preparation of banana oil. University of Missouri: Kansas. [5]Aberdeen‚ S.(2011). Chemistry and reflux.eHow. Retrieved July 6‚ 2013 from: http://www.ehow.com/facts_6811659_chemistry-reflux.html [6]Retrieved July 6‚ 2013 from:http://www.chemicalland21.com/specialtychem/perchem/ISO-AMYL%20ACETATE.htm [7] Fischer esterification. Organic Chemistry.org.Retrieved July 6‚ 2013 from http://www.organic-chemistry.org/namedreactions/fischer-esterification.shtm
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Synthesis of Isopentyl Acetate (Banana Oil) Using A Fischer Esterification Reaction Purpose: The purpose of this experiment is to synthesize Isopentyl Acetate using a Fischer esterification reaction. Fischer esterification is an acid-catalyzed condensation of an alcohol and a carboxylic acid‚ yielding an ester and water. Isopentyl Acetate has the scent of banana oil‚ once synthesized it will be purified by distillation. Then the analysis of the sample using H NMR and IR will determine purity
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Abstract: For the first part of this lab we refluxed different Carboxylic acids and alcohols in the presence of a acid catalyst in order to form Esters by Fischer Esterification. These Esters had different pleasant smells that we then evaluated. In the second part of the experiment‚ we broke the ester bonds of a triglyceride in order to form glycerol and carboxylate salts. This process is known as Saponification because it produces amphiphilic molecules that allow soap to remove dirt from the surface
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LAB REPORT ANDREW O. BAAFI Organic Chemistry I Lab. Instructor: Dr. Strange 09-24-01 TITLE: Preparation of Isopentyl Acetate (isoamyl acetate) / Gas Chromatography (Esterification). REFERENCE: Fischer‚ W. H.‚ A. G. Craig. “Microscale Esterification of Peptides and Analysis by MALDI-MS.” http://www.salk.edu/LABS/pbl/brukeran1.htm. 10-02-2001 Mayo‚ Dana W‚ Pike Ronald M‚ Trumper Peter K. Microscale Organic Laboratory. 3rd ed. New York: Wiley & Sons‚ 1994. Strange De Soria‚ Louise. Chemistry
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Flavor) Paul Symon C. Manuel*‚ Katherine Merene‚ Charlene Mondelo‚ and Pamela Mallari Department of Chemistry‚ University of Santo Tomas‚ Manila‚ Philippines Abstract: The purpose of this experiment was to synthesize isoamyl acetate via an esterification reaction between acetic acid and isoamyl alcohol‚ using concentrated sulfuric acid as a catalyst. The product was washed with sodium hydrogen carbonate‚ as well as with water‚ and then dried with anhydrous sodium sulfate. The percent yield of
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Synthesis of Banana Flavor via Fischer Esterification Patricia Faye R. Agnila‚ Joan Karla M. Alvaran*‚ Micaela Isabel N. Arellano‚ and Denzel Nicho T. Armendares Department of Biological Science‚ College of Science‚ University of Santo Tomas‚ Manila‚ Philippines Abstract This experiment is conducted to exhibit the synthesis of banana
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Abstract Fisher Reaction is a special type of esterification that uses an acid catalyst to reflux Carboxylic acid and Alcohol. The product Ester is in equilibrium to the reactants acid and alcohol. Ester is responsible for the smell and aroma of different fruits. After using the Fisher reaction‚ a combination of techniques is used to separate the product. Introduction Esters are naturally occurring compounds that possess a distinctive odor. It is responsible for the smell of different fruits
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Synthesis of Isopentyl Acetate Abstract Isopentyl acetate was synthesized via a Fischer Esterification and purified via simple distillation. The yield was determined to be 25%. The identity and purity of the product was confirmed by comparison of the measured ultra-micro boiling point (140°C) to the published value (142°C).1 Chemical Equation Procedure Isopentyl alcohol (0.787 g‚ 1.2 mL‚ 8.93 mmol)‚ acetic acid (1.574 g‚ 1.5 mL‚ 26.20 mmol)‚ and sulfuric acid (0.368
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an alkyl halide. Fischer Esterification is a nucleophilic acyl substitution reaction that converts a carboxylic acid into an ester when the carboxyl group of an acid and the hydroxyl group of an alcohol are condensed with the expulsion of a water molecule. The by product is removed to exploit Le Chatelier’s principle in order to favor the formation of the ester over the starting material. Fig. 1: Esterification of Isopentyl Acetate Fig. 2: Mechanism for the esterification of Isopentyl Acetate
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UNIVERSITI TEKNOLOGI MARA COURSE INFORMATION Confidential Code Course Level Credit Hours Contact Hours : : : : : CHM 556 Organic Chemistry II Degree 4 3 hr (Lecture) 3 hr (Practical) 3 Core CHM 456 Part Course Status Pre-requisite : : : Course Outcomes : Upon completion of this course‚ students should be able to: 1. Determine functional groups present in organic compounds using Infrared Spectroscopy and interpret Nuclear Magnetic Resonance spectra and relate the information to structural
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