Name: Bill Marano Due Date: 4-1-13 Experiment Title: TLC Analysis of Analgesic Drugs Purpose: The purpose of this experiment is to identify the brand name of an unknown commercial analgesic product by TLC analysis. Unknown #1 solution was run against standard solutions of individual analgesics. The components of the unknown product were identified by comparing characteristic traits‚ such as Rf‚ fluorescence and iodine staining‚ to those exhibited by the standards. The name of the commercial product
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Maryssa Buffano Miss Arnold Science – Current Astronomer Essay 4/12/2011 JMJ Dr. Debra Fischer – Astronomer An astronomer is an astrophysicist who studies stars‚ planets and galaxies. Astronomers use the laws of physics to investigate the matter and energy of celestial bodies. They then apply the research findings to solve space navigation and communication problems and even discover new planets and stars. In 1512‚ Copernicus theorized that the planets orbit the sun and the race
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January 24‚ 2013 TLC Analysis of Analgesic Drugs Introduction: The purpose of this lab was to determine the composition of four different over-the-counter drugs (Anacin‚ Bufferin‚ Excedrin‚ and Tylenol). These compositions were determined by using the method of thin-layer chromatography (TLC) of the four over-the-counter drugs‚ which were then compared to four different components of drugs (acetaminophen‚ aspirin‚ caffeine‚ and salicylamide). Experiment Scheme1:
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Figure 1: Formation of benzocaine from p-aminobenzoic acid Experimental P-aminobenzoic acid (1.211g) and absolute ethanol (15mls) were combined with three boiling chips in a 50ml round bottom flask. The round bottom flask was placed on a heating plate and was refluxed starting at 109 ̊C. The solution began boiling at 111 ̊C. It was allowed to reflux for approximately 30 minutes and the solid was dissolved. The round bottom flask was then placed in an ice bath and allowed to cool to
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TLC TLC were one of the biggest-selling female R&B groups of all time‚ riding a blend of pop‚ hip-hop‚ and urban soul to superstardom during the ’90s. Tionne "T-Boz" Watkins‚ rapper Lisa "Left Eye" Lopes‚ and Rozonda "Chilli" Thomas managed to question justly to pop and R&B audiences‚ fuse popular hooks and playful alarm with a fresh‚ inviting attitude.first‚ their image was equal parts style and spirit‚ help
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Experiment #5: Esterification of Methyl Benzoate from Benzoic Acid October 28‚ 2010 Abstract: This experiment was conducted to synthesize methyl benzoate from benzoic acid and methanol by using the Fischer esterification method. Methanol (12.5ml) and Benzoic acid (4.9 grams) are heated together in the presence of concentrated sulfuric acid (1.5ml) until equilibrium is achieved. A reflux apparatus is set up for 1 hour to carry out the reaction at the boiling point of the solvent (Methanol
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decreasing polarity (this can be done according to structure of the individual solvents and % composition of the mixtures). Also rank the 3 compounds in order of decreasing polarity (this compound ranking can be based on structure as well as on these TLC results). Explain each of your rankings. Compounds: 9-fluorenone‚ 9-fluorenol. Fluorene Solvent: Ethyl acetate 10% in hexane‚ Ethyl acetate 25% in hexane‚ 100% hexane Polarity of each compound reacted differently to each of the solvents used
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Abstract: In this lab‚ the chemical components of Excedrin and Tylenol‚ two common‚ over-the-counter analgesic drugs‚ were determined by utilizing the technique of thin-layer chromatography‚ or TLC. The active ingredients of Excedrin were caffeine‚ acetaminophen‚ and aspirin with Rf values of 0.11‚ 0.38‚ and 0.61‚ respectively. The lone active ingredient of Tylenol was acetaminophen with an Rf value of 0.39. The elution sequence obtained in the experiment is as follows: ibuprofen (least polar)
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GROUP 2 Kinetics of De-esterification for Synthesis of Benzoic Acid BATCH REACTOR Shane Bulk Chris Crosley David McGuire Max Skula Yunjing Song Shriram Sundarraj Nelson Zhou 155:416 Process Laboratory II Professor Jerry Sheinbeim January 28 – February 28‚ 2014 ABSTRACT The observed reaction that took place in this experiment was the de-esterification of ethyl benzoate to form benzoic acid. This experiment was used to determine the rate constant k of the synthesis of benzoic
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Dyes by TLC Pre-lab Properties: Ethyl acetate‚ ethanol‚ silica‚ azobenzene‚ azulene‚ 4-(p-nitrophenylazo) resorcinol‚ methyl red‚ bromocresol green (solubilities in water and ethanol) Purpose: To identify compounds from an unknown mixture using TLC Up to 100% of missed points can be recovered from this lab Watch the video: http://www.youtube.com/watch?v=e99nsCAsJrw (MIT) TLC plates are near the main hood DO NOT BREAK CAPILLARY TUBES Keep spots small and concentrated (video) Stop TLC before solvent
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