and Potentiometric Determination of its Purity and Dissociation Constant ------------------------------------------------- Abstract The purpose of the study is to synthesize salicylic acid from the ester‚ methyl salicylate‚ and determine the acid’s dissociation constant and purity. The ester was converted to salicylic acid by base hydrolysis. The products were refluxed and recrystallized‚ to ensure maximum purity‚ and filtered‚ dried‚ and weighed. The melting point of the product was determined using
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Date Performed: September 9 ‚2011 SPECTROPHOTOMETRIC DETERMINATION OF THE ACID DISSOCIATION CONSTANT OF METHYL RED M.C. Caligagan ‚M.N.Q. Tolentino and M.Q. Clores Institute of Chemistry‚ College of Science University of the Philippines‚ Diliman‚ Quezon City‚ Philippines Received :September 21‚2011 ABSTRACT This experiment aims to determine the acid dissociation constant value of Methyl Red by means of spectrophotometry. Ten samples were spectrophotometrically analyzed under a UV-Vis
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! ! ! ! ! ! ! Determining the solubility of Sodium hydroxide ! ! ! ! ! ! ! ! ! ! ! ! Yunha Kim! Gyeonggi Suwon International School ! IB DP Chemistry SL! Research Question! How is the solubility of sodium hydroxide (NaOH) in water affected by temperature? ! ! Introduction ! Sodium hydroxide is categorised as metal halide salt‚ composed of sodium and chlorine.! The ions present in the solid crystals of potassium chloride dissolve and gain mobility in water
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TITLE: Solubility and Thermodynamics PURPOSE: The purpose of the lab was to determine the thermodynamics variables of ∆H‚ ∆S‚ and ∆G for the dissolution reaction of potassium nitrate in water. The solubility of potassium nitrate in mol/L was measured over a range of various temperatures by finding out at what temperature crystallization began for solutions of different molarities. Then‚ the equilibrium constant was calculated and a graphical relationship between the natural logarithm of the
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wont dissolve. Solubility of a solute = mass of a solid required to a saturate 100g of water at a particular temperature. Calculating Solubility 2g potassium chlorate dissolves in 20g water at 28oC what is its solubility? 2 x 100/20 = 10.0g potassium chlorate/100g water 4g potassium sulphate dissloves in 30g water at 50oC what is its solubilty? 4 x 100/30 = 13.33g potassium sulphate/100g water 30g sodium chloride dissolves in 75g water at 10oC what is its solubility? 30 x 100/75
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excess amount of each solvent. For the second part of the experiment‚ approximately 25 mL of distilled water was combined with 1 g of salicylic acid and it took 6 mL of water to dissolve the sample at the boiling point. When it was crystallized‚ the product was almost white to colourless and it formed needle-like crystalline structure. DISCUSSION The effect of polarity on interactions between the molecules was the focus of the first experiment. For the compounds which dissolved in the solvents used
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354-355 Experiment 2 SOLUBILITY 1. Part A. Solubility of Solid Compounds. Use your observations to complete the following table‚ rating each system as soluble‚ insoluble‚ or partially soluble. Organic Compound Benzophenone Water Methyl Alcohol Hexane Malonic acid Biphenyl 2. Considering the polarities of the compound and the solvent and the potential for hydrogen bonding‚ answer the following: a) There should be a difference in your results between the solubilities of biphenyl and benzophenone
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n this lab experiment factors that affected solubility are temperature‚ liquids‚ concentration‚ pressure‚ polarity‚ and molecule. In this experiment we use temperature‚ centrifuge‚ and concentration solutions to be able to achieve the results that we wanted. Step one of the experiment was to mix HCl‚ to cause a precipitation form‚ after that we had to decant the solution‚ then we used a centrifuged to separate the the precipitate of the supernatant liquid. After the decant was done‚ then the process
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1. Provide a general discussion of the solubility/miscibility behavior observed in procedure A-D. For part A of the procedure we worked with the solubility of solid compounds in various solvents. The three solid compounds that were worked with during this procedure were benzophenone‚ malonic acid‚ and biphenyl. These three solids were then mixed with water (highly polar)‚ methyl alcohol (intermediately polar)‚ and hexanes (nonpolar). When benzophenone is mixed with water the results turned out to
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However‚ for a metal ion indicator to be suitable in n EDTA titration‚ it must not bind as strongly with metal ions as EDTA does. Murexide is therefore suitable. AIM The aim of this experiment is to determine the percentage of nickel in a nickel(II) salt using EDTA. METHOD The following apparatus was collected: 50cmᶟ burette ●Glass stirring rod 20cmᶟ pipette ●Hydrated nickel(II) sulphate (NiSO₄.6H₂O) 100cmᶟ standard flask ●Standardised 0.10moll⁻¹ EDTA solution 250cmᶟ conical flask ●1 moll⁻¹ ammonium
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