Infrared Spectroscopy Organic Chemistry Lab 301A B. The purpose of this lab is to study Infrared Spectroscopy‚ which focuses on the study of the electromagnetic spectrum. The area to be studied is the infrared region‚ which is made up of gamma‚ X‚ and UV rays. We want to be able to identify spectra’s to their complementary structures. The background of this experiment particularly deals with the study of compound structure determination‚ and traits. We must be aware of the functional groups
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Technical Paper WFGD Case Study -- Maximizing SO2 Removal by Retrofit with Dual Tray Technology A.A. Silva and P.J. Williams The Babcock & Wilcox Company Barberton‚ Ohio‚ U.S.A. J. Balbo Michigan South Central Power Agency Litchfield‚ Michigan‚ U.S.A. Presented to: EPRI-DOE-EPA-AWMA Combined Power Plant Air Pollutant Control Mega Symposium August 28-31‚ 2006 Baltimore‚ Maryland‚ U.S.A. 6 The Babcock & Wilcox Company BR-1785 WFGD Case Study - Maximizing SO2 Removal
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CH 202 Breakdown UV/Vis: Molecules containing π-electrons or non-bonding electrons (n-electrons) can absorb the energy in the form of ultraviolet or visible light to excite these electrons to higher anti-bonding molecular orbitals. The more easily excited the electrons (i.e. lower energy gap between the HOMO and the LUMO)‚ the longer the wavelength of light it can absorb. Conjugation raises the energy of the bonding orbitals and lowers the energy of the antibonding molecular orbital. This
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Introduction Objectives Validate the Beer-Lambert law for KMnO4. To determine the pKa for an acid-base indicator To estimate the equilibrium constant for the formation of complex ion Fe(NSC)²ꭞ The function of part two of the experiment is to find the value of the constant K‚ in the following equilibrium constant: K=[Fe (NSC) ²⁺]/ [Feᶟ⁺] [NCS⁻]‚ while not disrupting the equilibrium. Theory For part one. The majority of chemical compounds are known to absorb UV or visible light. Depending
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Callam 1/8 CHEM – 254 – WI -2009 Problem Set #1 – IR Spectroscopy - KEY 1. Which of the indicated bonds absorbs at the higher frequency in an IR spectrum? a. O or OH C=O > C-O b. N or NH C=N > C-N c. H or H C-H sp2 > C-H sp3 Callam 2/8 CHEM – 254 – WI -2009 2. What major IR absorptions are present above 1500 cm-1 for each compound? a. b. O sp3 C-H stretch 2950 C=O - ketone 1715 cm-1 cm-1 c. O sp3 C-H stretch 2950 cm-1 sp3 C-H stretch 2950 cm-1
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Introduction: This investigation used spectroscopy to evaluate light absorption in different solutions. A spectrophotometer was used in the lab to determine these values. A spectrophotometer is an apparatus used to “measure the absorption of radiation in the visible and UV regions of the spectrum and allows precise at a particular wave length” (Jones et al.‚ 2007). The amount of light absorbed by a substance is directly in relation to the concentration of the solute and also the wavelength moving
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Introduction At any particular wavelength the absorption of light when visible light passes through a solution depends on two factors: * The length of the light path * The concentration of the colored path The connection of these two variables is known as the Beer-Lambert Law: Absorbance (A) = ε c l Where ε is the absorption coefficient C is the concentration of the compound And l is the length of light usually 1cm When I is constant‚ this proves a linear relationship between
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Electron Spin Nuclear Magnetic Resonance (NMR) Spectroscopy Organic Chemistry BCH3015 • Electron spin is quantized. • The spin quantum number ms has only two allowed values: ms = +½ or –½ • The two directions of spin create oppositely spin create oppositely directed magnetic fields. fields. 61 Proton Spin Organic Chemistry BCH3015 62 Nuclear Spin States • A proton (the nucleus of a 1H atom) also possesses spin. For each nucleus having the spin quantum number
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Mass Spectroscopy Mass spectroscopy is a method used in science and industry in order to obtain the masses and relative concentrations of atoms and molecules and to detect isotopes in a sample based on their masses. In order to do this the method requires an instrument called the ‘mass spectrometer’‚ of which‚ is able extract accurate information of the relative masses of isotopes and their relative abundance. This makes the mass spectrometer very useful for applications such as carbon dating
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Contents Series Preface Preface Acronyms‚ Abbreviations and Symbols About the Author 1 Introduction Electromagnetic Radiation Infrared Absorptions Normal Modes of Vibration Complicating Factors 1.4.1 Overtone and Combination Bands 1.4.2 Fermi Resonance 1.4.3 Coupling 1.4.4 Vibration–Rotation Bands References 2 Experimental Methods 2.1 Introduction 2.2 Dispersive Infrared Spectrometers 2.3 Fourier-Transform Infrared Spectrometers 2.3.1 Michelson Interferometers 2.3.2 Sources and Detectors 2.3.3
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