Katie Smith April 11‚ 2013 Competitive Nucleophiles Introduction The purpose of this experiment was to compare the nucleophilicities of chloride and bromide ions toward the n-butyl and t-pentyl alcohols. We were able to analyze this by using refractometry to measure the amounts of alkyl chloride and alkyl bromide in each reaction. Experiment Scheme (Procedure A) To begin the experiment‚ we assembled a reflux apparatus in the fume hood with a 100 mL round bottom flask and a condenser
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Procedure: Oxone reaction Dissolve 0.40 g oxone ® in 2.0 mL of water by shaking vigorously in a sealed vial. (Caution! Be sure the vial is sealed because oxone is a strong oxidizer.) Dissolve 50 L of cyclohexene in 2.0 mL of acetone in a small Erlenmeyer flask. Cool the cyclohexene solution in an icebath‚ then add the oxone solution dropwise over 5 minutes with swirling in the icebath. Remove the Erlenmeyer flask from the icebath and allow the reaction to sit for 15-30 minutes. (To save
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Place 1 ml of sample A (cyclohexane) into a test tube containing 4 mls of the potassium permanganate solution. Record observations of any reaction. 3. Place 1 ml of sample B (cyclohexene) into a test tube containing 4 mls of the bromine water solution. Record observations of any reaction. 4. Place 1 ml of sample B (cyclohexene) into a test tube containing 4 mls of the potassium permanganate solution. Record observations of any reaction. RESULTS Sample Reaction with br2 water Reaction with acidified
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Diels-Alder is also called a [4+2] cycloaddition because a ring is formed by the interaction of four pi electrons of the alkene with two pi electrons of the alkene or alkyne. The product of the Diels-Alder reaction is usually a structure that contains a cyclohexene ring system. The mechanism of the reaction involves a cyclic flow of electrons in a single step in which the diene‚ supplies 4 π electrons and the alkene or alkyne‚ also called the dienophile‚ supplies 2 π electrons. In this process‚ two new
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bromine solution is added then the reaction would not be able to run to completion and bromine would be the limiting reagent causing less final product. (c) If cyclohexane was used then it would not react with the bromide nearly as much as the cyclohexene and there would be a larger amount of bromide in the final
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Lab 22: 4-Methylcyclohexene Abstract: We treated 4-methylcyclohexanol with phosphoric acid‚ and after purification we produced the end product 4-methylcyclohexene. We determined we had a pure product based on the results of the tests with Br2 and KMnO4‚ as well as the IR absorbtion spectrum of the final product. Purpose: The purpose of this experiment is to obtain pure 4-methylcyclohexene by reacting 4-methylcyclohexanol and phosphoric acid. Through distillation
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REACTIONS OF HYDROCARBONS Vanessa P. Manibpel De La Salle University - Dasmariñas ABSTRACT Five substances namely Hexane‚ Eugenol‚ Unknown hydrocarbon 1‚ Unknown hydrocarbon 2‚ and Acetylene gas was used for the selective reactivity of hydrocarbons to functional group tests; Bayer’s test‚ Bromine test light‚ Bromine test dark‚ and Tollen’s test. In Bayer’s test‚ only Acetylene‚ Eugenol and Unknown hydrocarbon 2 reacted positively and the rest retain the purplish color of KMnO4. On the other hand
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Analysis of Hydrocarbons Myra Gurango‚ Geneva Guy‚ Micah Hernandez* and Joyce Lagarde Department of Chemistry‚ University of Santo Tomas‚ Manila‚ Philippines Abstract The organic compounds hexane‚ toluene‚ cyclohexene and naphthalene in hexene were subjected to parallel chemical testing to differentiate their intrinsic physical properties in terms of structure and behavior. The physical state and color were noted by simple physical observation. Nitration Testing was conducted for preliminary
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attachment of an OH to the ring; the ether group is oxygen bonded to two R groups on either side of it. THC contains 20 sigma bonds and four pi bonds. Three rings are present as well‚ two cyclohexene rings and one benzene ring. Attached to the first cyclohexene ring is one methyl group. On the second cyclohexene ring‚ two methyl groups are present as well as the ether group. On the benzene ring‚ the hydroxyl group is the substituent‚ and a pentane chain is attached to the ring as well. THC contains
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Keghan Chapter 8 MULTIPLE CHOICE QUESTIONS Topic: Structure Elucidation 1. An alkene adds hydrogen in the presence of a catalyst to give 3‚4-dimethylhexane. Ozonolysis of the alkene followed by treatment with zinc and acetic acid gives a single organic product. The structure of the alkene is: CH3 A) CH3CH=C-CHCH2CH3 (cis or trans) CH3 CH3 B) CH3CH2C=CCH3 (cis or trans) CH2CH3 C) CH3 CH2=CCH2CHCH2CH3 CH3 CH2 D) CH3CH2CCHCH2CH3 CH3 CH3 E) CH3CH2CHCHCH=CH2
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