Determination of Manganese in Steel Submitted by: ------------------- Date of Submission: 27.03.11 Objectives: In steel production aside the iron‚ which is the primary source‚ some amounts of manganese is used together with carbon. The objective of this experiment is determining the manganese amount in the steel compound by using UNICAM UV-VIS Spectrometer. Theory: Many molecules absorb ultraviolet or visible light. The absorbance of a solution increases
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Figure 1: Schematic illustration of the principle of Biacore SPR to measure the interaction between analyte molecules in the flow with immobilized receptor binding sites on the surface. A) SPR uses an optical method to measure changes in the refractive index near the surface of a thin gold film on a glass slide. At a critical angle of incident light on the surface-solution interface an electromagnetic field or evanescent wave is generated. This is detected as absorption of light and a decrease in
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Qualitative Analysis Lab Report Organic Chemistry Laboratory II ABSTRACT: The purpose of this lab was to separate and purify two unknown compounds‚ one solid and one liquid‚ from an ethereal solution using the techniques of chemically active extraction‚ vacuum filtration‚ simple distillation‚ and recrystallization. Then identifying information was compiled about these unknowns by obtaining experimental melting/boiling point ranges‚ and analyzing IR and proton/carbon NMR spectrums It was determined
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Substitution Reactions of Molybdenum Hexacarbonyl and the Use of Infrared Spectroscopy as a Structural Tool 01-09-2011 Abstract A variety of metal carbonyl derivatives can be synthesized by substitution reactions. In this experiment two geometric [Mo(CO)4(PPh3)2] isomers A and B were synthesized and their molecular geometries were determined by means of infrared spectroscopy. Isomer A was synthesized first by reacting [Mo(CO)6] with sodium borohydride employed as a reducing agent and triphenylphosphine
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Computer Lab Rules & Regulations Electronic workstations may only be used by current Swinburne University students and staffs. Swinburne identity card must be presented on request. Swinburne computing facilities should only be used for educational‚ research and administrative purposes of Swinburne. All other uses are strictly prohibited. The following rules and terms apply to all computers on campus. Terms and Conditions 1. All users must abide by the license requirements of any software
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FEASIBILITY STUDY FOR COMPUTERIZED AUTOMATION OF EPA REGIOTCfl TECHNICAL SUPPORT BRANCH ^Fred B. Stephens‚’William F. Morris‚ 7 George W. Barton‚ Jr.‚ and Eugene R. Fisher February 9‚ 1978 Work performed under ths auspices of the U.S. Department of Energy by the UCLLL under contract number W-7Jo5-ENG-48. INHLAWREISiCE I U 5 UVERMORE I S LABORATORY ^^OPTal-DOCDMSOT-B «nica3Sl> Distribution Category UC-11 LAWRENCE LIVERMORE LABORATORY University of CakfaTiia/Livetmore‚ CaHfomie^/94550
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XRD – X-Ray Diffraction X-ray diffraction (XRD) is a powerful non-destructive technique for characterizing crystalline materials. It provides information on structures‚ phases‚ preferred crystal orientations (texture)‚ and other structural parameters‚ such as average grain size‚ crystallinity‚ strain‚ and crystal defects. X-ray diffraction peaks are produced by constructive interference of a monochromatic beam of X-rays scattered at specific angles from each set of lattice planes in a sample. The
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ABSTRACT: Silver nanoparticles are nanoparticles of silver which are in the range of 1 and 100 nm in size. Silver nanoparticles have unique properties which help in molecular diagnostics‚ in therapies‚ as well as in devices that are used in several medical procedures. The major methods used for silver nanoparticle synthesis are the physical and chemical methods. The problem with the chemical and physical methods is that the synthesis is expensive and can also have toxic substances absorbed onto
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Title: Competing Nucleophiles (Exp 24‚ pp 211-221‚ pp 808-823‚ pp 836-842) Purpose: The purpose of this experiment is to determine the nucleophilic strength of chloride and bromide ions as it reacts with 1-butanol (n-butyl) and 2-methyl-2-propanol (t-butyl alcohol) under SN1 and SN2 conditions. Method: 40 g of ice and approximately 30 ml of sulfuric acid is cautiously added to a 100 mL beaker respectively. Weigh 7.6 g of ammonium chloride and 14.0 g of ammonium bromide and place it in
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Quartz-type FePO4 was investigated from 294 up to 1073K by neutron powder diffraction. The cell parameters and fractional atomic coordinates in the α phase tend towards the values found in the β phase. The first order transition of FePO4 is at 980 K‚ during which several observations are made. Firstly‚ the cell parameters and fractional atomic coordinates show discontinuous shifts. Secondly‚ the intensities of a large number of diffraction lines decrease‚ as shown in Fig. 1. Lastly‚ bond distances
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