X-ray Absorption Spectroscopy X-ray absorption spectroscopy (XAS) techniques probe short- and medium-range order‚ yielding information on bond lengths‚ coordination numbers‚ local coordination geometry and the oxidation state of atoms for a wide range of solid and liquid systems. XAS experiments require an intense‚ tunable photon source only available at synchrotrons. Features • medium and high energy (from atomic number Z=20 upwards) XAS‚ XANES (x-ray absorption near-edge structure)
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Lab Report Preparation Guidelines—IR Spectroscopy‚ General Unknowns‚ CH 315. Introduction/Purpose State in simple terms what the purpose was. Since one is issued a vial of an unknown substance‚ the “purpose” as such is not exactly in doubt. The object is simply to state that obvious purpose‚ as well as summarize (a comma-ed list here is fine) the various means‚ tests‚ so forth that are performed in the approximate order that they are performed. (approximately 10 points) Experimental
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Introduction Fluorescence is a type of photoluminescence spectroscopy. Fluorescence occurs when a photon is emitted from a molecule as it moves from a higher excited state to a lower excited state with in the same spin. A molecule normally is in its ground state energy. When a light source puts off an electromagnetic energy‚ the molecule can move to a higher more excited energy. When the molecule transitions down in energy‚ it usually is released as heat. Conversely‚ if the molecule is subject to
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~ 10 cm-1. It can be divided into near-infrared region (12800 ~ 4000 cm-1)‚ mid-infrared region (4000 ~ 200 cm-1) and far-infrared region (50 ~ 1000 cm-1). scientists have established various ways to utilize infrared light. Infrared absorption spectroscopy is the method which scientists use to determine the structures of molecules with the molecules’ characteristic absorption of infrared radiation. Infrared spectrum is molecular vibrational spectrum. When exposed to infrared radiation‚ sample molecules
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Background The scientific concepts involved in this lab include Spectroscopy‚ Beer’s law‚ Calibration curve‚ concentration‚ and electronic transitions. The main objective of this experiment is to see how the percent composition of brass can be determined to verify the properties influenced by copper and zinc. Brass is a generic term for alloys of copper and zinc. The main technique used in this experiment is Spectroscopy. The three equations used in this lab are: Y = mx + b‚ where y = absorbance‚ x = concentration
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Lab 2: Infra-Red (IR) - Nuclear Magnetic Resonance (NMR) Exercises In Molecular Spectroscopy - Structural Determination Organic Chemistry II CHEM 2425 Manrique October 30‚ 2012 Alex Wolf Introduction For the purposes of this lab‚ the chemical formula will be given‚ and the degrees of unsaturation can be calculate from the formula (2C+2)-(H+Hal-N)/2. The degrees of unsaturation will give clues as to the structure. A double bond‚ as well as a ring will have one degree of unsaturation each
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31 October 2012 Atomic Emission Spectra Lab Atomic spectroscopy is the determination of elemental composition by its electromagnetic or mass spectrum. An arrangement of all wavelengths of electromagnetic radiation is called the spectrum; the plural being spectra. As light passes through a prism‚ the frequencies of light emitted by an element separate into separate lines to give the atomic emission spectrum of the element. There are two spectrums in the lab: the incandescent and fluorescent. An incandescent
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using spectroscopy and graphical analysis. We will be using beers law to find the unknown concentration of dye in a sports drink. Materials: Beakers‚ 50-mL‚ 2-3 ; Test tubes (13 x 100)mm 3-8 ; FD&C Blue 1 stock solution‚ 50-mL ; Lens tissues ; Pipets‚ serological‚ 10-mL ; Sample of consumer sports drink‚ 10-mL ; Spectrophotometer ; Test tube rack Procedure: 1) Preeminently‚ follow all laboratory safety guidelines ensuring that you have safety goggles on at all times throughout the lab. 2) Fill
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Emission Spectroscopy Lab Introduction: According to the Bohr atomic model‚ electrons orbit the nucleus in fixed paths with specific energies. Each path is therefore often referred to as an “energy level”. Electrons possessing the lowest energy are found in the levels closest to the nucleus. Electrons of higher energy are located in progressively more distant energy levels. If an electron absorbs sufficient energy to bridge the “gap” between energy levels‚ the electron may jump to a higher
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Flame Test Laboratory Report Introduction The purpose of this lab is to observe and identify metallic ions‚ using flame tests. The traditional flame test originated when Robert Bunsen invented the Bunsen burner to test two new alkali metals he and his partner had discovered. “A flame test is an analytic procedure used in chemistry to detect the presence of certain elements‚ primarily metal ions‚ based on each element’s characteristic emission spectrum” (Flame Test 1). Using this test‚ an element
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