Classification Tests for Carboxylic Acid and Derivatives Mary Catherine Sarte‚ John Emmanuel Sy‚ Allurie Umel‚Franklin Yap‚ Mary Christine YouIntroduction Carboxylic acids derivatives are simply groupsof compounds that contain a carbonyl group butwith an electronegative atom attached to thecarbon. The difference in the structure leads to amajor change in reactivity. The reactions of thesegroups of compounds involve nucleophilicsubstitution. Although there are abundant kindsof carboxylic acid derivatives‚ the
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Synthesis of Phenols You can prepare phenols in large quantities by the pyrolysis of the sodium salt of benzene sulfonic acid‚ by the Dow process‚ and by the air oxidation of cumene. Each of these processes is described below. You can also prepare small amounts of phenol by the peroxide oxidation of phenylboronic acid and the hydrolysis of diazonium salts. Pyrolysis of sodium benzene sulfonate In this process‚ benzene sulfonic acid is reacted with aqueous sodium hydroxide. The resulting salt
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alkoxide or phenoxide ion. Gives best results when 1o alkyl halides are used. Mechanism is SN2. Alkoxides may be prepared by reacting an alcohol with NaH or by reacting an alcohol with Na metal. Phenoxides may be prepared by reaction of phenols with NaOH ROH + NaH ROH + Na ArOH + NaOH RO Na - - + + H2 RO Na + + 1/2 H2 + ArO Na - + H2O When 3o alkyl halides are reacted with alkoxide or phenoxide ions‚ elimination is the major reaction‚ not substitution
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which reinforce the theory and concepts studied in Organic Chemistry 1 (CHM456). It covers the learning of simple laboratory techniques such as reflux‚ distillation‚ extraction‚ crystallization and melting point determination‚ preparations of organic compound and separation of mixtures. The Techniques Students are REQUIRED to read and understand the various techniques that will be covered in the laboratory sessions from the textbook. | Techniques | Page | 1 | Laboratory Safety | 6 | 2 | Laboratory
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Properties of Alcohols and Phenols Experiment #3 Objectives: To observe the solubility of alcohols relative to their chemical structure‚ to perform chemical tests to distinguish primary‚ secondary and tertiary alcohols‚ and a color test for phenol. Introduction The general formula of an alcohol is ROH in which the R is an aliphatic hydrocarbon group. Alcohols may be looked upon as derivatives of water‚ HOH. One hydrogen of water is substituted by an alkyl group‚ R. Like water‚ alcohols show hydrogen
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Experiment #1: Separation of Acid‚ Base‚ and Neutral Compounds from a Solid Mixture by Liquid-Liquid Extraction Introduction Liquid-liquid extraction is a technique used to separate chemical substances in order to purify or identify the various components of a mixture. Flavors‚ spices‚ perfumes‚ and medicines are just some of the everyday things that are extracted from plants and other natural sources [1]. The basic principle used to carry out this separation is the mixing of two liquids that are
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Phenol‚ also known as carbolic acid‚ is an aromatic organic compound with the molecular formula C6H5OH. It is a white crystalline solid that is volatile. The molecule consists of a phenyl group (-C6H5) bonded to a hydroxyl group (-OH). It is mildly acidic‚ but requires careful handling due to its propensity to cause chemical burns. Phenol was first extracted from coal tar‚ but today is produced on a large scale (about 7 billion kg/year) from petroleum. It is an important industrial commodity as a
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Total Carbohydrates Using the Phenol-Sulfuric Acid Method This lab introduced the students to analyzing carbohydrate content using a spectrophotometer and phenol-sulfuric acid methods. Virginia Smith 983976633 Lab Partner: Jeff Martz Due Date: 3-22-11 Introduction The objective of this lab was to have students use a spectrophotometer to analyze the carbohydrate content in the sample. Phenol-sulfuric acid methods were also applied to
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Experiment #8 – properties of Alcohols and Phenols Introduction As has been mentioned before‚ over 20 million organic compounds have been identified. If each substance had to be studied as an entity completely separate from all the other substances‚ the study of organic chemistry as a whole would be impossible; that is to say‚ even more impossible than you currently believe it to be. Fortunately‚ the subject can be organized and it is often organized around the concept of the functional group
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The purpose of the first part of the experiment was to produce a chemical compound which was the alum crystals by using aluminum‚ potassium hydroxide and sulfuric acid. After the compound was present‚ the purpose of the second part of the experiment was to make sure that the compound that was formed in the first half of the experiment was actually alum. Some of the experimental techniques that were used in this experiment was filtration using the Büchner funnel vacuum filtration‚ recrystallization
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