– Separating Sand & Salt Purpose: The purpose of this experiment is to separate a mixture of sand and salt. Materials: Small beaker Electric balance Sand Salt Water Graduated cylinder Stirring rod Filter paper Flask Rubber policeman Wash bottle Funnel Bunsen burner complete with rubber tubing and a source of gas Hot hands Insulator pad Ring stand complete with a ring Wire gauze Striker Pre-lab Questions: 1. Water will be useful in separating the salt and sand because salt is soluble in water‚
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Lab 5 n-Butyl Bromide Preparation Introduction: The purpose of this lab is to properly extract and distill n-butyl bromide It is ideal to perform this technique with accuracy‚ which can be measured by the percent yield. Chemicals: n-Butyl Bromide- clear‚ yellow liquid that is slightly soluble in water. Molar weight of 137.02g and has zero reactivity. Sodium Bromide- white‚ crystals‚ granules. Soluble in water with no reactivity. Molar weight of 102.89g. Sulfuric Acid- colorless liquid
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Benning Introduction The purpose of the coordination complex lab is to determine the absorbance spectra of complexes based on their color. Every complex has its own color which results from the wavelengths of white light it reflects. The complexes will be compared by the color each reflects and by the energy of the waves each absorbs. The purity of the synthesized complex will also be found. Procedure Part I: Preparation of the Complex A sample of copper sulfate pentahydrate (6.285g) was
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Preparation of Esters Introduction Esters are known for their pleasant smells such as perfumes and artificial flavorings in contained labs. They are formed when a carboxylic acid reacts with alcohol and a strong acid such as a catalyst called sulfuric acid (H2SO4) for this lab. The structural formula for esters can be represented as R-COO-R’. The R and R’ symbolizes different alkyl groups that can be combined to the ester. When naming an ester the first part comes from the alcohol followed
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Let’s Make Salt Purpose: Could NaCl be made using NaHCO3‚ hydrochloric acid‚ and a boiling chip? Hypothesis: If I combined NaHCO3‚ hydrochloric acid‚ and a boiling chip I think it will form NaCl because when you balance the equation it makes a new chemical reaction. Materials needed: test tube cleaner‚ test tube‚ test tube tongs‚ hot plate‚ a scale‚ graduated cylinder‚ water‚ goggles‚ fire retardant glove‚ beaker‚ test tube holder‚ a scoopula‚ hydrochloric acid‚ sodium bicarbonate‚ soap‚ pipette
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Alkylbenzene (LAB) Complex Petrochemical Petrochemical Introduction Linear alkylbenzene (LAB) is the most common raw material in the manufacture of biodegradable household detergents. LAB is produced using normal paraffins as a raw material. Normal paraffins are derived from straight run kerosene. UOP offers processes‚ catalysts‚ adsorbents and equipment for the production of LAB from kerosene or normal paraffins. The processes can be utilized in combination in a new complex or retrofitted
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Potentiometric Titrations Accuracy The accuracy of a potentiometric analysis is limited by the measurement error for the cell’s potential. Several factors contribute to this measurement error‚ including the contribution to the potential from interfering ions‚ the finite current drawn through the cell while measuring the potential‚ differences in the analyte’s activity coefficient in the sample and standard solutions‚ and liquid junction potentials. Errors in accuracy due to interfering ions
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Experiments 4A-C: Synthesis and Component Analysis of an Iron (III) Oxalate Complex My Name TA‚ Section B## Work Performed on 10/23‚ 10/30‚ & 11/4‚ 200# Report due Tuesday‚ November ##‚ 200# 1. Abstract This experiment initially involved the synthesis of an iron (III) oxalate complex with the general formula Kw[Fex(C2O4)y]·zH2O. The variables x‚ y‚ and z were determined through the duration of the entire experiment. From 1.2000g of Fe(NH4)2(SO4)2 were synthesized 1.1###g of K3[FeIII(C2O4)3]·3H2O
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Preparation of N‚N-Diethyl-m-toluamide (DEET) and its Identification by IR and NMR Spectroscopy Eim A. Chemist CHEM 304 July 10‚ 2005 INTRODUCTION N‚N-Diethyl-m-toluamide (DEET) is the active ingredient in many insect repellants.1 In this experiment‚ DEET will be prepared from m-toluic acid through the intermediate acid chloride and then identified by its IR and proton NMR spectra. The overall reaction is a series of two acyl substitutions and is shown in Scheme 1 below: [pic] Scheme
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Moles of Iron and Copper Lab Data and Observations Before the reaction: Mass of empty‚ dry beaker: 153.44g Mass of beaker + copper (II) chloride: 161.44g Mass of two iron nails: 7.27g After the reaction: Mass of two iron nails: 6.29g Mass of beaker + copper (dry): 154.50g Questions and Calculations 1. a) Mass of two iron nails before the reaction – Mass off two iron nails after the reaction = Mass of iron used in the reaction = 7.27g – 6.29g = 0.98g
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