Separation Of a Sample Mixture By Liquid-Liquid Extraction Reading assignment: Techniques in Organic Chemistry 2nd ed pages 75-99. 3rd ed pages 113-140. Topics and Techniques i) identification of solvent layers of two immiscible solvents ii) partioning of a compound between two immiscible solvents and determination of KD iii) liquid-liquid extraction with aqueous acids and bases with organic solvents. iv) use of drying agents Introduction Liquid-liquid extraction is a method used for the separation
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Experiment 3 Liquid-Liquid Extraction Discussion The success of extracting each compound out of the solution can be seen in the IR graphs for each substance. For ethyl 4-aminobenzoate‚ the N-H‚ C=O and C-O are distinguishable in their proper wavenumber positions. The amino N-H stretch was found between 3224 cm-1 and 3423 cm-1. The C=O was found at 1681 cm-1 and the C-O was at 1280 cm-1. The IR for benzoic acid also displays its significant bonds‚ O-H and C=O. The O-H was between 2566 and
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Laboratory #16: Analysis of Grease in Water by Solvent Extraction Experiment Date: 2/19/10 Due Date: 2/26/10 II. Objective The goal of this lab was to determine the amount of impurity‚ in the form of oil‚ in water using the method of solvent extraction‚ also known as liquid-liquid extraction‚ a method of separating two materials with different physical and/or chemical properties. Two methods of evaporation will be used to finally determine the concentration of impurity- one using an explosion-proof
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of Acetyleugenol (Clove Oil) from Cloves Purpose In this experiment‚ you will obtain the essential oil from cloves by steam distillation. You will then separate a component (acetyleugenol) from the oil by liquid-liquid extraction. Finally‚ you will isolate the acetyleugenol by using a rotovap for reduced pressure distillation‚ which will remove the organic solvent (dichloromethane). Background Whole cloves contain between 14% and 20% by weight of essential oils‚ but only half
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when dried‚ provide the cloves of commerce. The flowers have a strong refreshing odour if the seed are allowed to mature‚ most of the pungency is lost. Each berry has only one seed. The trees fruit usually about eight or nine years after planting. The whole tree is highly aromatic. The finest cloves come from Mallacca and Pemba and also East & West Indies‚ Mauritius and Brazil. Ethenomedicinal Practice It is used as a domestic spice world-wide. Tincture of cloves has been used for skin infections
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H83 CEL – CHEMICAL ENGINEERING LABORATORY PROJECT TITLE: SOLID LIQUID EXTRACTION OF GANODERMA LUCIDUM NAME: WIJETUNGE MUDALIGE DINITHI ISHARA WIJETUNGE ID NO: 007118 SUPERVISOR: DR SIVAKUMAR MANICKAM GROUP MEMBERS: KOW NIEN WEI AAZRA OUMAYYAH PANKAN JASON HEW YIP SENG DATE: 30 APRIL 2012 H83 CEL Chemical Engineering Laboratory Solid Liquid Extraction of Ganoderma Lucidum Author: W.M.Dinithi Ishara Wijetunge I certify that: (i) Apart from the experimental results reported in the
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Part A: Diffusion on a liquid in a liquid. I did an experiment with three different glasses of tap water from the faucet. All three cups measured the same which happened to be 13 cm from the top of the cup to the bottom of the cup. I let the water settle‚ and sit for about an hour so the temperature was the same for all three cups. I then placed one drop of food coloring into the first glass and waited for the coloring to reach the bottom. I calculated 93 seconds. I then went to the second glass
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------------------------------------------------- Liquid–liquid extraction From Wikipedia‚ the free encyclopedia Liquid–liquid extraction also known as solvent extraction and partitioning‚ is a method to separate compounds based on their relative solubilities in two different immiscible liquids‚ usually water and an organic solvent. It is an extraction of a substance from one liquid into another liquid phase. Liquid–liquid extraction is a basic technique in chemical laboratories‚ where it is performed
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39. The Viscosity of Liquids After studying the present lecture‚ you will be able to Define viscosity and viscosity coefficient Outline the method to measure viscosity using Ostwald viscometer Determine the average molecular weight of a polymer Determine the surface concentration of 1-butanol in aqueous solution Measure the distribution coefficient of a solute betweenn two solvents 39.1 Introduction Viscosity‚ one of the transport properties‚ arises because of intermolecular attractive and
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packed closely together‚ but they are able to move around. Hence a fluid does not have a rigid shape‚ but adapts to the contours of the container that holds it. Like a liquid a gas has no fixed shape‚ but it has little resistance to compression because there is enough empty space for the molecules to move closer. Whereas a liquid placed in a container will form a puddle at the bottom of the container‚ a gas will expand to fill the container. Although the three categories seem very well defined
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