Gravimetric Analysis CHEM 200-03 Fall Semester 2012 September 19‚ 2012 Jeff Marasigan Abstract Gravimetric analysis is based on the quantitative isolation of the desired constituent the analyte of interest from the sample in highly pure form or in some combined form and weighing the isolated constituent. The desired constituent is usually isolated or separated by precipitation. From the weights of sample and precipitate‚ the percentage of the constituent in the original sample can
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GRAVIMETRIC ANALYSIS Methods in GA Precipitation Method - involves isolation of an ion in solution by a precipitation reaction‚ filtering‚ washing the precipitate free of contaminants‚ conversion of the precipitate to a product of known composition‚ and finally weighing the precipitate and determining its mass by difference. From the mass and known composition of the precipitate‚ the amount of the original ion can be determined. Volatilization Method -the analyte or its decomposition products
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11/17/2011 The Preparation of Calcium Carbonate Purpose: To create chalk (calcium carbonate) and to find the percentage yield in order to see the amounts of anhydrous sodium carbonate and calcium chloride were used up. Also to see if there’s any alterations like mass differentials. Objectives: 1. To introduce the concept of “limiting factor” in a chemical reaction 2. To practice a. Writing a balanced equation b. Determining the number of moles of each reactant and product
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SynopsisThe objective is to determine the amount of Sulphate in anhydrous Barium Sulphate precipitate by gravimetric method. Gravimetric method is by the quantitative determination of the mass of anhydrous Barium Sulphate precipitate. Barium sulphate precipitate is form when Barium Chloride is added excessively to a hot given Sulphate solution slightly acidified with concentrated Hydrochloride acid. The white precipitate of hydrate Barium Sulphate formed is than digest‚ filtered out‚ washed and dried
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Density of Metals Problem: How does the mass and volume help determine the density of known metal samples? Hypothesis: When comparing the density of Zn(zinc) and Cu(copper)‚ you will find that Copper is more dense than Zinc. You can test this out by using the density formula D=m/v. Materials: * 2 metals (options: zn‚ al‚ or cu) * 3 samples of each metal (small‚ medium‚ and large) * Scale/Balance * Calculator * Water * Graduated Cylinder Safety: * Be prepared for your
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Density of Metals Lab 1. Purpose The purpose of this lab was answered in 4 questions‚ and their answers are here shown. The density of the metals we used were 5g/cm3. The density of a metal piece does not depend on its size‚ it depends on the total mass and total volume. The most accurate way of determining density is dividing mass by volume. You can’t identify metals by their density. It can help you narrow the options down‚ but you can’t identify a metal by using only its density. 2. Question
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Experiments with Metals and Ions of Metals Introduction Metals are similar in their physical properties in general‚ but they are not identical. Most of the metals are solids; few of them are liquids‚ such as mercury and cesium. Density of metals is not similar also. For example‚ sodium has density of 0.97g/cm3 while lead has density of 11.4g/cm3. Melting point of sodium is 98.0oC while for lead it is 327.6oC. Metals have the capability to lose electrons when they react with non-metals such as
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I. Title: Reaction of Metals II. Problem: The purpose of the experiment was to determine if and how different metals react to different solutions. III. Hypothesis: IV. Materials: Dropper‚ Beakers‚ wax pencil‚ Goggles‚ eight test tubes‚ a rack for the tubes‚ three strips of Zinc‚ two strips of Copper‚ three strips of Magnesium‚ steel wool‚ Lead nitrate‚ Silver nitrate‚ Copper sulfate‚ Magnesium chloride‚ Zinc chloride‚ Sodium chloride‚ and Potassium. V. Procedure: In tube 1 add five
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Abstract Gravimetric analysis describes the methods for finding the chemical constituent of analyte in a solution through analytical chemistry. This method uses the mass of solid SO42-‚ with an unknown quantity and quality‚ to qualitatively determine the makeup of the solid SO3-. Two separate experiments with the initial compounds of BaCl2 and SO42- were put into solution to allow for the BaSO4 precipitate to form. Through filtration and ignition of precipitate containing ashless papers
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are required for Calcium carbonate precipitation Abstract: Introduction: Different minerals precipitation by microbes is a common phenomenon‚ and carbonates are most common mineral formed. Many micro-organisms are having the ability in undergoing the process of mineralization‚ although different minerals have been precipitated by microbes which include carbonates‚ sulphates‚ silicates etc [1]. Amongst all these‚ carbonates are the most common minerals formed. Carbonate precipitation has been applied
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