Isolation of Trimyristin from Nutmeg by Extraction Introduction: Extraction is the physical process by which a compound or mixture of compounds is transferred from one phase into another. We will be looking specifically at an organic solvent extraction which is a type of solid-liquid extraction. This type of extraction utilizes an organic solvent that has a high affinity for the compound of interest. Most reactions produce a crude mixture of undesired reagent‚ byproducts‚ as well as the
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EXTRACTION OF TRIMYRISTIN FROM NUTMEG: Paul I. PURPOSE: The purpose of this experiment was to illustrate the extraction of a solid natural product from its natural source by partition with the aid of an organic solvent. Extraction is the process by which a compound or mixtures of‚ is transferred by separation from one phase into another. In this case‚ the major triglyceride contains a single fatty acid identified as myristic acid. It is a substituent
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ISOLATION OF TRIMYRISTIN FROM NUTMEG ABSTRACT The purpose if the experiment was to extract the Trimyristan from ground nutmeg using extraction‚ distillation and recrystallization procedures. This experiment involves extraction and separation techniques that yield a purified product. The product was extracted and a distillation process was used to remove any remaining solvent. The recrystallization of the sample in turn produced a pure sample‚ which was proven using the known melting
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Organic Chemistry I – CHEM 201-DL01 September 26‚ 2014 Organic Chemistry Experiment 4B Lab Report Extraction of Organic Compounds From Natural Sources: Extraction of Trimyristin From Nutmeg Introduction The purpose of this experiment is to illustrate how a solid natural product can be extracted from its natural source through the use of an organic solvent. Natural products are organic compounds that are synthesized by natural biological processes in plants‚ animals
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Isolation of Trimyristin from Nutmeg and preparation of Myristic Acid from Trimyristin by Hydrolysis Introduction Over 40% of medicinal chemicals in the world were developed from isolation of the natural source. These sources were from fungi‚ plants‚ bacteria‚ animals‚ etc. The techniques used to isolate and purify has been by extraction‚ distillation‚ recrystallization‚ and chromatography. In this experiment we will be trying to obtain a pure organic compound from a natural source. Because this
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Nutmeg Isolation of Trimyristin from Nutmeg and preparation of Myristic Acid from Trimyristin by Hydrolysis Introduction Over 40% of medicinal chemicals in the world were developed from isolation of the natural source. These sources were from fungi‚ plants‚ bacteria‚ animals‚ etc. The techniques used to isolate and purify has been by extraction‚ distillation‚ recrystallization‚ and chromatography. In this experiment we will be trying to obtain a pure organic compound from a natural source. Because
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Trimyristin is an ester with the chemical formula C45H86O6 that can be isolated from the common spice nutmeg. The seed of the evergreen trees in the genus Myristica Fragrans is what nutmeg is obtained from. Trimyristin is the triglyceride of myristic acid also known as saturated fat (3). The phase of trimyristin is solid and is only found soluble in dichloromethane‚ chloroform‚ ether‚ benzene‚ and ethanol (1). Only twenty to twenty-five percent of trimyristin makes up the mass of nutmeg and it
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SUPPLEMENTARY MATERIAL (#2000-0709) SOAP FROM NUTMEG: AN INTEGRATED INTRODUCTORY ORGANIC CHEMISTRY LABORATORY EXPERIMENT Marcio C.S. de Mattos and David E. Nicodem Departamento de Química Orgânica‚ Instituto de Química‚ Universidade Federal do Rio de Janeiro‚ Caixa Postal 68545 21945-970‚ Rio de Janeiro‚ Brazil 1) Written material used by students 2) Instructor notes 3) Chemical abstract registry number of chemicals 1) Written material used by students Soaps
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Experiment 2: Extraction – Evaluation Summary Labs reports must be typed and chemical structures must be drawn with ChemDraw. Report must not exceed three pages (including this page). Page limit does not include any attached spectra or references. ** Deductions for hand written report/structures and exceeding page limit ** Report Breakdown Data/Results: _________________ /10 Discussion: _________________ /10 Report Total: _________________ /20 Other Lab Marks
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chemical synthesis: extraction of crude caffeine pose little toxicity to human health and the environment.(1) Q2) Things not green: According to GCP# 5 i.e. Safer solvent and auxiliaries: In liquid-liquid extraction of caffeine‚ Dicholoromethane was used which is a hazardous chemical and have potential acute health effects(2). According to GCP#12 i.e. Inherent safer chemistry for accident prevention: The separatory funnels used in the experiment for liquid-liquid extraction was a dangerous procedure
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