PRE LAB REPORT Reynaldo Riboul TLC and Column Chromatography October 6‚ 2013 Table of Chemicals: Chemical Hazards Mol. Wt. Density Grams Moles Acetone Flammable‚ Irritant 58.08 g mol−1 0.791 g cm−3 2.0 g 0.0344 Hexane Flammable‚ Irritant‚ Dangerous to Environment 86.18 g mol−1 .6548 g mL−1 9.0 g 0.1044 Fluorene Very toxic to aquatic life with long lasting effects 166.223 g/mol 1.202 g/mL 0.3 g 0.00180 Fluorenone Irritant 180.20 g mol−1 1.13 g/cm3 0.3 g 0.00166
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Experiment 1: Bromination of Acetanilide1 Precautions: Ethanol is flammable Sodium hypochlorite is an oxidizing agent and releases toxic fumes (handle in fume hood) Acetic acid is corrosive‚ harmful if inhaled‚ flammable and can cause burns (handle in fume hood) Gloves are recommended to avoid chemical contact with skin Reaction Scheme: Conversion of acetanilide to p-bromoacetanilide Procedure: To a 125 mL Erlenmeyer flask containing a mixture of 95% ethanol (6 mL) and acetic acid (5 mL)‚ dissolve
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Response: “After sealing the bottle with a butyl rubber stopper and an aluminum crimp‚ the bottle was purged with pure nitrogen (for 10 min) to obtain anaerobic conditions.” This explanation is added to the revised manuscript. (Page 8‚ line 13-15) Comment 14: Page 8: Explain if pH was controlled during fermentation. In any case‚ do a reference in the result section to the pH at the end of fermentation Response: The pH was not directly controlled during the fermentation. In the line with typical
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TITLE: Determination of Riboflavin by using UV-Vis spectrophotometry. ABSTRACT: The amount of Riboflavin in various brand of children multivitamins was determine by using UV-Vis spectroscopy instrument‚ the series of standard of riboflavin was prepared in order to determine the amount of the riboflavin in the sample of children multivitamins. The maximum amount of riboflavin was found in the Champs multivitamin that contains 0.1155 mg followed by Chewies 0.1131 mg and Scott’s 0.0672 mg. OBJECTIVES:
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Simple Distillation of Ethyl Acetate contaminated with Methyl Violet Operational OrganicChemistry A Problem Solving Approach to the Laboratory Course‚ 4th edition‚ by John Lehman‚ Experiment 4‚ OP-30 pg 710-719 I. Introduction The students will use the distillation method to extract pure Ethyl acetate by using the distillation equipment. The distillation is the process of vaporizing a liquid mixture in one vessel and condensing the vapors into the receiver. II. Experimental procedures. 1
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Scent-Infused Textiles consumer acceptance of fragrance-embedded textiles. Consumer willingness of finished products. The Sensory Perception Technologies (SPT) allows textile producers to weave particles of moisturisers‚ deodorants‚ fragrances and even anti-tobacco agents into fabrics. "Early trials have proved SPT a success with many global clothing companies interested‚" ICI‚ whose fragrances unit Quest developed the technology. ICI said the technology allows fabric makers to incorporate tiny
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5.1 MANUFACTURING PROCESSES: Acetone is produced directly or indirectly by propylene. Early processes for the manufacture of acetone were based on the thermal decomposition of calcium acetate or the carbohydrate fermentation of corn starch or molasses. The ready availability of propylene in the 1960s led to routes based on the dehydrogenation of isopropyl alcohol or cumene peroxidation. (1) By Cumene Oxidation (Hock Process). Propene is added to benzene [71-43-2] to form cumene [98-82-8]‚ which
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Making Ethyl Ethanoate Alternative methods of production To compare the effectiveness of producing ethyl ethanoate in the experiment I completed to other alternative methods I am going to use the atom economies. Atom economy = molar mass of useful product/molar mass of all reactants *100. Alternative 1 2CH3CHO CH3COOC2H5 This experiment would produce an atom economy of 100%‚ as there is one reactant making one product meaning there are no waste products produced. Although this experiment would
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Abstract The purpose of this experiment is to synthesize isopentyl acetate via an esterification reaction between glacial acetic acid and isopentyl alcohol‚ using concentrated sulfuric acid as a catalyst. The product was washed using sodium bicarbonate and water‚ then dried with anhydrous sodium sulfate. It was then distilled using a standard simple distillation apparatus. The percent yield of isopentyl acetate was 60.39%. This may have been low due to incomplete distillation or evaporation once
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Experiment 12: Isopentyl Acetate 19 October 2012 Introduction: The purpose of this experiment is to prepare isopentyl acetate by direct esterification of acetic acid with isopentyl alcohol. After refluxing there is an isolation procedure where excess acetic acid and remaining isopentyl alcohol are easily removed by extraction with sodium bicarbonate and water. The ester is then purified by simple distillation and the IR is then obtained. Techniques and equipment used throughout the experiment
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