Chemical Engineering Design and Professional Skills B Second assignment M A N U F A C T U R E O F S T Y R E N E Assignment 2 – Monday 28/01/13 You have a provisional flowsheet for a process to manufacture 30 ton/h of styrene from ethylbenzene. This is described below. (It may differ in some details from the one you developed last term – but if so‚ you should use the version described here‚ so that all groups are working with the same‚ correct process.) For Assignment 2 of
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Introduction 3 Results 4 Discussion 6 Conclusion 7 Experimental 7 References 8 Preparation of 2-Acetylcyclohexanone Introduction When hydrogens are present on the α-carbon of ketones (like the reaction used in this experiment)‚ carbonyl compounds and aldehydes‚ they turn the compound slightly acidic1. These functional groups are removed by using a basic solution as shown in (i) below1. The product formed with water is stable only due to resonance‚ but does
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The Distillation of an Unknown Compound INTRODUCTION Distillation is the process heating a liquid to form vapor which is then collected when cooled and separated from the original liquid. The purpose of this experiment was to determine the identity of an unknown substance using simple and fractional distillation. Gas chromatography analysis the components of a mixture by separation of the materials by their different boiling points. EXPERIMENTAL The simple distillation apparatus was assembled
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1.4 Methods of Extraction of Essential Oils Following are the methods used to extract essential oils from aromatic and medicinal plants: • Hydrodistillation: For the isolation of essential oils by Hydrodistillation‚ the aromatic plant substances are packed in a still and a sufficient amount of water is added and brought near to a boil. Due to the influential effect of hot water and steam‚ the essential oil is unbounded from the oil glands present in the plant tissue. The combination of water
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2. From the plots of the boiling point versus the volume of distillate in the simple distillation experiments‚ what can you conclude about the purity of your product? Product not very pure. No distinct line to know when one begins and one ends. Distillation of cyclohexane and toluene crossed over into the other’s range. Would need to perform more distillations to better purify the solvents. 5. What is the effect on the boiling point of a solution (e.g. water) produced by a soluble non-volatile
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Biotechnology‚ Mapua Institute of Technology [pic] ABSTRACT The purpose of this experiment is to prepare cyclohexene form cyclohexanol‚ and know the properties of alkene. The first part of this experiment is preparation of cyclohexene. Simple distillation set-up is assembled. (See Figure 1). Exactly 6.0mL of cyclohexanol is weighed in a quick-fit one-necked pear shaped flask. 1.50mL of 85% H3PO4 is measured using the 2mL pipet and added to the weighed cyclohexanol. Another 0.25mL of concentrated
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using it. It is done by a method called fractional distillation which involves separation of two or more liquids having different boiling points. The refining is done by changing the liquid into its gaseous state and then cooling the gaseous mixture at controlled temperatures such that at a time only one of the vapours having boiling point I liquefies first. This is generally done by a special tower called fractionating column. Fractional distillation of petroleum Crude petroleum is heated to a temperature
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CHM 2210L-009 Experiment 1: Simple and Fractional Distillation of a Binary Mixture Aim: The aim of this experiment is to perform a simple and a fractional distillation and separate a mixture containing two liquids‚ cyclohexane and toluene. Post Lab: At any given temperature a liquid is in equilibrium with its vapor. This equilibrium is described by the vapor pressure of the liquid. The vapor pressure is the pressure that the molecules at the surface of the liquid
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This page intentionally left blank SEPARATION PROCESS PRINCIPLES Chemical and Biochemical Operations THIRD EDITION J. D. Seader Department of Chemical Engineering University of Utah Ernest J. Henley Department of Chemical Engineering University of Houston D. Keith Roper Ralph E. Martin Department of Chemical Engineering University of Arkansas John Wiley & Sons‚ Inc. Vice President and Executive Publisher: Don Fowley Acquisitions Editor: Jennifer Welter Developmental Editor:
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Fractional Distillation Name: Pinaki Das Partner’s Name: Alice Kim Course: Advance Science Grade 9 Slot: B Date: November 6th 2013 Fractional distillation separates a mixture of liquids based on differences in the boiling points of the liquid. The purpose of this experiment was to identify
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