Experiment 29 – Borohydride Reduction of Vanillin to Vanillyl Alcohol Goal To perform a sodium borohydride reduction of an aldehyde to produce an alcohol. Reading and Working Ahead Your discussion should include a mechanism for this reaction. Review: OP 12 – Vacuum filtration OP 28 – Melting point (using Mel-Temp®) Procedure Notes Calculate the necessary mass of vanillin and sodium borohydride for the procedure below. Also calculate theoretical yield of vanillyl alcohol. You
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John Heger CMY 211 Lab Section 13 11-30-2011 Borohydride Reduction of Vanillin to Vanillyl Alcohol Introduction: The purpose of this lab was to reduce vanillin to vanillyl alcohol. This lab report recaps the procedure and results of the lab. The chemical process studied in this lab was reduction‚ the process of reducing the number of bonds to oxygen and increasing the number of bonds to hydrogen. Other chemical processes included in the lab were recrystallization‚ melting point‚ and extraction
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experiment of making borneol from camphor (FIGURE-3) is performed in two different methods‚ Sodium Borohydride Reduction and Meerwein-Ponndorf-Verley Reduction‚ to compare the relative product ratio of borneol to isoborneol. The concept of reduction and also oxidation‚ the opposite procedure of reduction‚ deals mostly with electron transfer between atoms. It will not be elaborated here‚ but the reduction procedure involved in this experiment is basically adding hydrogens and losing the carbon-oxygen
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Sodium borohydride Reduction of Benzil Introduction: The Purpose of this experiment is for the students to learn how to use sodium borohydride to reduce benzil to its secondary alcohol product via reduction reaction. This two-step reaction reduces aldehydes by hydrides to primary alcohols‚ and ketones to secondary alcohols. In order for the reaction to occur and to better control the stereochemistry and yield of the product‚ the metal hydride nucleophile of the reducing agents such as LiH‚ LiAlH4
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WHAT IS HARM REDUCTION? Harm reduction is a set of practical strategies intended to reduce the negative consequences of high risk behavior such as over drinking or drug abuse. Harm reduction is a non judgmental approach that attempts to meet people where they are at with their drinking or drug abuse. Instead of demanding perfect abstinence‚ this pragmatic approach is supportive of anyone who wishes to minimize the harm associated with a high risk behavior such as drinking or drug abuse. Harm
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The Pros and Cons of a Breast Reduction Shavanna Levette Hudson Instructor: Pamela Jongbloed ENG 121 English Composition I July 29‚ 2014 The Pros and Cons of a Breast Reduction The decision to have a breast reduction surgery came after years of continuous back pain throughout my life. My experience has been a real journey in researching the right doctor and asking the right questions for this type of surgery. My journey began in 2012 after many attempts to lose weight. I began doing
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Experiment 5B: Ketone Reduction Objective: Using sodium borohydride as a reducing agent‚ the ketone 4-tert-butylcyclohexane is reduced to its corresponding alcohol. It is purified through extraction techniques to give the cis and trans diasteromer products. Procedure: The procedure was followed as outlined in Mayo’s book for Experiment 5B with the following modifications: 1. Reagents and Equipment – The reaction will be on a scale of 2X what is described in the text. 2. Reagents and Equipment
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Titus‚ Godley and White‚ 2006; Dennis‚ et al.‚ 2007) thus an alternative method to preventing further problems is the concept of harm reduction. This essay will thereby explore the strategies of harm reduction including its potential negative and positive aspects for injecting drug users and its relation to crime. Furthermore‚ it will explore extended harm reduction services specifically for drug users in Austria. Injecting drug use is acknowledged in 135 countries (UNODC‚ 2004) and is associated
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Borohydride Reduction of a Ketone Results 1. Draw a three-dimensional structure of the stereoisomer formed in the reaction. Name the compound. meso-Hydrobenzoin 2. Include other results as suggested by your data. * The attached IR and NMR spectroscopy data. * The melting point that ranges from 135.6-137.90C. Spectroscopic Analyses Data tables IR Spectroscopy Hydrobenzoin Peaks (cm-1) | Stretches | Intensity | 3332 (cm-1) | O—H stretch | Strong and broad | 3027
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Harm Reduction paper Randy Jones Substance Abuse Counselling January 18‚ 2012 This paper will discuss the principles and position of harm reduction. It will also examine the public perception of the user‚ which has created an ineffective philosophy. Most importantly‚ my paper seeks to recognize the harm of harm reduction. This discussion will highlight the lack of hope it creates in the user. Harm reduction needs to be addressed so that a long-term solution for the user can be implemented‚ not
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