Experiment 2 and 3: Synthesis of Aspirin and Determination of Melting Point A. Abstract Aspirin is the common name for the compound acetylsalicylic acid‚ widely used as a fever reducer and as a pain killer. The first part of the experiment aims to synthesize aspirin from the reaction of salicylic acid with acetic anhydride with the aid of phosphoric acid as a catalyst. The second part of the experiment aims to assess the purity of aspirin through the determination of its melting point and
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Lab Report Synthesis and Characterization of Aspirin (Acetylsalicylic Acid) The Synthesis and Characterization of Aspirin (Acetylsalicylic Acid). Summary: In this experiment‚ we produced 4.21 g of acetylsalicylic acid. Our theoretical yield was calculated to be 5.22 g. Therefore our % yield was determined to be 80.6%. The experimental boiling point range of acetylsalicylic acid was found to be 130-132° C. The true melting point of acetylsalicylic acid is 135° C‚ therefore our percent
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Preparation and melting point of Aspirin Aspirin is a painkilling drug and is produced worldwide to reduce and stop pain. Aspirin is made up of ehtanoylation of 2-hydroxbenzenecarboxylic acid in a presence of phosphoric acid. AIM: The aim of the experiment is to prepare and produce aspirin as pure as possible. I will do this threw preparing the aspirin and purifying the product threw recrystallization. I will then obtain a melting point of my product to get an estimate of its purity. By the end
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EXERCISE 11 SYNTHESIS OF ASPIRIN MARAVILLA‚ Ana Mikaela B Group 4 CHEM 40.1 1L Date performed: September 30‚ 2013 Date submitted: October 7‚ 2013 VI. RESULTS AND DISCUSSION Aspirin is prepared by the esterification of salicylic acid with acetic anhydride under acidic conditions. The phenol group in salicylic acid is replaced by a carboxyl group through electrophilic substitution. The mechanism for the reaction can be summarized
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1. Aim To determine the percentage of aspirin in different commercial preparations and to find which is the best value for money 2. Hypothesis The greater the percentage of acetylsalicylic acid (ASA) in the tablet‚ more powerful and efficient the aspirin would be due to the way aspirin works in human’s body. Aspirin is often used to alleviate the pain‚ and the sensation of pain is mainly attributed to a chemical substance called prostaglandins‚ which is responsible to send a strong signal
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Darnell Shaw Lab Extra Credit Hippocrates of Cas (460-377 B.C.)‚ The Healer‚ noted that chewing leaves of willow (Salix) reduced pain‚ and he prescribed this remedy for women in labor. The Healer certainly did not discover this drug‚ which was used for centuries earlier in European folk medicine. Ancient Egyptians took an infusion of dried myrtle leaves to treat muscle pain. The myrtle leaves were also found to contain salicylic acid. Two Italians‚ Brugnatelli and Fontana‚ had in fact already
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History Of Aspirin Aspirin is one of the most commonly used drugs in the world.. For centuries people throughout the world. Aspirin was discovered about 3500 years ago. A collection of 877 medicinal recipes‚ The Ebers papyrus‚ before Christ‚ from the middle of the second millennium had been bought during the last century from an Egyptian street vendor by Georg Ebers‚ a German Egyptologist Georg. He recommended an infusion of dried myrtle leaves for rheumatic and back pain. More than a
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Learning Center‚ Inc. 6539 Isabel‚ Leyte Synthesis of Aspirin An Investigatory Project Presented to: Edmundo A. Quiñones Chemistry Teacher In Partial Fulfillment of the Requirements In Science and Technology III (Chemistry) Presented by: Kenneth Ivan P. Durano Cyrill Val G. Lozano March 6‚ 2010 APPROVAL SHEET This investigatory project entitled “The Synthesis of Aspirin” requirement for Science and Technology III (Chemistry) has been
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Experimental Synthesis of Aspirin and Melting Point Purity Analysis Donald Yeargin CH 222‚ Section 24221 Department of Chemistry Portland Community College Portland‚ OR Abstract The various methods available to synthesize aspirin lead to the need to examine and evaluate production efficiency and purity. The purpose of our experiment was to synthesize acetyl salicylic acid (aspirin) and then determine the relative purity of the synthesized sample by observing the melting point temperature
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Preparation and Recrystallisation of Aspirin Contents Page Synopsis iii 1 Introduction 1 1.1 Objective 1 1.2 Background 1 2 Theory 1 3 Procedure 2 3.1 Materials 2 3.2 Preparation 2 3.3 Recrystallisation 3 3.4 Determination of Melting Point 3 4 Results and Calculation 4 4.1 Mass 4 4.2 Percent yield 4 4.3 Melting Point 4 4.4 Appearance 4 5 Discussion 5
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