EXPERIMENT II: SEPERATION OF A MIXTURE OF SOLIDS PURPOSE: The purpose of this experiment was for me to become familiar with the separation of mixtures and solids and to learn separation techniques based on the chemical properties of a substance. PROCEDURE: Before beginning‚ I set up a data table to record data from the experiment. 1. Separating out the Iron a) I used my digital scale to determine the mass of my weighing dish. b) I emptied the entire mixture of solids from the plastic bag into
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included‚ not everything. 2. WE + acidified K2Cr2O7 2 = sol 3 turns green 3. WE + acidified KMnO4 = pink colour of KMnO4 is discharged 4. Sulphide: Colourless gas with a smell of rotten eggs (H2S); turns lead acetate paper black 1. Sodium nitroprusside test: WE + sodium nitroprusside 4 = purple / violet colour 2. Lead acetate test: WE + lead acetate 5 (aq) = black ppt 5. Nitrite: Pungent light brown gas 1. Starch-iodide test: WE + dil H2SO4 (or dil acetic acid); boil‚ then add solid KI + fresh starch
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Name : ……………………………………………………………….. Date Due : …………………………………………………………….. Year 12 80% A 70% B AS Level Chemistry 60% C 2008 – 2009 50% D 40% E Below U Questions on % Haloalkanes 2.8 32 1. Chloromethane can be prepared by a reaction between methane and chlorine in the presence of ultraviolet radiation. (i) Outline the mechanism for this reaction. .....................................................................................
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Aim: To compare the foaming capacities of five different commercial soaps. Apparatus: 5 test tubes‚ 5 conical flasks (100 ml)‚ test tube stand‚ Bunsen burner and stop watch. Materials Required: 5 different samples of soap and distilled water Theory: The foaming capacity of a soap sample depends upon the nature of soap and its concentration. This can be compared for various samples of soaps by taking the same concentration of solution and shaking them.The foam is formed and the time taken
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10-4 mol KIO3 4.675 x 10-4 mol KIO3 x (6 mol Na2S2O3 / 1 mol KIO3) = 0.002805 mol Na2S2O3 0.002805 mol Na2S2O3 / 0.03005 L Na2S2O3 = 0.093344426 M Na2S2O3 Determination of the Ascorbic Acid Titration Mass of the ascorbic acid sample‚ g Volume of Sodium Thiosulfate solution‚ mL Weight % of the Ascorbic Acid in the tablet 1 0.1018 19.50 85 % 2 0.1016 19.20 88 % 3 0.1003 19.20 89 % IO3- + 8 I- + 6 H+ → 3 I3- + 3 H2O I3- + 2 S2O32- → 3 I- + S4O62- C6H8O6 + I3- + H2O → C6H6O6 + 3 I- + 2 H+ TITRATION
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amount of heat absorbed or released during the dissolving of ammonium nitrate and of sodium acetate in water. 2.0 g of solid NaOH is dissolved in 100 mL of water. The initial and final temperatures are measured and recorded. The heat of solution is calculated (ΔH1) Reaction 2. Na+(aq) + OH-(aq) + H+(aq) + Cl-(aq) → Na+(aq) + Cl-(aq) + H2O(l) 50 mL of 1.0 M hydrochloric acid solution is combined with 50 mL of 1.0 M sodium hydroxide solution. The initial and final temperatures are recorded‚ and the heat
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Emission Spectra & Flame Tests Intro The emission spectrum is used in modern chemistry to help further studies of wavelengths and the spectrum. When a metal in a compound reacts in a flame and produces a color‚ it helps to show the strongest color in the emission spectrum. The purpose of performing these operations on the flame was to see how different metals would react. Using a spectroscope‚ it is possible to observe the line emission spectrum produced by sunlight‚ artificial light‚ and
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very well. When NaCl solution is dissolved in water‚ the solution conducts very well‚ because the solution contains ions. The ions come from the table salt‚ whose chemical name is sodium chloride. Sodium chloride contains sodium ions‚ which have a positive charge‚ and chloride ions‚ which have a negative charge. Because sodium chloride is made up of ions‚ it is called an ionic substance. After completing the experiment and plotting each conductivity value I found that as the NaCl increased in concentration
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3.13 Test for Saponin glycosides 2g of dried plant powder add 5ml of distill water shake vigorously. Persistent of foam indicate the presence of saponin glycosides. 3.14 Test for Steroids (Salkowski’s test) 5ml of test solution add with 2ml of Chloroform and then Conc. H2SO4 sides of the test tubes. The appearance of color at the interface indicates the presence of steroids. 3.15 Experimental Procedure for preliminary Phytochemical studies (Brindha et al.‚ 1981) S. No Name of the Test
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a) Calculate the molar enthalpy change for the reaction b) Calculate the minimum quantity of magnesium required to ensure it is in excess. c) Calculate the temperature change if only 0.8 g of magnesium is added. 3. When 5.73 g of sodium chloride (NaCl) dissolves in 100 cm3 of water‚ the temperature of the water fell from 22.4 oC to 19.8 oC. Calculate the enthalpy change of the reaction. 4. When 2.3 g of magnesium chloride dissolves in 200 cm3 of water‚ the temperature rose by
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