by Georg Wittig in 1954‚ the Wittig reaction is a robust organic synthesis method for preparing stereospecific alkenes. In general‚ Wittig reactions involve an aldehyde or ketone and a Wittig reagent (triphenylphosphonium ylide) and result in the formation of an alkene product and triphenylphosphine oxide (side product). Stereospecific alkene products can be synthesized by adjusting the reaction reagents and conditions. In the 60 years since the Wittig reaction was discovered‚ many articles have
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CHEM111AC‚ Experiment#9 - Ionic Reactions Discussion/Error Analysis In the first part of this experiment‚ the student was presented with 7 unique and unidentified bottles of solutions labeled A-G and was expected to be able to analyze the 7 solutions through trial and error and mixing them with one another. For solution A: mixing A + B formed a precipitate‚ A + C generated heat‚ A + D gave no reaction‚ A + E gave no reaction‚ A + F gave no reaction‚ A + G formed a precipitate. For solution B: mixing
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In this lab my group and I tested to see how yeast would react to different substances. Yeast is a fungi that releases carbon dioxide which can be used in the process of bread making. During this lab we used sugar‚ warm water‚ cornstarch‚ yeast‚ a gas sensor‚ plastic cylinders‚ and a laptop. The process of this lab was to create cellular respiration‚ which is what cells do to break up sugars into a form that the cell can use as energy. When yeast and a certain substance were combined‚ this substance
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Grignard Reaction: Synthesis of Triphenylmethanol Hai Liu TA: Ara Austin Mondays: 11:30-2:20 Abstract: In this experiment‚ phenylmagnesium bromide‚ a Grignard reagent was synthesized from bromobenzene and magnesium strips in a diethyl ether solvent. The Grignard reagent was then converted to triphenylmethanol‚ a tertiary alcohol with HCl. The reaction for phenylmagnesium bromide was: The reaction for Grignard to triphenylmethanol was: In the formation of the Grignard reagent
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of the reaction: The effect of the temperature of the reaction on the activity of the purified enzyme was carried out by make the enzymatic reaction for 10 minutes at different temperature 25‚30‚35‚40‚45‚50‚60 and 70°C using an enzyme protein 0.1mg/reaction mixture and substrate concentration of 15 mg/reaction mixture‚ using a control of previously heated enzyme solution in the reaction. The data recorded in (table 27) and (figure 29) illustrate the effect of temperature of the reaction on the pectinase
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98.) Consider the unbalanced redox reaction: Cr2O72- (aq ) + Cu(s ) → Cr3+ (aq ) + Cu2+ Balance the equation in acidic solution and determine how much of a 0.850 M K2Cr2O7 solution is required to completely dissolve 5.25 g of Cu. Nitric acid is usually purchased in concentrated form with a 70.3% HNO3 concentration by mass and a density of 1.41 g/mL. How much of the concentrated stock solution in milliliters should you use to make 2.5 L of 0.500 M HNO3? Mass %= Mass Solute/ Mass Solvent + Mass
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Introduction‚ aim and hypothesis Chemical reactions are accompanied by the release or absorption of energy. Reactions which release energy are described as exothermic and those which absorb energy are endothermic. The energy released in chemical reactions was previously stored as chemical potential energy in the reactants; this stored energy is called enthalpy. The aim of this practical is to observe and classify chemical processes as endothermic or exothermic‚ based on the changes in temperature
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The SN2 reaction requires three qualities: a strong nucleophile‚ a good‚ unhindered leaving group‚ and a polar‚ aprotic solvent. For our reaction‚ we have all three bases covered. The nucleophile is an alkoxide‚ a deprotonated alcohol. Technically‚ because our alcohol is a phenol‚ the conjugate base is called a phenoxide. Phenol itself has a pKa of about 10‚ but our alcohol has more resonance opportunities‚ so the pKa is down around 8. This is sufficiently acidic for use of weak base like K2CO3 for
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Link reaction The link reaction takes place in the mitochondrial matrix and its main function is to turn the pyruvate into acetate for the kerb cycle. During the link reaction the pyruvate molecule undergoes decarboxylation and dehydrogenation‚ the enzymes pyruvate decarboxylase and pyruvate dehydrogenase remove the carboxyl group (which becomes a carbon dioxide molecule) and removes the hydrogen atoms from the pyruvate molecule. The coenzyme NAD accepts the two hydrogen atoms and becomes reduced
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The Grignard Reaction Abstract Through the use of the Grignard reaction‚ a carbon-carbon bond was formed‚ thereby resulting in the formation of triphenylmethanol from phenyl magnesium bromide and benzophenone. A recrystallization was performed to purify the Grignard product by dissolving the product in methanol. From here‚ a melting point range of 147.0 °C to 150.8 °C was obtained. The purified product yielded an IR spectrum with major peaks of 3471.82 cm-1‚ 3060.90 cm-1‚ 1597.38 cm-1‚ and 1489
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