reflux and distillation is complete 13C NMR and IR spectrum is used to identify the product or products for each reaction: 1a‚ 1b‚ and 2. Every individual in the group was assigned either 1a (1-propanol) or 1b (2-pentanol)‚ and 2 (1‚4-dimethyl-3-pentanol). The purpose of this experiment was to understand and become familiar with the reaction mechanisms and be able to observe and compare the product or products for each of the reactions using 13C NMR and IR. The reaction of 1-propanol (1a) with NaBr/H2SO4
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information‚ however they did not determine which solution an IR spectrum would be obtained for. This was determined by the strongest‚ or more visible spot on the plate. An error for this lab could have occurred at this point because the wrong spot was chosen. If the RF values were used to determined which spot to choose‚ results may yield a smaller presence of pure naphthyl ether and a larger presence of dichloromethane in the IR spectrum. The spot that is most visible on the TLC plate is the solution
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Anise oil was successfully able to be extracted from anise seeds during this experiment. It was done by first crushing the seeds‚ then placing them into a distillation apparatus. The distillation apparatus evaporated the liquid from the seeds‚ which was captured in a flask. Next‚ DCM was added to the distillate‚ which allowed the water to be separated from the anise oil. Finally‚ the DCM evaporated and the pure anise oil was collected. The process of steam distillation allowed the anise oil in
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Name CHE 173 Sec # January 25‚ 2005 Experiment 36: Determination of the Structure of a Natural Product in Anise Oil Purpose: The purpose of this experiment is to isolate the major component of anise oil and determine its identity and structure using melting point determination and IR spectroscopy. Introduction: The major component of anise oil has the chemical formula C10H12O. This compound is said to be hydrogen deficient‚ meaning that it contains less hydrogen atoms than would be needed for
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Callam 1/8 CHEM – 254 – WI -2009 Problem Set #1 – IR Spectroscopy - KEY 1. Which of the indicated bonds absorbs at the higher frequency in an IR spectrum? a. O or OH C=O > C-O b. N or NH C=N > C-N c. H or H C-H sp2 > C-H sp3 Callam 2/8 CHEM – 254 – WI -2009 2. What major IR absorptions are present above 1500 cm-1 for each compound? a. b. O sp3 C-H stretch 2950 C=O - ketone 1715 cm-1 cm-1 c. O sp3 C-H stretch 2950 cm-1 sp3 C-H stretch 2950 cm-1
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ORGANIC CHEMISTRY LAB I IR INTERPRETATION EXERCISE NAME ______________________________________________ ASSIGNMENT GRADE __________ Total points: 100 Assign one of the structures A – J presented on page 2 to each of the IR spectra provided (1 – 10). Base your assignment on one or more key frequencies‚ according to guidelines presented in the recitation notes and on p. A19–A31 of your textbook. Especially useful are p. A19 and A20. For each spectrum do the following: 1. Mark key absorption frequencies
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Running head: TRANSFORMATION AT THE IRS Module 8: Transformation at the IRS AMP 492 September 25‚ 2011 Introduction The purpose of this paper is to discuss the transformation at the IRS by examining the need for change‚ the outcome of change and the process of change. The challenges faced by the IRS will be discussed and Kotter’s 8-step model will be applied to the case study to determine whether or not it was or could have been implemented more effectively. This paper will provide an opinion
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EXECUTIVE SUMMARY The objective of this project is to study the dynamics of IR in SAIL‚ Bokaro Steel Plant and to analyze and reason out the possible causes for the same. Industrial Relations is the composite result of the attitudes and the approaches of the employers and the employees towards each other with regard to the planning‚ supervision‚ direction‚ and co-ordination with a minimum of human efforts and friction‚ with an animating spirit of co-operation‚ and with proper regard for the
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Ethyl Benzoate 3. 3-Pentanone 4. Pentanal * For given unknown Infrared spectra‚ figure out the compounds based on the absorption frequencies of C=O str.‚ C-H str.‚ and C-H bend. DATA AND RESULTS: Assignments for unknowns A-D: Spectrum letter: | Compounds | A | 3-Pentanone | B | Ethyl Benzoate | C | Pentanal | D | Benzaldehyde | Comparison of Observed and Calculated absorption Frequencies: Absorption Description | Experimental v | Calculated
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Table of Contents 1 Aims and Objectives Our aim is to reach mutually agreed outcomes by recognising where the employees and the business are now‚ where we want to be in the future and how we can get there. We began the negotiation process with very optimistic outcomes in mind‚ whilst considering our fall back options which would exceed current employer/ competitor offerings and protect the long term interests of the employees. We as the employee/ union group believed that the
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