add 5drops of 1 M ammonia solution. Mix. Record color change. B. Calcium oxalate equilibrium Put 5 mL of .1 M calcium chloride and 5 mL of .1 M sodium oxalate into 6 inch test tube. Mix by stoppering and inverting. Equilibrium is established by formation of white precipitate. Add concentrated HCl. Shake after each drop. Record any changes. C. Cobalt chloride equilibrium Heat 2 mL of saturated aqueous solution of cobalt chloride to boiling in a 6 inch test tube. Record the color before heating
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Common name cuprous cupric ferrous ferric stannous stannic chromous chromic manganous manganic Symbol Hg22+ Hg2+ Pb2+ Pb4+ Co2+ Co3+ Au + Au 3+ Systematic name (Stock system) mercury(I) mercury(II) lead(II) lead(IV) cobalt(II) cobalt(III) gold(I) gold(III) Common name mercurous mercuric plumbous plumbic cobaltous cobaltic aurous auric Formula NO3¯ NO2¯ CrO42¯ Cr2O72¯ CN¯ MnO 4¯ OH¯ O22¯ NH2¯ CO32¯ Symbols and Charges for Polyatomic Ions Name
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azide 13863-88-2 AgNO3 silver nitrate 7761-88-8 Ag2O silver oxide 1301-96-8 AgONC silver fulminate 5610-59-3 AgSNC silver thiocyanate 14104-20-2 Ag2C2 silver acetylide 7659-31-6 Ag2CO3 silver(I) carbonate 534-16-7 Ag2C2O4 silver oxalate 533-51-7 Ag2Cl2 silver(II) dichloride 75763-82-5 Ag2CrO4 silver chromate 7784-01-2 Ag2Cr2O7 silver dichromate Ag2F silver subfluoride 1302-01-8 Ag2MoO4 silver molybdate 13765-74-7 Ag2O silver(I) oxide 20667-12-3 Ag2S silver sulfide
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COrdination compounds Question 9.1: Explain the bonding in coordination compounds in terms of Werner’s postulates. =Werner’s postulates explain the bonding in coordination compounds as follows: (i) A metal exhibits two types of valencies namely‚ primary and secondary valencies. Primary valencies are satisfied by negative ions while secondary valencies are satisfied by both negative and neutral ions. (In modern terminology‚ the primary valency corresponds to the oxidation number of the metal
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brown gas 1. Starch-iodide test: WE + dil H2SO4 (or dil acetic acid); boil‚ then add solid KI + fresh starch sol = deep blue colouration Group II (conc H2SO4 group) – Cl(chloride)‚ Br- (bromide)‚ I- (iodide)‚ NO3- (nitrate)‚ CH3COO- (acetate)‚ C2O42(oxalate): Salt + conc H2SO4 1. No reaction: Group II anion not present. Continue to group III. 2. Chloride: Colourless white pungent fumes (HCl); intensify when glass rod dipped in NH4OH is brought near mouth of test tube 1. Silver nitrate test: WE + AgNO3
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PAC-II COMPLEXOMETRIC TITRATION Course Contents: C OMPLEXOMETRIC TITRATION T ITRATION Complexation‚ Chelation. Werner’s co-ordination number‚ Titrants Stability of complexes‚ titration curves. Types of complexometric titrations. Methods of detecting end point‚ Standardization. Application of complexometric titrations. COMPLEXOMETRIC TITRATIONS COMPLEXOMETRIC TITRATIONS What is Complexometric Titration (CT)???? What What is a complex metal ion? A complex
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occurred. PROCEDURE: 1 Cotton Swabs‚ 1 Sheet each of white and black paper‚ 1 Distilled water‚ Goggles-Safety‚ 1 Well-Plate-24‚1 Well-Plate-96‚ Bag-CK1 1 Pipet‚ Empty Short Stem‚ Experiment Bag Ionic Reactions 1 Barium Nitrate‚ 0.1 M - 2 mL in Pipet‚ 1 Cobalt (II) Nitrate‚ 0.1 M - 2 mL in Pipet1 Copper (II) Nitrate‚ 0.1 M - 2 mL in Pipet‚ 1 Iron (III) Nitrate‚ 0.1 M - 2.5 mL in Pipet‚ 1 Nickel (II) Nitrate‚ 0.1 M - 2 mL in Pipet‚ 1 Sodium Bicarbonate‚ 0.1 M - 2 mL in‚ Pipet‚ 1 Sodium Carbonate‚ 0.1 M -
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insoluble we can check the chart in the textbook containing solubility rules and tables. The goal of the experiment is to study and observe the nature of ionic reactions. Procedures: Perform the following actions in the 96-well plate. Place 2 drops of cobalt (II) nitrate solution into seven of the A row wells. Place 2 drops of copper (II) nitrate into seven of the B wells. Place 2 drops of iron (III) nitrate into seven of the C wells. Place 2 drops of barium nitrate into seven of the D wells. Place
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Perolles‚ CH-1700 Fribourg‚ Switzerland ´ ´ Abstract Carbon nanotube composite materials were produced by catalytic decomposition of gaseous carbon sources Žsuch as carbon monoxide or hydrocarbons. on nanometer-size metal clusters of iron‚ cobalt and nickel embedded in matrices of inert metal oxide particles. The resulting multiwalled carbon nanotubes are several micrometers long with tube diameters ranging from 5 to 20 nm. A fluidised bed reactor was developed for a large-scale synthesis
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Guide Questions Experiment 1 Calibration of the calorimeter: 1. Give the net ionic thermochemical equation of the reaction used to calibrate the calorimeter. a. Is the reaction endothermic or exothermic? b. Which is the limiting reactant? c. How much (in moles) limiting reactant was used? d. How much heat was generated (or absorbed) by the reaction? 2. Relate the sign of the ΔT to the ΔH of the reaction used for calibration. 3. What is the heat capacity of the calorimeter? Relate
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