Simple Distillation Experimental Organic Chemistry: A Miniscale and Microscale Approach. 4th Edition. By Gilbert and Martin. Section: 4.4 Introduction: Distillation is a technique used to purify various liquids. In a simple distillation‚ a liquid is boiled and the vapors work through the apparatus until they reach the condenser where they are cooled and reliquified. Liquids are separated based upon their differences in boiling point in which each pure substance is at least greater than 40-50
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Chemistry 3373F Lab Manual 2008 Modified 11/07 Table of Contents Chem 3373 Laboratory Schedule for Fall 2008.............................................................................2 The Benzoin Condensation of Benzaldehyde ..............................................................................3 Synthesis of Dilantin and Related Compounds (two weeks).........................................................6 Synthesis of an Alkaloid: Pseudopelletierine (two weeks) .............
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4.3.8 Cause and Effect Essay How Water Vapor and Clouds Cause Rain It’s a rainy day! Have you ever thought about how rain is formed? The process by which water vapor and clouds cause rain will be explained here. Water vapor and clouds are key elements in the production of rain. The process in which water travels from the earth to the air and‚ eventually‚ back to the earth again is called the water cycle. In this cycle‚ there is a chain of ev
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unconscious when the mind redirects a thought or word dangerous or unacceptable and substitutes it with a more affable thought or word. Condensation; where all the different elements‚ bits and pieces of thought and dreams combine into one to make sense. In this way they can stand for several different thoughts‚ feelings‚ wishes‚ ideas‚ etc. For Freud‚ condensation and displacement / substitution were used as a defense mechanism to contain aggressive and sexual impulses and hide the true unconscious
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this experiment is to be able to conduct an aldol condensation reaction using an unknown aldehyde and an unknown ketone. H NMR is used to identify the unknown aldehyde and ketone. Melting point is used to identify the aldol condensation reaction. Theory: Condensation reaction is also known as a dehydration reaction. In the mechanism of condensation reaction‚ a bond is formed between two molecules and creates water as a byproduct. Aldol condensation is a C-C bond forming reaction between the alpha
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Experiment: Preparation and Identification of Dibenzylidene Acetone Purpose: Prepare dibenzylidene acetone by the famous Claisen-Schmidt condensation reaction. Learn the experimental skills of organic synthesis‚ separation‚ purification‚ structural characterization by instrumental analysis. Train the ability to solve the practical problems. Principle: Aromatic aldehydes can have aldol reaction with aldehydes or ketones which have α-hydrogen atoms‚ dehydrate to form high yield of α‚β-unsaturated
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takes place. Actually this reaction is a combination of two reactions. One is ’Michael Addition ’ and the other is ’Aldol Condensation ’. Robinson Annulation Mechanism In the first step‚ Micheal addition takes place to an α‚β-unsaturated ketone. Enolate is formed and tautomerization takes place for further reaction. Cyclization takes place. That is‚ aldol condensation reaction to form six-membered cyclic product. Further hydrolysis results in the formation of α‚β-unsaturated cyclic ketones
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Aldol Condensation: Synthesis of Dibenzalacetone Aldol Condensation: Synthesis of Dibenzalacetone Leah Monroe May 15‚ 2003 Organic Chemistry Lab II Experiment performed on May 6 and 8‚ 2003 Abstract: The purpose of this experiment was to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde. This was done by mixing the two reactants with NaOH and ethanol‚ then allowing the reaction to sit for thirty minutes. The crystals were then washed with
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carbonyl groups. One technique used was Doebner reaction and the other technique used was Claisen-Schmidt reaction. Therefore the aim of this experiment is to synthesize trans p-methoxycinnamic acid and to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde. The products would be recrystallized using ethanol‚ then characterized using melting point analysis. Introduction: In this experiment we learnt on carbonyl compounds‚ enols and enolates. We also learnt
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ketone (1‚3-diphenyl-2-propanone) with benzil in the presence of base. The reaction then proceeded with an aldol condensation reaction.5 This product was obtained using extraction (reflux)‚ recrystallization and vacuum filtration to separate the product from the waste. Experiment Scheme: Figure 1: Experiment Reaction5 Figure 2: Step wise reaction mechanism including aldol condensation reaction5 Procedure: About 1.55-g of benzil‚ 1.51-g of dibenzylketone and 12-mL of ethanol were placed in a 50-mL
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