Reactions: Procedure: 1. Measure 120 mg of 1‚4-dimethoxybenzene‚ 0.4 mL acetic acid‚ and 0.2 mL t-butyl alcohol 2. In a 10X100 mm reaction tube‚ dissolve the120 mg of 1‚4-dimethoxybenzene in the 0.4 mL of acetic acid. 3. Gently warm the solution within the reaction tube‚ it may be necessary to agitate the solution with a glass stirring rod and add the 0.2 mL of t-butyl alcohol 4. Cool the solution in an ice bath‚ once the solution is sufficiently cooled‚ place the reaction tube
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alcohols are oxidized to ketones. Tertiary alcohols are not oxidized at all by the reagent. Hence‚ this reaction can be used to distinguish tertiary alcohols form primary and secondary alcohols. Procedures: 1. Place ethanol‚ isopropyl alcohol and tert-butyl alcohol in three different test tubes. Label them accordingly. 2. Add potassium dichromate solution to each of the test tube. Mix thoroughly. 3. Cautiously add concentrated sulfuric acid and mix. 4. Observe the change in color of
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Experiment No. 1: MELTING POINT AND BOILING POINTS OF ORGANIC COMPOUNDS ABSTRACT The properties of organic compounds depend on their chemical structures. Intermolecular forces of attraction affect physical properties such as melting and boiling point. Through the Thomas Hoover apparatus‚ the melting point of 8 test compounds was determined. Salicylic acid exhibited the highest melting point while naphthalene‚ the lowest. The stronger the intermolecular forces of attraction‚ the higher the melting
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Chemical Water Quality Sarah Tilly Table of Contents 1. Introduction 2. Methods 3.1 Figures 3.2.1 Figure 1. Satellite Image from Google Maps of collection site in Stephenville City Park (Google‚ 2013). 3.2.2 Figure 2. Pictures I took of collection site taken on April 7th‚ 2013 3.2 Tables 3.3.3 Table 1. Quick reference guide—water-sample collection methods‚ preservation‚ storage‚ and handling. 3. Results 4.3 Tables 4.4.4
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Mapua Institute of Technology School of Chemical Engineering and Chemistry Muralla St.‚ Intramuros‚ Manila Melting Point and Boiling Point of Organic Compounds Group No. 5 Manacup‚ Cris Vincent L. Oblena‚ Adrian D. Ong‚ Joshua Jyro B.* *Leader ABSTRACT In compounds‚ two of the physical properties affected by the varying structures are melting point and boiling point. Through the use of the Thomas-Hoover Melting Point Apparatus or the micro method‚ the melting and boiling point of
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Introduction to Alkane Nomenclature A. Determining the Priority of Functional Groups. What’s in a name? 3-ethyl-5-(1-methylpropyl)-4‚4-dimethylnonane Too big a subject to cover on one sheet! This paper will focus on alkanes. Determining functional group priority will be the subject of a subsequent sheet. suffix http://masterorganicchemistry.com D. Applying the Lowest Locator Rule F. Dealing With Branched Substituents (the IUPAC Way) Number the chain from one end so as
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Social Alchemy 2nd Quarter / SY 2012 – 2013 Eng’r. Josephine A. Ng CHM142L/B21 Concepcion‚ Jermin B. Group# 2 Experiment No. 1 ------------------------------------------------- MELTING POINT AND BOILING POINT OF ORGANIC COMPOUNDS ------------------------------------------------- ABSTRACT The melting point (MP) and the boiling point (BP) are probably the most widely used physical constant in the field of science. Determining the boiling point and the melting point of a compound helps you to characterize
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NAME OF COURSE COURSE CODE CREDIT TOTAL STUDENT LEARNING HOURS PREREQUISITE LEARNING OUTCOME : : : : Organic Chemistry I CHM 3201 4 (3+1) 160 hours per semester : : None At the end of the course‚ students will be able to: 1. Define and explain the basic concepts in organic chemistry such as electronegativity‚ orbital hybridization‚ nomenclature‚ resonance and isomerism‚ as well as organic reactions mechanisms (C4‚ CTPS) 2. to conduct experiments that demonstrate the characteristic reactions
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Thus a solution α-naphthol 1a‚ 4-methylbenzaldehyde 2a and tert-butyl isocyanide 3a in EtOH was magnetically stirred at 45 C for 12 hours under an oxygen atmosphere with an equimolar ratio of the three reactants. TLC monitoring of the reaction mixture exhibited formation of a new product‚ which was purified (Table 1‚ entry 1). Identification of its structure by NMR spectroscopy revealed that it was 2-(4-methylbenzoyl)-1-naphthyl N-(tert-butyl)carbamate (4a). Next‚ in order to improve the yield of 4a
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by : Directorate of Education‚ Delhi SOME IMPORTANT REASONING BASED QUESTIONS OF ORGANIC CHEMISTRY 1. Chlorobenzene is less reactive than chloromethane. Ans. In chlorobenzene‚ each carbon atom of benzenering is sp2 hyridised and is electron withdrawing. Chlorine atom donates a lone pair of electron and acquire positive charge. The negative charge is delocalised on ortho and para position by resonance. C-Cl bond acquires partial double bond character and is 169 pm as compared to 17.0 pm in chloromethane
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