Experiment #1: Separation of Acid‚ Base‚ and Neutral Compounds from a Solid Mixture by Liquid-Liquid Extraction Introduction Liquid-liquid extraction is a technique used to separate chemical substances in order to purify or identify the various components of a mixture. Flavors‚ spices‚ perfumes‚ and medicines are just some of the everyday things that are extracted from plants and other natural sources [1]. The basic principle used to carry out this separation is the mixing of two liquids that are immiscible
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Experiment II. Separation Of a Sample Mixture By Liquid-Liquid Extraction Reading assignment: Techniques in Organic Chemistry 2nd ed pages 75-99. 3rd ed pages 113-140. Topics and Techniques i) identification of solvent layers of two immiscible solvents ii) partioning of a compound between two immiscible solvents and determination of KD iii) liquid-liquid extraction with aqueous acids and bases with organic solvents. iv) use of drying agents Introduction Liquid-liquid extraction is a method used
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Experiment Separation of Organic Compounds by Acid-Base Extraction Techniques 5 A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require extraction at some stage of product purification. In this experiment you will use extraction techniques to separate a mixture of an organic acid‚ a base‚ and a neutral compound. Organic acids and bases can be separated from each other and from neutral compounds by extraction
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Experiment 3 Liquid-Liquid Extraction Discussion The success of extracting each compound out of the solution can be seen in the IR graphs for each substance. For ethyl 4-aminobenzoate‚ the N-H‚ C=O and C-O are distinguishable in their proper wavenumber positions. The amino N-H stretch was found between 3224 cm-1 and 3423 cm-1. The C=O was found at 1681 cm-1 and the C-O was at 1280 cm-1. The IR for benzoic acid also displays its significant bonds‚ O-H and C=O. The O-H was between 2566 and
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Experiment 2: Acid- Base Extraction Separation of an Organic Acid‚ a Base and a Neutral Compound Introduction: The extraction technique is often used in the organic lab to separate organic compounds from mixtures. One type of an extraction technique is the acid-base extraction‚ which is used to separate organic compounds from a mixture based on their acid-base properties.1 There are certain principles that must be taken into account when choosing a solvent system to perform an extraction. The solvents
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– CHEMICAL ENGINEERING LABORATORY PROJECT TITLE: SOLID LIQUID EXTRACTION OF GANODERMA LUCIDUM NAME: WIJETUNGE MUDALIGE DINITHI ISHARA WIJETUNGE ID NO: 007118 SUPERVISOR: DR SIVAKUMAR MANICKAM GROUP MEMBERS: KOW NIEN WEI AAZRA OUMAYYAH PANKAN JASON HEW YIP SENG DATE: 30 APRIL 2012 H83 CEL Chemical Engineering Laboratory Solid Liquid Extraction of Ganoderma Lucidum Author: W.M.Dinithi Ishara Wijetunge I certify that: (i) Apart from the experimental results reported in the lab notebook
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The Separation of a Liquid Mixture by Simple Distillation Objective The purpose of doing this experiment is to separate two miscible liquids samples of cyclohexane and toluene using simple distillation. The objectives will be to record boiling range and volumes (mL) of distillates that are attained during the process of distillation. Background Distillation is a frequently used technique for separating mixtures based on differences in the boiling points of components in the mixture. The
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Liquids & Solids Pre Lab Questions: 3pts 1. What are the learning goals of this lab? The learning goal of this experiment is to view and experience the melting point and boiling point of different substances. 2. Why is acetamide not allowed in contact with your skin? What precautions does one have to take to work with this chemical? Acetamide is a carcinogen‚ which can cause cancer. Therefore‚ it should not be allowed to come in contact with a person’s skin. Any person working with this chemical
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Name:Shin Park|Date:06/14/2013| Exp 5: Liquids and Solids|Lab Section: | Data Table: Boiling Point Trial 1 Trial 2 Trial 3 Temperature when the last bubble has emerged ___83_˚C __82__˚C __82__˚C Average temperature from all three trials ___82.33_˚C % error ___.0849_% Melting Point Trial 1 Trial 2 Trial 3 Temperature when the acetamide melts __82__˚C _81___˚C __82__˚C Average temperature from all three trials ___81.66_˚C % error
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Date of Experiment October 7‚ 2012 Report Submitted: October 7‚ 2012 Title: Liquids and Solids Purpose: The purpose of this experiment is to determine the boiling point of liquids and the melting point of solids. Procedure: I got all of my materials together and set up. I poured rubbing alcohol in a beaker and rubber banded it with the thermometer. I logged the last bubble that came out of the capillary tubes. After that I crushed the acetamide and carefully put it in the capillary tube
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