High Performance Liquid Chromatography Analysis of Aspirin Problem: Was aspirin (acetylsalicylic acid) successfully synthesized? Are there impurities or by-products present in the synthesized aspirin? How pure is the synthesized aspirin? Introduction: In the last experiment‚ aspirin was synthesized followed by characterization of the product using several different techniques. Melting point was a test that provided information about the identity and purity of the aspirin product. The iron(III)chloride
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Standard Reduction Potentials‚ Equilibrium Constants and Investigating a Lead-Acid Electrolytic Cell Purpose Experimental Methods All procedures were followed according to the lab manual (experiment 10 – Electrochemistry Laboratory). Data and Observations Part A: Grams of FeSO4 used: 0.759 Voltage during voltmeter and battery check: 9.23V Table 1. Electrochemical Cells Data Part B: Table 2. Lead-Acid Battery Results and Calculations In order to make 5ml of 1M FeSO4(aq)
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Aspirin is prepared by the esterification of salicylic acid with acetic anhydride under acidic conditions. The phenol group in salicylic acid is replaced by a carboxyl group through electrophilic substitution. The mechanism for the reaction can be summarized as follows: Figure 11.4. Mechanism for the reaction of salicylic acid and acetic anhydride to form acetylsalicylic acid (aspirin) In this experiment‚ 85% phosphoric acid (H3PO4)‚ a strong acid‚ is used as a catalyst to speed up the reaction
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Experiment Four: Organic Synthesis of Aspirin Abstract The purpose of this experiment is to synthesize a common organic product called acetylsalicylic acid (aspirin)‚ and to become familiar with the optimum conditions needed for successful yields. Aspirin is produced from an acid catalyzed reaction between salicylic acid with acetic anhydride. The crystalline aspirin is synthesized and purified by recrystallization‚ although there is not a hundred percent yield due to sources of error. Introduction
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Y ou may have heard that omega 3 fatty acids can actually play a role in the treatment and prevention of depression. Does the rumor reign true? Can consuming omega 3 fatty acids really help fight depression? This article will give you all the information you need to know on the hot topic of omega 3 fatty acids and depression. To begin‚ we will start by explaining what omega 3 fatty acids are. Omega 3 fatty acids are essential fatty acids. This means that they are vital for human health. However
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Synthesis of Aspirin (Acetylsalicylic Acid) Abstract: This experiment is about the synthesis of aspirin under laboratory conditions. Aspirin is prepared by reacting salicylic acid and acetic anhydride; in the presence of sulfuric acid. After fully dissolving the salicylic acid with acetic anhydride‚ the solution is cooled and cold water is then added. Once the crystals form they are then filtered and left to dry out. There mass is measured and recorded then the yield is calculated. Introduction:
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acetylsalicylic acid (aspirin) by creating a reaction between acetic anhydride and salicylic acid. This was be accomplished through the use of recrystallization. Acetic anhydride and salicylic acid are mixed together‚ and then acidified by the addition of a few drops of concentrated sulfuric acid‚ which catalyzed the reaction. The percent yield is calculated to determine the effectiveness of the reaction in preparing the desired product (aspirin). The limiting reactant of the equation was salicylic acid. After
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Chemistry Laboratory I Acid Base Review Definition In general‚ an acid is a substance that can donate a proton (H+) and a base is a substance that can accept a proton. Any proton in an organic molecule can potentially be donated. The most acidic proton in a molecule would be donated first. Any lone pair in an organic molecule can act as the proton acceptor. An acid (HA) reacts with a base (in this case H2O) to form the conjugate base of the acid (A-) and the conjugate acid of the base (H3O+).
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Lab Report Introduction This lab has the following two concepts: synthesis of acetylsalicylic acid and analysis of acetylsalicylic acid. Synthesis is a purposeful execution of chemical reactions to obtain a product. This concept is used in the first part of the lab; when we have to produce crystals of aspirin. Analysis is the separation‚ identification‚ and quantification of the chemical components of natural and artificial materials. This concept is used throughout the lab when we are analyzing
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(ACETYLSALICYLIC ACID) Aim: The aim of this experiment was to react salicylic acid with ethanoic anhydride to produce Aspirin. CH3CO)2O + HOC6H4COOH → CH3CO2C6H4CO2H + CH3COOH i Mass: 5g Volume: 7.5 cm3 Mass: 6.52g RMM: 138g/mol RMM: 180g/mol Moles: 5/138 = 0.0362 RMM: 102g/mol Moles: 0.0362 OBSERVATIONS – First‚ Ethanoic acid was added to the salicylic acid which resulted in a cloudy solution. When adding a few drops of concentrated sulfuric acid‚ which acted as
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