Synthesis of Butyl Benzoate Using Phase Transfer Catalysis The objective of the experiment is to synthesize the butly benzoate by nucleophilic substitution and characterize it by IR spectroscopy. The percent yield of the final product is determined after the synthesis. Procedures: 2.0 mL of 1-bromobutane‚ 3.0 g of sodium benzoate‚ 5.0 mL of water‚ 4 drops of Aliquat 336‚ and a boiling stone were placed in a 50mL round-bottomed flask. The reaction mixture was refluxed for 1 hour and the flask
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1779 Microcontroller-Based High-Power-Factor Electronic Ballast to Supply Metal Halide Lamps Marco Antonio Dalla Costa‚ Member‚ IEEE‚ José Marcos Alonso Álvarez‚ Senior Member‚ IEEE‚ Jorge García‚ Member‚ IEEE‚ André Luís Kirsten‚ Associate Member‚ IEEE‚ and David Gacio Vaquero‚ Student Member‚ IEEE Abstract—The analysis‚ design‚ and implementation of a microcontroller-based electronic ballast to supply metal halide (MH) lamps are presented. The proposed topology is based on the integration of
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Experiment 8: Identification of an Adulterated Herb The purpose of this lab is to analyze the volatile oils of some herbs through TLC testing and then identify the adulterant in a sample. Unfortunately‚ we ran out of time to complete the lab; however‚ we were able to get through most of it‚ and were only missing the adulterant. The first step to identify our unknown samples was to create TLC plates that should results with each known compound and 95% hexane: 5% ethyl acetate‚ 90% hexane: 10%
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stoppers (held in large empty beaker) Wooden splint and lit candle Large beaker (500mL to 1L) half full of water Pre-lab Exercise: 1. In this lab we will produce acetylene by placing calcium carbide (CaC2) in water. Write the chemical formula for the reaction between calcium carbide and water knowing that the product is acetylene (C2H2). 2. The acetylene in this lab will be collected in a test tube and burned. Write the balanced equation for the combustion of acetylene. 3. Look at
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African Diaspora and the World After reading the short story “Diaspora” by Joanne Hyppolite‚ I got a vivid understanding of how diaspora can have an effect on one’s identity. Over the past month we have studied many theories and concepts concerning race‚ gender‚ and politics. There are three theories that capture the essence of Joanne Hyppolite’s worldview as a Haitian growing up in America: intersectionality‚ identity‚ and diaspora. Individuals oftentimes experience the theory of Intersectionality
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General College Chemistry LabPaq / Published by: Hands-On Labs‚ Inc. sales@HOLscience.com / www.HOLscience.com / Toll Free 866.206.0773 A Laboratory Manual of Small-Scale Experiments for the Independent Study of General College Chemistry 50-0123-CK-02 LabPaq® is a registered trademark of Hands-On Labs‚ Inc. (HOL). The LabPaq referenced in this manual is produced by Hands-On Labs‚ Inc. which holds and reserves all copyrights on the intellectual properties associated with the LabPaq’s
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r Lab Report 5 Introduction to the Classes of Chemical Reactions Course: Chem. 1151L‚ Tuesday & Thursday June 23‚ 2011 Mr. Nasir Uddin Pre Lab Questions: 1. CaBr2 (aq) + K3PO4 (aq) → CA(PO4)2(S) + KBr (aq) = Ca3(PO4)2 + 6 KBr Double Replacement 2. Li(s) + O2(g) = Li2O(s) =2 Li2O Decomposition 3. CH4 + O2 = CO2 + H2O = CO2 + 2 H2O Combination 4. AgBr(s) = Ag (s) + Br2(l) = 2 Ag + Br2 Combination 5. Mg(s) + H2SO4 (aq) = MgSO4 + H2
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LAB: Comparison of Reactions for Three Isomers of Butanol /23 TI /21 C /6 A Name: /50 MARKS Background: The reactivity of alcohols can be accounted for by their molecular structure – particularly by the attachment of their hydroxyl functional group. The isomers of butanol are used as examples of 1°‚2° and 3° alcohols to examine this relationship. Each of the three isomers of butanol will be mixed with concentrated hydrochloric acid. The presence of an alkyl halide product is
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Lab 5 n-Butyl Bromide Preparation Introduction: The purpose of this lab is to properly extract and distill n-butyl bromide It is ideal to perform this technique with accuracy‚ which can be measured by the percent yield. Chemicals: n-Butyl Bromide- clear‚ yellow liquid that is slightly soluble in water. Molar weight of 137.02g and has zero reactivity. Sodium Bromide- white‚ crystals‚ granules. Soluble in water with no reactivity. Molar weight of 102.89g. Sulfuric Acid- colorless liquid
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He a lt h 0 3 2 3 Fire 0 Re a c t iv it y 2 P e rs o n a l P ro t e c t io n Material Safety Data Sheet Sulfuric acid MSDS Section 1: Chemical Product and Company Identification Product Name: Sulfuric acid Contact Information: Catalog Codes: SLS2539‚ SLS1741‚ SLS3166‚ SLS2371‚ SLS3793 CAS#: 7664-93-9 Sciencelab.com‚ Inc. 14025 Smith Rd. Houston‚ Texas 77396 RTECS: WS5600000 US Sales: 1-800-901-7247 International Sales: 1-281-441-4400 TSCA: TSCA
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