Introduction The purpose of the experiment was to determine the melting points of compounds using a Mel-Temp device. The melting point of naphthalene‚ urea‚ and sulfanilamide are found. This is then followed by the measuring of an unknown compound‚ and an impure sample (a small amount of naphthalene mixed with the unknown). Experiment In the lab‚ the height of the chemical in the capillary was set to 2-3 mm thickness. The voltage at the Mel-Temp started at a low setting of 1.5-2. The heat was
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Freezing Point of Naphthalene I. Purpose To determine the freezing point of a known substance‚ naphthalene II. Materials ringstand gas source test tube test tube clamps thermometer naphthalene Bunsen burner goggles hose stopwatch III. Procedure 1. Assemble the Bunsen burner‚ attaching one end of the hose to the burner and the other to a gas source. 2. Assemble the ring stand so that a ring clamp is attached to the stand holding the test
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Melting Point Determination Identity and Purity of Solid Organic Compounds Objectives • To introduce the technique of melting point determination. • To use the concept of melting points for identification and characterization of organic compounds. • Properly fill and use a capillary melting point tube. • Determine accurate melting point ranges for a wide variety of organic substances. Introduction The melting point of a solid can easily and accurately be determined
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10‚ 2014 Lab # 4: Melting Point lab Partner: Instructor: The Testing of the Melting Points of p-dichlorobenzene and naphthalene Introduction: Melting point temperature is a physical property of pure substances. It is an intensive property‚ which means the amount of material tested is irrelevant. This lab will determine the melting point temperatures of two known pure substances‚ naphthalene and p-dichlorobenzene‚ using micro-sized quantities and a capillary melting tube apparatus. The
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Mixture Melting Points Abstraction Determining the melting point is very significant in order to identify an unknown. In this experiment‚ measuring the melting point was done by using melting point apparatus. The melting point of the unknown sample #10 was 111.5˚C. There were two possible compounds which were dibenzoyl ethylene and o-Toluic acid because their melting points were 111.2˚C and 109.8˚C when each compound was mixed with the unknown. Therefore‚ the unknown #10 was dibenzoyl ethylene
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Introduction The melting point is defined as the temperature at which the solid is in equilibrium with its liquid‚ and this characteristic is very unique‚ so a substance can be determined by the melting point. Determination of the melting point is very important technique in many areas of chemistry especially‚ in organic chemistry area because the melting point is really significant in order to identify the purity and the identity of a substance. Measuring the melting point is a fast and cost-effective
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Lab/ Chem 234 02/17/13 Lab 2: Melting Points Purpose: To determine the purity of a substance using melting point as physical property. We must also learn how to identify an unknown compound using its melting point. We got to identify an unknown compound using mixture melting point and finally we must learn to obtain an accurate melting point using Mel-Temp apparatus. Procedure: Set voltage to obtain the desired heating rate at the anticipated melting point range. The voltage control controls
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Melting Point Determination Lab Materials: Graduated pipette Capillary tube Tin wipe Sample Melting temperature apparatus Thermometer Procedure: Take open end of capillary tube and tap it gently into sample. Take tin wipe and place over the opening. Gently tab it so the sample will funnel to the bottom of the tube. You may also use a graduated pipette to accomplish this. Now‚ place the capillary tube in the designated spot in the melting apparatus‚ and once placed‚ turn the apparatus
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Melting Point Determination and Thermometer Calibration Lab Background: The melting point of a substance‚ a solid in this case‚ signifies the temperature at which the first crystal starts to melt until the temperature at which the last crystal disappears is reached. That being said‚ melting points are expressed in ranges‚ am organic compound will have a sharp range depending on the purity of the compound. Impurity of an organic substance will register an abnormal melting point based on its
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Engineering and Chemistry Muralla St.‚ Intramuros‚ Manila Melting Point and Boiling Point of Organic Compounds Group No. 5 Manacup‚ Cris Vincent L. Oblena‚ Adrian D. Ong‚ Joshua Jyro B.* *Leader ABSTRACT In compounds‚ two of the physical properties affected by the varying structures are melting point and boiling point. Through the use of the Thomas-Hoover Melting Point Apparatus or the micro method‚ the melting and boiling point of organic compounds are now determined. The aim of this
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