CP4001: ANALYTICAL & PHYSICAL CHEMISTRY | | Formal Report of the Quantitative Determination of Sulphate by Gravimetric Analysis (Experiment 4) | Maryjo Lee Wei Min 1111107 DBS/FT/1A/01 | (A) Synopsis The amount of sulphate is determined quantitatively as barium sulphate by gravimetric analysis. This determination consists of slowly adding a dilute solution of barium chloride to a hot‚ unknown sulphate solution which is slightly acidified with concentrated hydrochloric acid. A white precipitate
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t-Pentyl Chloride is a compound that is created through an SN1 nucleophilic substitution reaction in addition with Hydrogen Chloride in order to isolate the product. A variety of procedural techniques were utilized during the experiment including extraction‚ washing liquids‚ drying liquids‚ gravity filtration‚ and simple distillation. When a single solute or compound is transferred between two different solutes‚ it is known as extraction. Another technique that was utilized was washing‚ in which
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Gravimetric Determination of Calcium ABSTRACT Determining the mass of a pure compound is a method of a gravimetric analysis. One of the gravimetric analyses is the precipitation; it is a method of separating the analyte from the unknown sample as a precipitate where it will be filtered and converted into a known composition that can be weighed to determine its mass (Skoog et al‚ 2013). Determining the mass of calcium by using gravimetric analysis was the objective of the experiment. A 25 mL
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In order to find the formula of the copper chloride hydrate‚ we had to separate the compound to find the mass of water and copper. To begin this process‚ we evaporated the water and created an anhydrous compound‚ meaning we were left with only CuxCly. By calculating the weight of both the anhydrous and the hydrated compounds‚ we could conclude that the difference in the weights was the weight of the H2O. From this we were able to calculate the percent composition of CuxCly and H2O (see Calculations:
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Phuong Pham Prof. Johnson Lab 3 Gravimetric determination of Calcium as CaC2O4.H2O Feb‚ 27‚ 2014 I. Objective: The purpose of this lab is to determine how well gravimetric method measures the calcium level in a solution of known calcium concentration. II. Method: a) Overview: In this lab we will prepare 25 mL known concentration Calcium solutions. Then we will use Gravimetric method to determine the concentration of Calcium in each solution to figure out how well this method is. As we know
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THE GRAVIMETRIC DETERMINATION OF SULFATE Learning Goals. 1. To determine the amount of Sulfate in an Unknown sulphate sample. 2. To perform and develop skills in precipitation Gravimetric method of quantitative analysis. DISCUSSION: Gravimetric analysis is one of the oldest analytical techniques and for this reason is referred to as a "classical method." Gravimetric procedures are usually very accurate‚ but more tedious than other methods. The only major equipment needed
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Experiment 5 Gravimetric Determination of Sulfate Eisman E. Morales TA: Jackeline Pennywiit Chemistry 121 02/14/2011 Purpose: To determine the percent sulfate in a sample using a semimicro scale gravimetric procedure. Procedure: Refer to pages 41-42 of General Chemistry volume 1 Laboratory Experiments by Judith Casey and Robert Tatz‚ Hayden McNeil Publishing‚ 2010 Report Sheet See attached report sheet. Report Questions 1. Explain how your calculated value for percent
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Chem 102 - Lab #2 Quantitative Analysis of a Soluble Sulfate Steven English Lab Instructor: Dr. Campo Date: Tuesday‚ February 5th 2013 Pre-Lab Questions A. Adding the acid to the sodium sulfate solution results in an increase in the solubility of any free anions present in the sample. This will happen because the present anions will bind with the hydrogen cations present in the acid. B. The sodium sulfate is boiled because experiments have shown that barium sulfate is 50
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Sodium chloride‚ also known as salt‚ common salt‚ table salt‚ or halite‚ is an ionic compound with the formula NaCl. Sodium chloride is the salt most responsible for the salinity of the ocean and of the extracellular fluid of many multicellular organisms. As the major ingredient in edible salt‚ it is commonly used as a condiment and food preservative. [edit] Properties Thermal conductivity of pure NaCl as a function of temperature has a maximum of 2.03 W/(cm K) at 8 K and decreases to 0.069 at 314
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GRAVIMETRIC DETERMINATION OF SULFATE Purpose You will be given a solid powder‚ which has been dried to constant mass. The sample is water soluble. The purpose of this experiment is to determine the concentration of sulfate in your solid sample using gravimetric analysis. Background Gravimetric Analysis The goal of most quantitative chemical analysis measurements is to estimate the relative abundance of an analyte in a chemical sample. For solid and liquid samples‚ a very common expression
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