Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5% and
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objective of the experiment was to prepare Benzilic acid by multistep synthesis starting with benzaldehyde. In this setup however‚ product of the first step‚ Benzoin‚ is provided thereby omitting the first step involving the conversion of benzaldehyde. For this experiment‚ the microscale techniques of reflux‚ crystallization‚ and melting-point determination were used. Utilizing these techniques a product yield of 93% for benzil and 57% for Benzilic acid was obtained‚ as well as a melting point range
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Spectra Analysis Organic Chemistry Lab‚ CHEM 369 The University of Tennessee‚ Knoxville Dr. Smith Spectra 1: tert-butyl cyanoacetate Molecular formula: 141/13 = 10 R 11 => C10H10+11 => C10H21 C10H21NO2 – C3H10 = C7H11NO2 DBE: 2(#C - #H/2 - #X/2 + #N + 2)/2 =2(7 – 11/2 – 0/2 + 1 + 2)/2 = 3=> 1 double bond and 1 triple bond Mass spectrum table: m/z fragment |40
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Chapter 13—Chromosomal Rearrangements and Changes in Chromosome Number Reshape Eukaryote Genomes Fill in the Blank |1. |Events that reshape genomes by reorganizing the DNA sequences within one or more chromosomes are known as ____________________. | |Ans: |rearrangements | | |Difficulty: 2
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by everyday pollution from houses‚ factories‚ cars‚ and etc. This is the concept of acid rain‚ which according to EPA.gov is a broad term referring to a mixture of wet and dry deposition from the atmosphere containing higher than normal amounts of nitric and sulfuric acids. Acid rain isn’t just rain‚ its forms like hail or snow‚ which is wet deposition‚ and smoke or dust‚ which is dry deposition. The effects of acid rain are quite terrifying bringing all types of problems to the Earth‚ for example
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Acid Base Titration bre’ana March 1‚ 2013 Purpose: The purpose of this experiment is to determine the concentration of a solution of NaOH by titration with a standard solution of HCl. It was also the purpose to determine the concentration of a sample of white vinegar by titration with a standard solution of NaOH. Introduction: Using the method of titration is how the experiment gets to the conclusion of the concentration of a solution. When doing this experiment‚ measurement is very important
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Advantages: Sulfamic acid is the fastest de-scaler - It dissociates into hydroxonium ions more readily in aqueous solution than the others‚ therefore giving a greater concentration of atoms that are able to react with the calcium in lime scale. It is safe to use because it does not produce chlorine gas [5]‚ which can be toxic. Sulfamic acid also has a low volatility. Disadvantages: Sulfamic Acid can be an irritant to eyes or skin and is the most expensive of the de-scalers. Q2) How these de-scalers
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Exercise No. 8 CARBOXYLIC ACIDS AND ACID DERIVATIVES I. OBJECTIVES: • To investigate the physical and chemical properties of Carboxylic acid and its derivatives • To understand the reactions of carboxylic compounds and derivatives. II. EXPERIMENTAL RESULTS Solubility of Carboxylic acids in 10% NaHCO¬3 Acetic acid - formation of bubbles Benzoic acid - formation of bubbles Test for Acetic acid NaOH + Acetic acid - blue litmus paper turned red NaOH + Acetic acid + FeCl3 - red colored
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used (ml) | 30.6 | 30.2 | 30.0 | | | | | Acid to Base Ratio | 0.87 | 0.86 | 0.86 | Average acid/base ratio | 0.86 | | | | | Base to Acid Ratio | 1.14 | 1.16 | 1.17 | Average base/acid Ratio | 1.16 | Name: Jared Philip Condez Date Performed: June 28‚ July 2 & 5‚ 2013 Partner: Shiela Mae Molina Date Submitted: July 12‚ 2013 Experiment 3 ACID – BASE TITRATION I. Objectives * Determine the purity of Potassium Acid Phthalate * To titrate effectively
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Formic acid is known to be the simplest carboxylic acid‚ and it is an important factor in chemical synthesis and occurs naturally. The chemical formula for Formic Acid is CH202‚ and is mostly found in the venom of bee and ant stings. Formic acid is clear and colorless with a pungent odor. Formic acid is used in many ways; Formic acid is used to preserve livestock. It is also sprayed on animal food and fresh hay to reduce the decay rate. It can also be used as a pesticide to protect bee
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