Preparation and melting point of Aspirin Aspirin is a painkilling drug and is produced worldwide to reduce and stop pain. Aspirin is made up of ehtanoylation of 2-hydroxbenzenecarboxylic acid in a presence of phosphoric acid. AIM: The aim of the experiment is to prepare and produce aspirin as pure as possible. I will do this threw preparing the aspirin and purifying the product threw recrystallization. I will then obtain a melting point of my product to get an estimate of its purity. By the end
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experiment‚ synthesis of copper compounds‚ the purpose was to recover the original amount of copper after series of chemical reactions. Then returning the copper back to its original form. The copper wire originally weighted 1.0099 g‚ but after the copper was transformed into Cu(OH)2 to CuO to CuSO4 and finally into Cu‚ the mass of the recovered copper was 1.1023g; the percent yield was 109%. Since the percent yield is more than 100%‚ an error must have occurred somewhere in the lab. A possible error
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UNIVERSITY OF WATERLOO Department of Chemistry Synthesis of ACETAMINOPHEN Laboratory Report 1 CHEM 123L January 19‚ 2014 Prepared for: Dr. S. Stathopulos Department of Sciences‚ Chemistry Faculty University of Waterloo Teaching Assistant: Aaron Chan Prepared by: Section 001 Vithurjan Satkunarasan 20495383 Lab Partner: Ken Xu Introduction The synthesis of Acetaminophen is based on the amine group of p-aminophenol being acetylated by acetic anhydride to form an amide functional group
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Synthesis of Benzoin Date of Experiment: 1-26-15 Chelsea Price Lab Partner: Joey Simmons Abstract: In this experiment‚ benzoin was synthesized from benzaldehyde‚ using thiamine hydrochloric acid as a catalyst. The thiamine HCl was deprotonated by sodium hydroxide and acted as a nucleophile to attack the benzaldehyde. A water-cooled condenser was used to heat the solution at reflux. Vacuum filtration was used to wash and dry the product. The benzoin product was recrystallized
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For this lab‚ 40.2 mL of canola oil were used as the initial volume for the production of synthesized biodiesel. Through the synthesis process‚ 31.307 grams of canola biodiesel was produced‚ which is a percentage yield of 85.714%. In order to get this percentage yield‚ the following calculations were made: 40.2 mL canola oil × 0.9073 g1 mL=36.5 g × 1 mol376.6 g=0.0416 moles canola oil From the prelab‚ for every 1 mole of oil‚ 3 moles of biodiesel are produced. 0.0416 mol oil × 3 mol biodiesel1
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ineffective. In order to help resolve the crisis‚ antibiotics were found through screenings of soil microorganisms. However‚ soil microorganism’s antibiotics were depleted by the 1960s and their antibiotic effects were unable to be replicated through synthesis. In this experiment‚ the researchers developed numerous methods to cultivate uncultured organisms in their environment. The goal of this experiment was to find antimicrobials in the uncultured soil. Through this successful experiment‚ the researchers
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Soluble aspirin tablets Adult dosage: To treat pain or fever in adults‚ the recommended dose is 325 mg to 650 mg every 4 to 6 hours as needed. The maximum daily dose is 4‚000 mg‚ unless otherwise directed by your doctor. For adults with conditions caused by inflammation such as rheumatoid arthritis‚the usual dose is 975 mg 4 to 6 times daily on a regular basis. Sometimes‚ higher doses may be used. To treat migraine headache pain‚ the recommended adult dose is 1‚000 mg at the onset of pain or
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Once the aspirin is prepared‚ it is isolated from the reaction solution and then it is purified. The aspirin is insoluble in cold water‚ and it is isolated by filtering the chilled reaction solution. Purification is essential to remove any unreacted salicylic acid and acetic anhydride as well as the acetic acid product and phosphoric acid. Acetic anhydride is caused to decompose by the addition of water once the formation of aspirin is complete. C4H6O3 (Acetic anhydride) + H2O (Water) ------------------------->
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A small amount of the unknown (approximately the tip of the spatula was used for all the pigments) was added into each clean dry test tube. For the first test 1 mL of 3 M of HNO3 was added. As soon as the acid came into with the solid‚ the pigment was observed to dissolve while also turning the solution into a pale clear colour. The same amount was used for the HCl reagent. As soon as the acid touched the pigment it yielded in a clear solution (solid dissolved after a few shakes). When the KI was
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In this lab we employed various assays utilizing a biuret reagent‚ coomassie brilliant blue reagent‚ and ultraviolet light in order to determine the identity of six unknown solutions and the concentration of a bovine serum albumin sample. We were given three samples that lacked protein‚ and three samples containing proteins‚ and using a spectrophotometer we assessed the amount of light absorbed versus the light transmitted‚ based on the principles of the Beer-Lambert Law. The three proteins used
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