Reactions of Three Isomers of Butanol Purpose: To test the reactions of primary‚ secondary‚ and tertiary alcohols with acid and with an oxidizing agent. Equipment and Materials: Chemical safety goggles Lab apron Protective gloves 3 test tubes Test-tube rack Eyedropper Dropper bottles containing the following Butan-1-ol Butan-2-ol 2-methylpropan-2-ol Potassium permanganate solution‚ KMnO4(aq) (0.01 mol/L) Concentrated hydrochloric acid‚ HCl(aq) (12 mol/L) *Alcohols are flammable and
Premium Potassium permanganate Alcohol Hydrochloric acid
Synthesis of 1-Bromobutane from 1-Butanol Reference: Discovering Organic Chemistry in the Laboratory; John R. Ganson Ph. D‚ Revised 2011 by Alfredo Mellace Ph. D www.Aldrich.com Purpose: To synthesize 1-bromobutane from 1-butanol via SN2 reaction. Alcohols are converted into the alkyl halides adding an aqueous solution sodium bromide. The sulfuric acid acts as a catalyst in converting the OH functional group of butanol‚ to a better leaving group. In order for this reaction to synthesis 1-Bromobutane
Premium Distillation Chemistry Sulfuric acid
Lab: Comparison of Three Isomers of Butanol Pre-lab: 1. Write the general reaction of an alcohol and HCl. 2. What would the solubility be of an alcohol in water. 3. What would the solubility be of an alkyl halide in water? 4. What is the purpose of KMnO4 in the reactions? Safety: Concentrated hydrochloric acid is corrosive and the vapour is very irritating to the respiratory system. Avoid contact with skin‚ eyes‚ clothing‚ and the lab bench. Wear eye protection and a lab apron.
Premium Ethanol Oxygen Chemistry
This lab will allows the comparison between elimination reactions under acidic and basic conditions through an analysis of two separate reactions: an acid-catalyzed dehydration of 1-butanol and 2-butanol using sulfuric acid and a dehydrobromination under basic conditions using potassium tert-butoxide of 1-bromobutane and 2-bromobutane. The products of all four reactions will be analyzed with gas chromatography‚ which separates organic compounds to see how each reaction’s product are formed under
Premium Chemistry Chemical reaction Acetic acid
Preparation of 1-bromobutane from 1-butanol by SN2 reaction Objective: 1. To study the preparation of 1-bromobutane from 1-butanol by an SN2 reaction 2. To study the method of purification of an organic compound by simple extraction 3. To study the test of identification of alkyl halide Chemicals and Apparatus: ~18.0 g 1-butanol‚ ~20.0 g sodium bromide‚ 15 ml of concentrated sulfuric acid‚ anhydrous magnesium sulfate‚ ~10 ml of 5% aqueous sodium bicarbonate‚ ~1 ml of sodium iodide – acetone reagent‚ 1 ml of
Premium Sulfuric acid Alcohol Bromine
Comparison of Three Isomers of Butanol Introduction An alcohol’s reactivity is determined based on the attachment of their hydroxyl functional group. The location of this hydroxyl functional group will impact the molecular structure of the alcohol‚ making it either primary (1° )‚ secondary (2° )‚ or tertiary (3° ). The purpose of this experiment is to observe and predict the reactions that take place between all three alcohols and an oxidizing agent‚ as well as to test our theories of how the
Premium Alcohol
A: Dehydration of 1-butanol & 2-Butanol/Part B: Dehydrobromination of 1-Bromobutane & 2-Bromobutane Abstract The objective of this experiment is to successfully perform a dehydration of 1-butanol and 2-butanol‚ also dehydrobromination of 1-bromobutane and 2-bromobutane to form the alkene products 1-butene‚ trans-2-butene‚ and cis-2-butene. The dehydration reactions react under and acid-catalysis which follows an E1 mechanism. It was found that dehydration of 1-butanol yielded 3.84% cis-2-butene
Premium Acid Organic reaction Alkene
Introduction The production of acetone and butanol by means of solvent-producing strains of Clostridium spp. was one of the first large-scale industrial fermentation processes to be developed‚and during the first part of this century it ranked second in importance only to ethanol fermentation. The reason for the almost total demise of this fermentation in the early 1960s was the inability of the fermentation process to compete economically with the chemical synthesis of solvents. However‚ interest
Premium Maize Acetone Starch
Discussion and Conclusion: Preparation of 1-Bromobutane The purpose of this experiment was to demonstrate the conversion of a primary alcohol‚ 1-butanol‚ to a primary bromoalkane‚ 1-bromobutane‚ a SN2 reaction. The conversion of 1-butanol to 1-bromobutane relies on sulfuric acid which plays two important roles. First‚ it protonates the alcohol of 1-butanol to form an oxonium ion which is a good leaving group. Secondly‚ it produces the hydrobromic acid‚ the nucleophile‚ which attacks 1-butanol causing
Premium Marketing Management Strategic management
of Three Isomers of Butanol Introduction: An alcohol’s reactivity is determined based on the attachment of their hydroxyl functional group. The location of this hydroxyl functional group will impact the molecular structure of the alcohol‚ making it either primary (1° )‚ secondary (2° )‚ or tertiary (3° ). If the OH is bonded to only one other carbon‚ it is a primary alcohol (eg. 1-butanol); if bonded to two other carbons‚ it is a secondary alcohol (eg. 2-butanol); if bonded to three
Premium Alcohol Carbon