lab‚ caproic acid was synthesized in a multi-step process that involved the synthesis of three intermediates – diethyl n-butylmalonate‚ potassium n-butylmalonate‚ and n-butyl malonic acid respectively. An IR was used to characterize the starting material‚ n-bromobutane‚ and the first intermediate‚ diethyl n-butylmalonate; while IR and NMR were used to characterize the final product‚ caproic acid. Reactions‚ Mechanism and Theory Caproic acid a.k.a n-hexanoic acid is a carboxylic acid derived from
Premium Distillation Carboxylic acid Alcohol
of acetylsalicylic acid Results and Data treatment (A) Preparation of aspirin i) Details about the reactants Reaction of the acetylation of salicylic acid is following From the balanced reaction above‚ it can be seen that the stoichiometry between salicylic acid and acetic anhydride is 1: 1. In this experiment‚ 21.7mmol of salicylic acid was used to react 6.0mL of acetic anhydride and salicylic acid was limiting reagent. The expected amount of salicylic acid used: 21.7/1000*138
Premium Carboxylic acid Aspirin
covalent bond between these amino acids? Amine and Carboxylic acid = Amide 2. When the covalent bond is built between alanine and glycine‚ which functional group will alanine use for peptide bond? Carboxylic Acid 3. When the covalent bond is built between alanine and glycine‚ which functional group will glycine use for peptide bond? Amine 4. When the covalent bond is built between glycine and alanine‚ which functional group will alanine use for peptide bond? Carboxylic Acid; the NOOH group of forms the
Premium Amino acid Protein Oxygen
Acid-Base Extraction: Separation of an Organic Acid‚ Base and a Neural Compound Introduction/Background Acid base extraction is a widely used commercial method in separating acids‚ bases and neutral compounds. This is concept is based on several physical properties of the compounds‚ such as boiling point‚ melting points and solubility. The different solubility properties of the protonated and non-protonated forms of these compounds depend on the functional groups present‚ such
Free Acid Chemistry Carboxylic acid
Separation of Amino Acids by Paper Chromatography Chromatography is a common technique for separating chemical substances. The prefix “chroma‚” which suggests “color‚” comes from the fact that some of the earliest applications of chromatography were to separate components of the green pigment‚ chlorophyll. You may have already used this method to separate the colored components in ink. In this experiment you will use chromatography to separate and identify amino acids‚ the building blocks of proteins
Premium Chromatography Amino acid Acid
Trimyrisitin to Sodium Myristate to Myrisitic Acid Mandy Boyle Chem 213‚ Section 002 Due Date: December 3‚ 2009 I. Introduction People encounter esters everyday in both natural and synthesized forms. Esters are present in a variety of common compounds‚ from fragrances to animal fat (McMurry‚ 2008). Although these esters can undergo many different important reactions‚ this lab is particularly interested in the hydrolysis of esters into carboxylic acids and alcohols. Companies such as Dove‚ Palmolive
Premium Acetic acid Ester Alcohol
Acetylsalicylic Acid (Aspirin) Synthesis Telow‚ AJV Sumicad‚ CJ‚ Tavanlar‚ EMMT‚ Chem 40.1‚ Institute of Chemistry‚ University of the Philippines Los Baños I. Introduction Organic synthesis is the process where a desired organic compound is constructed or prepared from commercially available materials. The objective of organic synthesis is to design the simplest synthetic routes to a molecule. Aspirin‚ also known as acetylsalicylic acid is as salicylate drug often used as analgesic
Free Aspirin Acetic acid Carboxylic acid
Carboxylic acids are compounds which contain a carboxyl group‚ -COOH group‚ where the -COOH group is attached either to a hydrogen atom or to an alkyl group. One of the example of carboxylic acid is benzoic acid( benzene carboxylic acid) which has a benzene connected to the carboxyl carboxyl group‚ -COOH group. It has a formula of C6H5COOH. The carbon atom of a carboxyl group has a high oxidation state. Therefore‚ that many of the chemical reactions used for their preparation are oxidations. In
Premium Oxygen Alcohol Hydrogen
Formic acid is known to be the simplest carboxylic acid‚ and it is an important factor in chemical synthesis and occurs naturally. The chemical formula for Formic Acid is CH202‚ and is mostly found in the venom of bee and ant stings. Formic acid is clear and colorless with a pungent odor. Formic acid is used in many ways; Formic acid is used to preserve livestock. It is also sprayed on animal food and fresh hay to reduce the decay rate. It can also be used as a pesticide to protect bee
Premium Acetic acid Carboxylic acid Oxygen
Synthesis of Salicylic Acid Experimental Data: 1. Mass of methyl salicylate used: 0.232 g 2. Theoretical yield of salicylic acid: 0.211 g 3. Volume H2SO4 added‚ with units (drops or mL): 3mL 4. Mass of crude salicylic acid obtained: 0.250 g 5. Volume of water used as recrystallizing solvent: 2 mL 6. Mass of purified salicylic acid: 0.134 g 7. Percent yield of purified salicylic acid from reaction: 63.5% 8. Melting point of purified product: 158-160 oC 9. Name of NMR solvent used and
Premium Carboxylic acid Salicylic acid Acetic acid