EXPERIMENT 3: INTRODUCTION TO TITRATION – DETERMINATION OF THE MOLARITY AND CONCENTRATION OF SULPHURIC ACID BY TITRATION WITH A STANDARD SOLUTION OF SODIUM HYDROXIDE INTRODUCTION Reaction of acid and base is one of the most common reaction in chemistry. This reaction is also widely known as neutralization. In this experiment‚ we used titration technique which involves accurately measuring the volume of a solution required to react with another reagent. An indicator must be used to determine the
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rocks Acetic Acid Looks like a clear liquid Solution of Sodium Thiosulfate Looks like a clear liquid Granular Zinc Looks like shredded pieces of silver Iodine Crystals Looks like small silver balls Zinc Ion and Iodine-Iodide-Triiodide ion in water Looks like a brown liquid Solid Zinc Iodide Looks like a white powder Mineral Oil Looks like a clear liquid Silver Nitrate Looks like a clear liquid Magnesium Turnings Looks like a small silver curved figure 3M Hydrochloric Acid (HCL) Solution
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10-fold dilution of this ionic iron solution and 5 drops of concentrated HNO3 was made. This solution served as the source of ionic Iron for the remainder of the lab and was labeled “stock ionic Iron solution.” Next‚ a 50-mL aqueous ionic Iron and FerroZine® complex solution was prepared by adding 5.00mL stock ionic Iron‚ 3-mL of acetic acid buffer‚ 2-mL of 5% hydroxylamine hydrochloride‚ allowing five minutes for hydroxylamine to reduce Fe3+ to Fe2+‚ adding 2.5-mL of 0.01 M FerroZine® solution‚ and
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Chamberlin Date: 29 April 2017 Experiment Title: Acid-Base Titration Abstract: Vinegar is a common household item containing acetic acid as well as some other chemicals. This experiment is designed to determine the molar concentration of acetic acid in a sample of vinegar by titrating it with a standard solution of NaOH. CH3COOH(aq) + NaOH(aq) -> CH3COONa(aq) + H2O(l) By adding the sodium hydroxide‚ which is a basic solution‚ to the acetic acid‚ which is an acidic solution‚ a neutralization
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Determination of Ka for a Weak Acid Introduction In the experiment preformed the objective is to titrate a weak acid with a strong base. In a titration of a weak acid with a strong base the titrant is the strong base and the analyte is a weak acid. The reaction that will occur is the direct transfer of protons from the weak acid to the hydroxide ion. The data gathered will be represented on the titration curve‚ a graph of the volume of titrant being the strong base plotted against the pH .The
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because of the amount of time given in summer lab we had to save time and cut some days out. We were able to do this by being given our own Salicylic acid (SA) prepared for us instead of having to used wintergreen to make it and recrystallize it. In addition‚ we skipped the qualitative test of our purity for SA and Aspirin (ASA). The first part of this experiment is the preparation of ASA from SA were‚ we prepared our aspirin from the collected salicylic acid. A screw-capped vial was weighed empty to
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Title: ACID BASE TITRATION. Objectives: 1. To determine the concentration of acid using titration. 2. Skills of titration techniques. Apparatus: 1. 250 volumetric flask 2. 10mL measuring cylinder 3. 25mL pipette 4. 50mL burette 5. 250mL beaker 6. 150mL conical flask 7. Retord stand 8. White tile 9. Stopwatch 10. Pipette bulb Chemicals: 1. HCl solution 2. 0.1M NaOH solution 3. H2SO4 solution 4. Distilled water 5. phenolphthalein
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The purpose of the Weak Acid Dissociation experiment is to determine the dissociation constant of a weak acid experimentally by using acid-base titration with a strong base and stoichiometry. An acid-base titration is a method by which a basic (or acidic) solution of unknown concentration is reacted with an acidic (or basic) solution of known concentration. (1) The pH in acid-base titration is measured using a pH meter or color changing indicator‚ such as phenolphthalein‚ as the known solution is
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Abstract: The purpose of this lab was to synthesize triphenylmethanol from benzophenone and bromobenzene by the formation of a Grignard compound with the reagents bromobenzene and magnesium metal. The bromobenzene was first transformed into the Grignard compound and was then reacted with the benzophenone to make the final product. The mixture was then mixed with sulfuric acid and the organic layer was extracted via a separatory funnel. The mixture was then recrystallized from methanol and was allowed
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Acetylsalicylic acid is the active pharmaceutical ingredient in aspirin and can be synthesized by the esterification reaction of salicylic acid and acetic anhydride in the presence of an acid catalyst. An esterification reaction is when an acid is converted into an ester by combining with an alcohol and removing a water molecule. When heating the salicylic acid mixture in the warm water bath‚ the mixture should be removed from the bath within 8 minutes‚ to reduce the chance of the acetylsalicylic acid decomposing
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