observe the reactions of specific aqueous solutions with specific aqueous reagents. Introduction: A solution is as a homogeneous mixture containing two or more substances. Reagents are added to solutions to create a chemical reaction or added to see if anything occurs. Reagents can be added to solutions to see if there is a presence of other substances. For example‚ iodine added to a lead solution. Iodine would be the reagent and would cause a chemical reaction confirming the presence of lead. We
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Determining the Stoichiometry of Chemical Reactions Objective In this lab we took Fe(NO3)3 and NaOH and mixed 7 different mole ratios in graduated cylinders to determine what the mole ratio is. We also did the same thing with solutions of CuCl2 and Na3PO4. We determine the mole ratios by graphing the volume of reactant #1 vs. volume of precipitate for each reaction. Data Part 1.) Cylinder 1 2 3 4 5 6 7 Fe(NO3)3‚ 0.1 M‚ ml 5 10 12 15 17 20 24 NaOH‚ 0.1 M‚ ml 55 50 48 45
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dealing with such small quantities of reagents‚ any small inaccuracy in measurement creates a large difference in actual yield from theoretical yield. Through simple molar calculations‚ using the coefficients in the balanced chemical equation( CaCl2(aq) + 2NaOH(aq) Ca(OH)2 + CaCl2)‚ the limiting reagent could be determined from the volumes of reactants used. The number two to four tests turned out as expected‚ NaOH and CaCl2 respectively being the limiting reagents. In the second test‚ according to
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of thioacetamide TS and 1 mL of glycerin base TS‚ and heat in a boiling water bath for 20 seconds. Use the mixture immediately. Lead Nitrate Stock Solution— Dissolve 159.8 mg of lead nitrate in 100 mL of water to which has been added 1 mL of nitric acid‚ then dilute with water to 1000 mL. Prepare and store this solution in glass containers free from soluble lead salts. Standard Lead Solution— On the day of use‚ dilute 10.0 mL of Lead Nitrate Stock Solution with water to 100.0 mL. Each mL of Standard
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The Grignard Synthesis of 3-methyl-3-heptanol In this experiment‚ an example of an organometallic compound which has a carbon magnesium bond will be utilized to form a tertiary alcohol. Grignard reagents have been extremely useful in the synthesis of a large number of classes of organic functional groups. Although Grignard reagents are unstable and decompose in air and moisture‚ they can be prepared and used immediately with moderate difficulty in the undergraduate organic chemistry laboratory
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Exercise No. 8 CARBOXYLIC ACIDS AND ACID DERIVATIVES I. OBJECTIVES: • To investigate the physical and chemical properties of Carboxylic acid and its derivatives • To understand the reactions of carboxylic compounds and derivatives. II. EXPERIMENTAL RESULTS Solubility of Carboxylic acids in 10% NaHCO¬3 Acetic acid - formation of bubbles Benzoic acid - formation of bubbles Test for Acetic acid NaOH + Acetic acid - blue litmus paper turned red NaOH + Acetic acid + FeCl3 - red colored
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Discussion: For this experiment to occur‚ the limiting and the excess reagents needed to be determined. The limiting reagent was picked based upon the single displacement that was going to occur when the two substances‚ iron and copper(II)sulfate‚ were mixed together in water. Seeing that iron was going to displace copper and take its place‚ it was chosen to be the limiting reagent with the condition that if it was in excess then after the displacement was completed‚ there will be iron precipitate
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REPORT EXPERIMENT 9 CARBOXYLIC ACID AND DERIVATIVES Date: January 19‚ 2004 Objectives: 1. To understand the reactions of carboxylic compounds and derivatives. 2. To know the methods for preparing carboxylic acid derivatives. 3. To know the methods for testing the carboxylic acid derivatives. Experimental Procedures: 9.1 Solubility 1. Prepare 3 test tubes with 3 ml of water in each. 2. Place 3 drops of acetic acid‚ benzoic acid‚ and oxalic acid in separate test tubes. 3. Shake and observe
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A carboxylic acid is an organic acid characterized by the presence of at least one carboxyl group. The general formula of a carboxylic acid is R-COOH‚ where R is some monovalent functional group. A carboxyl group (or carboxy) is a functional group consisting of a carbonyl (RR’C=O) and a hydroxyl (R-O-H)‚ which has the formula -C(=O)OH‚ usually written as -COOH or -CO2H. Carboxylic acids are Brønsted-Lowry acids because they are proton (H+) donors. They are the most common type of organic acid. Among
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The first days in the lab will be used to practice with collecting bare footprints from different individuals using the bare footprint reagent cream. To get access to the lab‚ a Practical Risk Assessment must be made (see appendix I)‚ and three Health & Safety courses must be completed (see appendix II). After practicing with collecting bare footprints‚ the study starts with collecting footprints from six specific participants‚ whose footprints have already been collected by two other investigators
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