was to learn how to use salicylic acid to make aspirin. Aspirin is the most widely used over-the-counter drug in the world. The average tablet contains about 325 milligrams of acetylsalicylic acid with an inert binding material such as starch. Aspirin is used to relieve pain‚ reduce inflammation‚ and lower fever. Aspirin originally was derived by boiling the bark of the white willow tree. Although the salicin in willow bark has analgesic properties‚ purified salicylic acid was bitter and irritating
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Acid Base Titration bre’ana March 1‚ 2013 Purpose: The purpose of this experiment is to determine the concentration of a solution of NaOH by titration with a standard solution of HCl. It was also the purpose to determine the concentration of a sample of white vinegar by titration with a standard solution of NaOH. Introduction: Using the method of titration is how the experiment gets to the conclusion of the concentration of a solution. When doing this experiment‚ measurement is very important
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goals of this experiment are to determine if the products derived from amide synthesis and Williamson Ether Synthesis are identical‚ and if one of the synthetic routes is more advantageous than the other. In Part 1‚ an attempt to synthesize acteophenetidin crystals by amide synthesis was made. We began by removing the colored impurities from the p-Phenetidine (reddish-brown) by placing 2g of the sample in 38 mL of hydrochloric acid and heating the solution to boiling point. Upon reaching just below
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PREPARATION OF BIODIESEL FROM WASTE COOKING OIL In partial fulfillment of the requirements for the award of the degree of Bachelor of Engineering in Mechanical Engineering Submitted by Ritesh Shukla Pankaj Singh Bais Ciby Ninan Ankush Deshmukh Under the guidance of Prof. SUSHANT S. SATPUTALEY (Assistant Professor of Mechanical Engineering) Academic Year 2010-11 Department of Mechanical Engineering ST. VINCENT
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Starting with the weight of .198 g of salicylic acid‚ the moles of the reactant was determined to be 1.43 x 10-3‚ as shown in Equation 3. The purified aspirin product was a white powder that had a weight of .140 g. The number of moles of the purified aspirin product after extraction was 7.77 x 10-4 as shown in Equation 4. These two moles calculated a chemical yield of 54.3% as shown in Equation 5. The melting point of the pure aspirin product was ranged at 117.8-125.2C as shown in Table 1.
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SYNTHESIS OF ESTERS USING GREEN AND NON-GREEN CHEMISTRY Abstract Esters are a class of organic compounds with the general formula RCOOR’. Ester also contributes the flavor and aromas in fruits and flowers. The esterification reactions will use in the procedure‚ which are the interaction of a carboxylic acid with an alcohol‚ aided by an inorganic acid catalyst (H2SO4). Moreover‚ the green method will not use any catalyst but using heating source instead (microwave). Based on the comparison of
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An Unknown Amino Acid From Titration Abstract Experiment 11 used a titration curve to determine the identity of an unknown amino acid. The initial pH of the solution was 1.96‚ and the pKa’s found experimentally were 2.0‚ 4.0‚ and 9.85. The accepted pKa values were found to be 2.10‚ 4.07‚ and 9.47. The molecular weight was calculated to be 176.3 while the accepted value was found to be 183.5. The identity of the unknown amino acid was established to be glutamic acid‚ hydrochloride. Introduction
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Experiment #5: Esterification of Methyl Benzoate from Benzoic Acid October 28‚ 2010 Abstract: This experiment was conducted to synthesize methyl benzoate from benzoic acid and methanol by using the Fischer esterification method. Methanol (12.5ml) and Benzoic acid (4.9 grams) are heated together in the presence of concentrated sulfuric acid (1.5ml) until equilibrium is achieved. A reflux apparatus is set up for 1 hour to carry out the reaction at the boiling point of the solvent (Methanol
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Synthesis of Isopentyl Acetate (Banana Oil) Using a Fischer Esterification Reaction Zhenshu Wang (Stan) TA: Aaron League September 23‚ 2012 Purpose: The purpose of the experiment was to perform the acid-catalyzed Fischer Esterification of acetic acid and isopentyl alcohol to form isopentyl acetate‚ or banana oil‚ which is used in flavor industries. The equilibrium of the reaction was changed by adding an excess amount of acetic acid. The reaction was refluxed and product was purified by extraction
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NUCLEIC ACIDS I.BASIC CONCEPTS II.CLASSES III.CHEMICAL NATURE IV.FUNCTION I.BASIC CONCEPTS NUCLEIC ACIDS polymeric macromolecules‚ or large biological molecules‚ essential for all known forms of life are made from monomers known as nucleotides Each nucleotide has three components: a 5-carbon sugar‚ a phosphate group‚ and a nitrogenous base If the sugar is deoxyribose‚ the polymer is DNA. If the sugar is ribose‚ the polymer is RNA. Together with proteins‚ nucleic acids are the most
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