Synthesis of DEET Abstract: For this experiment m-toluic acid was reacted with thionyl chloride resulting in a nucleophilic acyl substitution which could then be used to create DEET with excess diethyl amine (Figure 1). This was done by adding diethyl amine drop wise using a seperatory funnel which resulted in a gas formation which was controlled with a condenser attached to a gas vacuum. The resulting mixture was then washed to remove excess acids and bases and rotovapped. DEET was synthesized
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Experiment 23: Synthesis of an Alkene April 5‚ 2013 Purpose: Results and Discussion The weight of our n-Butyl Bromide sample (actual yield) was 0.09g. The percent yield was found to be 4.38%. Only 0.09g of the theoretical 2.055g yield was obtained. The boiling point was 104° C‚ which is higher than the literature value of 101° C. This is due to the sample being somewhat impure‚ as impurities tend to increase boiling point. When IR spectroscopy was performed‚ there were no OH stretches
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EXP-10 CHEM 233L SYNTHESIS OF p-BROMOANILINE Introduction: In this experiment‚ p-bromoaniline was synthesized in three steps starting from aniline. Since the amino group of aniline is a strong activator of aromatic ring‚ direct bromination is impractical (equation 1). In order to make a desired product‚ amino group needed to be protected as the acetamide which also maintained ortho and para position but slowed down the rate of reaction (equation 2). Slow reaction rate would increase
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GRADUATE SCHOOL MASTER IN BUSINESS ADMINISTRATION SYNTHESIS NO.1 (MODULE NO. 1-3) HUMAN RESOURCE MANAGEMENT Submitted by: WILLIAM L. BERMEJO MBA-1 Submitted to: MS. ESTELA MARIE O. VERANA‚ D.M. Professor November 23‚ 2013 In the first session‚ we learn deeply and discuss the overview of human resource management. Human resource management (HRM‚ or simply HR) is the management process of an organization’s workforce‚ or human resources. It is responsible for the attraction‚ selection‚ training
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Synthesis of Cyclohexanol Author: Ahmed Ayyash 06/06/13 Introduction: In this experiment‚ cyclohexanol was prepared from an initial cyclohexene. However‚ this occurred over a number of steps‚ these are out lined below. 1. Cyclohexene + aqueous acid cyclohexyl cation 2. cyclohexyl cation + hydrogen sulphate + water protonated cyclohexanol + cyclohexyl hydrogen sulphate 3. cyclohexyl hydrogen sulphate protonated cyclohexanol + HSO4 4. protonated cyclohexanol + HSO4
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Synthesis Essay Four The minimum drinking age articles “Tempest in a Bottle”‚ by Shari Roan‚ “The Perils of Prohibition”‚ by Elizabeth M. Whelan‚ “The Minimum Legal Drinking Age: Facts and Fallacies” by Traci L. Toomey‚ Carolyn Rosenfeld‚ and Alexander Wagenaar‚ “De-Demonizing Rum: What’s Wrong with “Underage” Drinking?” by Andrew Stuttaford‚ are articles that represent why underage people shouldn’t be allowed to drink alcohol beverages. In the “Tempest in a Bottle”‚ by Shari Roan‚ explains
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Anthony Felix 10/27/11 Che12ALR Synthesis of Diphenylacetylene Observation of Results: 1‚2-dibromo-1‚2-diphenylethane | 0.204g | Diphenylacetylene | 0.087g | Theoretical yield | 0.107g | Percent yield | 81.3% | Melting point range of diphenylacetylene | 57- 60°C | Average melting point | 58.5°C | Average literature melting point | 60.0°C | Percent error of melting point | 2.5% | Calculations: Theoretical yield: Limiting reagent (LR) x M.W. (LR) x Mole to Mole ratio x M.W. (product)
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Puritan Synthesis Puritans were European immigrants that had many beliefs. Some of the common beliefs were that only certain people could talk to God‚ and that God is mean‚ angry‚ and vengeful. People would often write Literature to express the way they view God‚ or to write a History that often has to due with themselves. Most Puritan Sermons‚ Histories‚ and Poems all include a Lesson throughout and Glorify their God. Both “Upon the Burning of our house‚” by Anne Bradstreet and “Sinners in
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Almenny Larchick John’s Crew JAM 7 Growth Synthesis Engine‚ Pitstop‚ Track Time. New words and meanings flow around in my head. This project opens me up to new information I would have never considered. Pushing me to work‚ helping me learn new things. The central idea for my growth see spaces is how I have made growth in my educational understanding this year. This does not include any of my grades but of the knowledge I’ve acquired. I showed growth this year in my mindset vocabulary quiz and
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The Synthesis of Aspirin Chemistry Standard Level Lab Report Data Collection and Processing and Conclusion and Evaluation Date: December 8th‚ 2011 Purpose: The purpose of this lab was to synthesize aspirin‚ determine the theoretical yield‚ compare the percent yield to the theoretical yield and test the purity of aspirin by adding Iron (III) chloride to the product. Hypothesis: I hypothesize that salicylic acid will react with acetic anhydride to produce acetylsalicylic acid (aspirin)
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