Melting Point and Boiling Point of Organic Compounds Bongo‚ Sayre‚ J1 1Student‚ Organic Chemistry 1 Laboratory / B11‚ School of Chemical Engineering‚ Chemistry and Biotechnology‚ Mapúa Institute of Technology ABSTRACT The melting point of a substance is the temperature at which the material changes from a solid to a liquid state while the boiling point is the temperature at which it changes from liquid to solid. In this experiment‚ the main objectives were to determine the effects of the following
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Melting Range Report Name: Date: Lab Section: Selected Known Compounds Name Structural Formula Literature Melting Point Acetanilide C8H9NO 114.3°C Fluorene C13H10 116.5°C Experimental Data Sample Composition 1. 100% Acetanilide 2. 10% Acetanilide 3. 25% Acetanilide 4. 50% Acetanilide Fluorene 5. 75% Acetanilide 6. 90% Acetanilide 7. 100% Fluorene Melting Range 108-116°C 108-112°C 105-112°C 102-109°C 105-112°C 109-115°C 108-114
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Solids: Recrystallization and Melting Points Reference: Chapter 3. Solids: Recrystallization and Melting Points. Read pages 93-94 and 113-117. Experimental procedure‚ pages 118-119. Parts 1-3. Part 1: Melting points of Urea and Cinnamic Acid. Part 2: Melting point of unknown. Part 3: Melting point of Mixture- Urea and Cinnamic Acid (take melting points of mixtures in 1:4‚ 1:1 and 4:1 ratios). Reactions Main Reaction: Not a chemical reaction but a physical reaction. Urea in solid mixed with
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Determine the melting points of two organic compounds known to have the same melting range when pure. b) Determine the mixture melting point of a mixture of the two pure compounds. c) Identify an unknown organic compound by determining its melting point and mixture melting point. Procedure and Observations: Using the procedure outlined in Appendix A of the Lab Manual‚ approximately equal samples of p-Nitrophenol and acetanilide‚ which are known to have the same melting range of 113-114
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------------------------------------------------- MELTING POINT AND BOILING POINT OF ORGANIC COMPOUNDS ------------------------------------------------- ABSTRACT The melting point (MP) and the boiling point (BP) are probably the most widely used physical constant in the field of science. Determining the boiling point and the melting point of a compound helps you to characterize an unknown solid in a quick‚ easy and cheap way. The temperature at which a compound turns from a solid state to a liquid state is known to be the melting point. On
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ago. My wide spread use over the course of human existence is the very reason that no one knows who discovered me. I belong to the group of elements called the transition metal group. I have several oxidation states and I also have a very high melting point which is around 1337.33 Kelvin. That is very high‚ in Fahrenheit it is 1947.92 degrees and in Celsius it is 1064.18 degrees. I am also paramagnetic‚ which means that I have very weak attractions to magnetic forces and can only be attracted when
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evaporating the weight of crude caffeine was .0321g‚ making the percent recovery before sublimation 1.43%. After sublimation the weight of pure caffeine was .0027g‚ making the percent recovery of caffeine after sublimation .12%. The percent recovery of caffeine is less in the second half of the experiment because the crude caffeine had some impurities in it which were taken out by the process of sublimation. The average cup of black tea has about .014g to .07g of pure caffeine in it (MayoClinic
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ABSTRACT Determining the melting point of a solid organic compound is the easiest way to identify the compound and determine its purity at the same time. For actual samples of compounds‚ the melting will occur over a range of temperatures making the melting points into a melting “range”. The difference between the temperature at which the sample begins to melt and the temperature at which it finishes melting‚ or the magnitude of the melting range‚ is a very important criteria of determining the
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Summary of Results A. Melting point of Benzoic Acid Temperature (¡ÆC) Observation Unmelted White salt First liquid appear point 122 Grainy and shiny white Becoming all liquid 125 Clear B. Melting point of unknown #42 1st trial Temperature (¡ÆC) Observation Unmelted Shiny light yellow crystal First liquid appear point 99 Grainy yellow Becoming all liquid 101 Clear 2nd trial Temperature (¡ÆC) Observation Unmelted Shiny light yellow crystal First liquid appear point 95 Grainy yellow
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Extraction and Sublimation of Caffeine from Tea Leaves By: Ashley Barnes CH 236 – P8 Experiment 4 & 4.5 Due: 10/15/2014 Table 1. Table of Reagents Discussion The extraction yield refers to the percent of caffeine in the tea leaves at start of the extraction experiment. Tea leaves had 0.55 grams of mass per eight ounce serving. The weight of the extracted crude caffeine was 0.264 grams. Therefore‚ the extraction yield was 48%. This means that we pulled out almost half of the caffeine
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