11/17/2011 The Preparation of Calcium Carbonate Purpose: To create chalk (calcium carbonate) and to find the percentage yield in order to see the amounts of anhydrous sodium carbonate and calcium chloride were used up. Also to see if there’s any alterations like mass differentials. Objectives: 1. To introduce the concept of “limiting factor” in a chemical reaction 2. To practice a. Writing a balanced equation b. Determining the number of moles of each reactant and product
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Design an experiment to investigate the stoichiometric mole ratio of a chemical reaction. Present your data in terms of the mass of one reactant compared to the mass of one product. Purpose: The experiment will be designed to find out the stoichiometric mole ratio of Barium Chloride and Silver Nitrate yielding a precipitate of Silver Chloride in a Barium Nitrate solution. (BaCl2 + 2AgNO3 -> Ba(NO3)2 + 2AgCl) Research Question: How will the amount of Barium Chloride and Silver Nitrate
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Atrazine (1-chloro-3-ethylamino-5-isopropylamino-2‚ 4‚ 6-triazine‚ CAS: 1912-24-9) was purchased from Dr. Ehrenstorfer GmbH (97.7%‚ Germany). Ethyl acetate (99.8%‚ ANPEL Scientific Instrument (Shanghai) Co.‚ Ltd.) was used as solvent for standard solutions. Acetonitrile used as HPLC eluent was purchased from ANPEL Scientific Instrument (Shanghai) Co.‚ Ltd.‚ KH2PO4·12H2O‚ K2HPO4·2H2O‚ dichloromethane and other chemical reagents used in cultivated media were purchased from Sinopharm Chemical Reagent
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Lab Report Macrocyclic Synthesis (Heme Analog) I. Purpose of Experiment and Introduction The purpose of this lab experiment is to prepare meso-tetraphenylporphin (TPP) and its copper‚ cobalt or zinc complex by condensing benzaldehyde with pyrrole in boiling propanoic acid. II. Introduction and Background There are two types of proteins that function as oxygen carriers: myoglobin (stores the oxygen) and hemoglobin (present in red blood cells and is responsible for oxygen transport)
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Abstract The experiment was conducted‚ which metals manganese (Mn3+)‚ Cobalt (Co3+) and Copper Cu3+ was prepared and acac complexes where also obtained. Recrystallization was performed of which Mn(acac)3 ‚Co(acac)3 and Cu(acac)3 was obtained at percentage yield of 32%‚ 85.6% & 92% for each of acac’s. TLC was performed which results deduced unknown mixture both contained manganese and cobalt since it had the same Rf vaues. Experiment aims The aim of the experiment was to prepare metal
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Purpose: This experiment is used to perform a series of synthesis reactions that convert aluminum foil to alum. Alum is used in cooking‚ to treat wastewater‚ and is used in common deodorant. In this lab a series of four reactions will occur to yield alum. Calculations: Aluminum foil: 0.5035 grams Alum & Watch Glass: 21.7691 grams Watch Glass: 15.1560 grams Alum: 6.6131 gram Theoretical Yield of Alum: 2Al(s) + 2KOH(aq) + 4H2SO4 + 22H20 -> 3H2(g) + 2KAl(SO4)2 + 12H2O(s) 0.5035gAl
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Synthesis and Isolation of Expectorant Guaifenesin By: Ben DuBose Dr. Cossey 3361L Abstract The purpose of this experiment was to isolate and synthesize Guaifenesin. Isolation was performed with the use of two Guai-Aid Tablets‚ each of which contained 400mg of pure Guaifenesin. Reflux‚ a technique used to heat a mixture without evaporating the solution‚ was used to synthesize Guaifenesin through a Williamson Ether Synthesis reaction with an SN2 mechanism. Introduction
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Nitration of Methyl Benzoate Date of Completion: February 29‚ 2012 Date Report Submitted: March 14‚ 2012 Objective of Experiment: The purpose of this experiment is was to synthesize methyl 3-nitro benzoate from methyl benzoate through an electrophilic aromatic substitution reaction. Chemical Equation: Materials: Name of Compound Molecular weight MP/BP Grams Used Moles Used Methyl benzoate 136.16 g/mol -12.5 OC /199.6 OC 0.28g 2.056*10-3 Sulfuric acid 63.01 g/mol 10 OC /337OC 0
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Jacobsen’s Method of Epoxidation of an Alkene | | Abstract Various types of reactions were completed to first create and then use Jacobsen’s catalyst in the asymmetric epoxidation of an unknown alkene with bleach in the laboratory. The chiral epoxide synthesized was then characterized with GC/MS and NMR. With this information the unknown alkene was able to be identified as 4-chlorostyrene. Introduction Organisms have evolved with mechanisms that use specific enantiomers of molecules
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Old Dominion University ORGANIC 214 Alkene Addition Submitted by: Alkene addition: Bromination of (E) Stilbene Introduction: In this lab we used the greener approach‚ which involves the addition of bromine across a double bond. When bromine reacts with E-stilbene (trans-1‚2-diphenylethene)‚ two new chiral carbons are created from the sp2 carbons‚ therefore 3 different dibrominated stereoisomers are possible: meso-(1R‚2S)‚ or the raceminc mixture-(1R‚2R) or (1S‚2S)-dibromo-1‚2-diphenylethane
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