Lab #24- Preparation 4-Methylcyclohexene Introduction: The goals in this lab were to have a reaction occur with 4-methylcyclohexanol and an acid catalyst to form our product of 4-methylcyclohexene via an E1 reaction. This reaction is accomplished by removing the –OH group on 4-methylcyclohexanol via dehydration and to have a double bond form via a loss of a hydrogen on a β-Carbon. Many techniques and skills were developed in this lab. Among them were dehydration‚ isolation‚ drying
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Copper in Silver Nitrate Lab: Making Silver Sabrina Kate S. Carranza – Chemistry Hour 6 I. Purpose: The purpose of this experiment is to distinguish the relationships between reactants and products‚ in addition to expanding on concepts such as single displacement reactions‚ mole ratio values‚ moles to mass‚ theoretical yields‚ limiting reactants‚ excess‚ stoichiometric relationships and percentage errors. II. Hypothesis: /3 -If the copper metal is submerged in the silver nitrate solution
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RECYCLING ALUMINUM PURPOSE To determine the mass of a hydrated aluminum potassium sulfate salt in a sample of impure scrap aluminum from a common beverage can. The sample will be passed through a filter paper using a funnel‚ after being boiled on a hot plate in a fume hood and dissolved in a solution of potassium hydroxide to remove the impurities. By adding an excess of sulfuric acid and cooling the solution in an ice bath‚ the technique of vacuum filtration using a Buchner funnel will be employed
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Experiment 2: Dehydration of an Alcohol: Distillation and Gas Chromatography Preparation of Methylcyclohexenes Purpose: The basic purpose of this experiment is to carry out the dehydration of an alcohol and isolate the reaction products by distillation. Gas Chromatography will be utilized to analyze the reaction mixture. Table of Reagents: Compound (g) Molecular Weight (g/mol) Grams (g) Moles 6 mL of 2-methylcyclohexanol (C7H14O) 114.19 g/mol 6 mL x 0.943g = 5.66 g 1 mL 5.66 g x
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Lab Report 1 Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene Objective: 1. To understand the general process‚ reaction and limitations of Friedel-Crafts Alkylation in regards to Dimethoxybenzene 2. To apply the reaction of Friedel-Crafts Alkylation to dimethoxybenzene Chemical Index: Chemical Structure Molecular Weight Melting Point Boiling Point Acetic Acid C2H4O2 60.05 g/mol 16-17°C 118-119°C T-Butanol C4H10O
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Limiting Reagent and Percent Yield Aim To determine the limiting reagent between the reaction of lead (II) nitrate and potassium iodide. To determine the percent yield of lead (II) iodide. Date Started: 13/4/12. Finished: 19/4/12. Data collection and processing Measurements: * Amount of distilled water: 75.0ml ± 0.5ml. * Mass of watch glass: 31.65g ± 0.01g. * Mass of watch glass + potassium iodide: 32.45g ± 0.01g. * Mass of potassium iodide: 0.8g ± 0.02g. * Mass of watch
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CALCULATIONS Determining the amount Limiting Reagent used. nlimiting reagent = Molarity x Volume or Mass / Molar Mass Example: Limiting reagent is 5mL of 1.0 M HCl nlimiting reagent = Molarity x Volume nlimiting reagent = (1.0 [mol/L]) x 0.005 [L]) = 0.005 mol Determining the qrxn and qcal. qrxn + qcal = 0 -qrxn = qcal qrxn = ΔHrxn x nlimiting reagent qcal = Ccal ΔT qrxn = - Ccal ΔT + mcsolid ΔT (note: only if there is a precipitate formed in the reaction)
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1.TITLE: To prepare isopentyl acetate (isoamyl acetate) 2. AIM: To make an ester referred to as banana oil from acetic acid and isopentyl alcohol 3.THEORY: This ester is often referred to as banana oil‚ since it has the familiar odor of this fruit O O CH3 H+ CH3 CH3C OH +
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(Name) (Course Name) (Instructors Name) (Date) Summary of chemistry lab report Introduction The two factors which affect the yield of products in a chemical reaction is the amount of starting materials (reactants) and the percent yield of the reaction. Many experimental conditions for example temperature‚ and pressure can be adjusted to increase yield of the desired product‚ in chemical reaction‚ but because chemicals react according to fixed mole ratios( stoichometrically)‚ the only limited
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Experiments 4A-C: Synthesis and Component Analysis of an Iron (III) Oxalate Complex My Name TA‚ Section B## Work Performed on 10/23‚ 10/30‚ & 11/4‚ 200# Report due Tuesday‚ November ##‚ 200# 1. Abstract This experiment initially involved the synthesis of an iron (III) oxalate complex with the general formula Kw[Fex(C2O4)y]·zH2O. The variables x‚ y‚ and z were determined through the duration of the entire experiment. From 1.2000g of Fe(NH4)2(SO4)2 were synthesized 1.1###g of K3[FeIII(C2O4)3]·3H2O
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