TITLE : * Analysis of an unknown acetic acid solution OBJECTIVES : * To prepare the sodium hydroxide solution‚ NaOH * To standardise the base against potassium hydrogen phthalate * To analyse the unknown acetic acid RESULTS : A. Preparation of the sodium hydroxide solution Volume of NaOH taken from the stock solution = 3.33 mL B. Standardisation of the base against potassium hydrogen phthalate | 1 | 2 | 3 | Weight KHP | 1.0000 | 1.0004 | 1.0006 | Final volume
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SODIUM gSodium is a chemical element with the symbol Na (from Latin: natrium) and atomic number 11. It is a soft‚ silver-white‚ highly reactive metal and is a member of the alkali metals; its only stable isotope is 23Na. The free metal does not occur in nature‚ but instead must be prepared from its compounds; it was first isolated by Humphry Davy in 1807 by the electrolysis of sodium hydroxide. Sodium is the sixth most abundant element in the Earth’s crust‚ and exists in numerous minerals such
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Observations Figure 1 Figure 2 Figure 3 Figure 1 show the crystallisation reaction when the saturated sodium chloride solution was added to the cool reaction mixture. The salt of p-Toluenesulphonic acid started forming. Figure 2 show the wet crystal after the precipitated salt was being filtered by suction. The wet crystal was light purple in colour. Figure 3 show the end product after drying the wet
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CHM 3120L ANALYTICAL CHEMISTRY I LABORATORY REPORT EXPERIMENT: DETERMINATION OF ASCORBIC ACID BY REDOX TITRATION Name: Section: Date Experiment Completed: 2.0008 g KIO3 x (1 mol/214 g KIO3) = 0.0093495327 mol KIO3 0.0093495327 mol KIO3 / 0.500 L = 0.0186990654 M KIO3 6 Na2S2O3 + KIO3 + 6 H+ → I-+ 3 H2O + 3 S4O62- + K+ + 12 Na+ 0.0187 M KIO3 × 0.025 L = 4.675 x 10-4 mol KIO3 4.675 x 10-4 mol KIO3 x (6 mol Na2S2O3 / 1 mol KIO3) = 0.002805 mol Na2S2O3 0.002805 mol Na2S2O3
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LAB REPORT Introduction: In a chemical change‚ the identities of substances change and new substances form. In an equation the substances on the left are the reactants. The substances on the right are the products. In this experiment the objectives are to observe evidence that a chemical change has taken place. Infer from observations that a new substance has been formed. Identify and record observations that show energy is involved in chemical change observe the color‚ solubility of some substances
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# Now You See It – Copper Cycle Lab The purpose of the lab is to discover what happens when someone executes a series of procedures‚ beginning with copper metal. What is done | What is observed | 1. Started with copper‚ Cu (s). | reddish‚ brownish‚ orange-ish‚ powder-like | 2. Added nitric acid‚ HNO3 (aq). | acid turns blue and smells like chlorine. | 3. Added water‚ H2O (l). | stayed the same | 4. Added sodium hydroxide‚ NaOH (aq). | changed consistency‚ gel-like | 5. Heated the
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calcium carbonate. Calcium carbonate decomposes to calcium oxide and CO2 on heating. Treatment with dilute mineral acids produces corresponding calcium salts with liberation of CO2: CaCO3 + 2HNO3 Ca(NO3)2 + H2O + CO2(g) In this experiment‚ the mineral acid is added in excess to the calcium carbonate and the excess titrated against standard sodium hydroxide. This kind of titration is termed back titration. In this procedure‚ the analyte is consumed using excess titrant and
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To make a standard solution Apparatus: Volumetric flask Method: 1) 2.4g to 2.5g of sulphamic acid was weighed out‚ firstly by weighing the container and the sulphamic acid together‚ then pouring the sulphamic acid into a beaker. The container was then weighed again and the initial weight and the weight of the container alone were subtracted from one another to provide the mass of the sulphamic acid. 2) The sulphamic acid was then dissolved in 50cm³ of distilled water‚ using a glass
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The effect on the pH of Distilled water‚ Potato Solution and Commercial Buffer‚ when Hydrochloric acid (0.1 mol/L) and Sodium Hydroxide (0.1 mol/L) is added Mahima Mandava Mrs. Haist September 23rd‚ 2014 SBI4U1 Background Information: The pH is the measurement of how acidic or how basic a substance can be. The pH scale is used to measure how acidic or basic a living cell can be. The pH scale ranges from 0-14; 0-6 being acidic‚ 8-14 being basic and 7 being neutral. There are many factors
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Experiment 7 Investigating Stoichiometry with Sodium Salts of Carbonic Acid Introduction: The student will perform the experiment in order to find the percent yield by using the theoretical value found using the balanced equation for sodium carbonate as well as sodium bicarbonate. The objective is to stabilize the substances by titrations and finding the percent yield when all the data is collected. The purpose of this procedure is so that the student will get better understanding of stoichiometry
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