NaOH Standardization and Titration of an Unknown Organic Acid Overview: Methods for counting the number of molecules in a sample is a major emphasis of laboratory work. In this experiment we will use the method of titration to count the number of acid molecules in a solution. Measuring mass is a relatively easy procedure to do in the lab (although a balance is expensive). Counting the number of particles requires more effort. Molecular counting can be done by setting an unknown amount of a substance
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Experiment 5- Standardization of NaOH and determination of Molarity of an unknown Acid Objectives 1. Preparation and standardization of a 0.1M NaOH solution 2. To learn the technique of titration 3. Determination of the concentration of an unknown diprotic acid. Introduction Titration can be traced to the origins of volumetric analysis‚ which began in the late eighteenth century. Study of analytical chemistry began in France and the first burette was made by Francois Antoine Henri
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Oxalic Acid Lab Aim: Use acid base titration to determine the number of water molecules in hydrated hydrochloric acid. Apparatus required: Oxalic acid solution 250 cm3 Weighing bottle Digital balance Beaker (250 cm3) Distilled Water Volumetric Flask 250cm3 Filter funnel Pipette Burette 50cm3 Retort Stand Beakers 100cm3 Standardized sodium hydroxide solution 0.1M Pipette filter Conical flasks 250cm3 Phenolphthalein Indicator Procedure 1) Rinse the burette with distilled
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Formula: for NaoH N NaoH = grm KHP / ml NaoH x KHp /1000ml Formula: for HCL (NV) HCL = (NV) NaoH or N HCL V HCL = N NaOH V NaoH N HCL = VNAOH (NNaoH) / VHCL (for more info page 62-63 of the photocopy) KHP = Potassium hydrogen phthalate = KHC8H4O4 = Mw - 204.23 Trial 1: NNaoH = 1grm / 20.6 x 204.23 /1000 = 1grm / 4.21 = 0.24 normal NHCL = 20.6 (0.24) / 39.5 = 4.94 / 39.5 = 0.125 or 0.13 Trial 2: NNaoH = 1grm / 20.8 x 204.23 /1000
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STANDARDIATION OF ACID AND BASE Eunice Ivy B. Gamboa ABSTRACT Solutions of known concentration are prepared by dissolving measured masses of standard acids in distilled water. The concentrations of unknown solutions of sodium hydroxide are determined by titration. An acid solution reacts with a base solution in a "neutralization" reaction. Titrations permit the concentrations of unknown acids/bases to be determined with a high degree of accuracy. In order to analyze unknown acids/bases‚ we must have
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EXPERIMENT 10 Volumetric Analysis I Standardization of NaOH Solution Outcomes After completing this experiment‚ the student should be able to: 1. 2. 3. 4. Demonstrate the concept of quantitative analysis. Make solution and standardize it. Explain the difference between primary and secondary standard solutions. Quantitatively determine the concentration of a base. Introduction Titration is a common method of quantitative analysis used to determine the concentration of an unknown substance in a solution
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| Preparation and standardization of 0.1 M NaOH using KHP | Analysis of unknown solid containing KHP | | Steanie Rodriguez | 6/7/2011 | CHEM-C311 Analytical Chemistry Laboratory July 7‚ 2011 The main purpose of this experiment is to identify an unknown organic acid by conducting various experiments to determine the acid’s unique properties. By determining selected constant properties of the unknown and then comparing these properties to the constant properties of known substances
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2b: Determination of the ASA Content of Aspirin Due Date: September 16‚ 2013 Experiment#: 2b Title: Determination of the ASA Content of Aspirin Aim: To determine the Molar Concentration of NaOH and HCl acid used in their Standardization processes and to determine the acetylsalicylic acid (ASA) content in Aspirin. Materials/Apparatus: materials used are the same as that outlined in the laboratory procedure prepared by the laboratory instructor. Procedure: The procedure used is the same
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Standardization of a NaOH Solution with Potassium Hydrogen Phthlate (KHP) Name:________________________________________________________________ Period:_____ Prelab 1. A 0.8234-g sample of "KHP" required 38.76 mL of NaOH for titration to the phenolphthalein endpoint. What is the exact molarity of the NaOH solution? 2. A 25.00-mL aliquot of an unstandardized HCl solution is titrated with the previously standardized NaOH solution from #1 above. If 32.55 mL of NaOH titrant
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Standardization of hydrochloric acid by sodium carbonate Concentrated hydrochloric acid is roughly 11 M. Pour out into a measuring cylinder about 2 cm3 of concentrated hydrochloric acid. Transfer it to a 250 cm3 flask and make up to the mark with water. Shake well. Put some pure sodium hydrogen carbonate or anhydrous sodium carbonate into an evaporating dish and heat gently over a low flame for about fifteen minutes‚ stirring continuously. Take care not to heat the mass too strongly or fusion
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